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In order to carry out the separation of the azeotropic mixture dipropyl ether + 1-propyl alcohol by extractive distillation, we are studied the influence on the phase equilibria behavior four different solvent: 1-pentanol [2], butyl propionate [3], N,Ndimethylformamide [4] and 2-ethoxyethanol.

为了用萃取性蒸馏法分离二丙醚和1-丙醇组成的共沸混合物,我们正在研究4种不同溶剂对相平衡行为的影响:1-戊醇[2]、丙酸丁酯[3]、N,N-二甲基甲酰胺[4]和2-乙氧基乙醇。

As can be seen in Fig. 5, dipropyl ether will be recovered in the distillate using 1-pentanol, N,N-dimethylformamide and 2-ethoxyethanol as entrainers and butyl propionate is the only entrainer studied that inverts the volatility of the azeotropic mixture.

从图 5可以看出,使用1-戊醇、N,N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收,丙酸丁酯是唯一与共沸混合物挥发性相反的共溶剂。

Acrylic-oil, acrylic cool are commonly used such as acrylic paint, clear acrylic via ethhyl and butylacralate, in the resin introduction of hydroxyl and carboxylated to aminosulfonic cross-linkers gubernacular as a tree.

丙烯酸型平油,凡是拔取羟基丙烯酸酷如丙烯酸不纬乙酯和丙烯酸共聚,在树脂洋引进羟基和羧基,以氨基树胎作为接联剂。

Water, Kaolin, Montmorillonite, Stearic Acid, Cetyl Alcohol, Glycereth-26, Glyceryl Stearate, Peg-100 Stearate, Aloe Barbadensis Leaf Juice, Triethanolamine, Titanium Dioxide, Menthyl Pca, Lauryl Pca, Fragrance, Diazolidinyl Urea, Propylene Glycol, Ethoxydiglycol, Methylparaben, Citric Acid, Panax Ginseng Root Extract, Zinc Pca, Copper Pca, Yellow 5, Blue 1

水,高岭土,蒙脱土,硬脂酸,鲸蜡醇,Glycereth-26,甘油硬脂酸酯,培格100硬脂酸,芦荟叶汁,三乙醇胺,二氧化钛,薄荷醇,香料,尿素醛,丙二醇,乙氧基二甘醇,对羟基苯甲酸甲酯,柠檬酸,人参精华,锌,铜,黄色5#,蓝色1#。

Water, methanol and ethyl acetate extraction method were used to extract non-oil components from Myrtus communis Linn. leaves, and then radical scavenging activity and antioxidant role of these extracts were investigated using four chemiluminescence systems and two colorimetric systems.

采用水提取法、甲醇-水提取法和乙酸乙酯提取法3种方法从香桃木叶中提取非精油组分,然后用4种化学发光体系和2种比色体系检测其清除自由基和抗氧化作用。

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR), among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-(2'-glycerin)-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl)-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究,利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物,经化学方法和波谱技术(红外,质谱,一维和二维核磁共振谱)鉴定了二十五个化合物的结构,其中四个为新的化合物,它们分别是:异海松-15-烯-3β,8β,20-三醇;苯乙醇-3-O-(2'-甘油基)-5-O-β-D-吡喃葡萄糖甙;3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙;迷迭香酸乙酯。

A new method for the synthesis of 1 methyl 3 propyl pyrazol e 5 carboxlic acid from 2 pentanone and diethyl oxalate is reported.

以 2 -戊酮和草酸二乙酯为起始原料,经缩合、与甲基肼环合、水解等三个步骤合成了 1 -甲基-3-丙基吡唑-5 -羧酸。

Triphosgene ; carbamic acid ethyl ester ; phthalimide

三光气;胺基甲酸乙酯;邻苯二甲酰亚胺

Results Six compounds were isolated and identified as:5α,8α-epidioxy-(22E,24R)-ergosta-6,22-dien-3β-ol,scopoletin,isofraxidin,p-hydroxy benzaldehyde,3,4,5-trimethoxy benzoic acid,protocatechuic acid ethyl ester...

结果得到6个化合物,分别鉴定为:5α,8α表二氧(22E,24R)麦角甾6,22二烯3β醇、东莨菪素、异秦皮啶、对羟基苯甲醛、3,4,5三甲氧基苯甲酸、原儿茶酸乙酯。结论化合物Ⅰ~Ⅵ均为首次从该属植物中分离得到。

Described in chapter 3 is the immediate application of the Clemmensen reductive rearrangement reaction to the polycyclic system as illustrated in a elaboration of the 5-6-7 tricyclie core skeleton of Stemona alkaloids in 5 steps: N-alkylation, [3, 2] -sigmatropic rearrangement, Dieckmann condensation, oxidative cyclization, reductive rearrangement, starting from ethyl pipecolinate hydrochloride.

我们以哌啶酸乙酯为起始原料,经氮烷基化,[3,2]-σ重排,Dieckmann缩合,自由基环化,6-6-6元环系到5-6-7元环系的还原重排五步反应,高收率地构筑了百部生物碱的5-6-7氮杂三环骨架,并用X射线晶体衍射法确定了其结构。

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