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Tebufenpyrad, a new high effective pyrazoleamide acaricide , was synthesized from 1-methyl-3-ethyl-4-chloro-5-pyrazolecarbon acid and 4-t-butylbenzylamine, the raw material are propionyl pyruvic ethyl ester and 4-t-butyl benzylchloride.

吡螨胺是一种新型、高效的吡唑酰胺类杀螨剂,本文以中间体1-甲基-3-乙基-4-氯-5-吡唑甲酸和4-叔丁基苄胺合成,起始原料丙酰丙酮酸乙酯和4-叔丁基苄氯,总收率为61.23%。

Eleven novel 2-alkylthio-5-(5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine-5-yl)-1,3,4-oxadiazole derivatives (5) and six novel 2-alkylthio-5-(5,7-dimethyl-1,2,4-triazolo[1,5-a]pyrimidine-5-yl)-1,3,4-thia- diazole derivatives (8) have been designed and synthesized by using 5-amino-3-ethoxycarbonyl-1H-1,2,4-triazole as a starting material.

以5-氨基-1H-1,2,4-三唑-3-羧酸乙酯为起始原料,设计合成了11个新型的2-取代硫醚-5-(5,7-二甲基-1,2,4-三唑并[1,5-a]嘧啶基)-1,3,4-恶二唑类化合物(5)和6个新型的2-取代硫醚-5-(5,7-二甲基-1,2,4-三唑并[1,5-a]嘧啶基)-1,3,4-噻二唑类化合物(8)。

The intermediate of flazasulfuron weedicide ,2-amino-4,6-dimethoxypyrimidineis conveniently obtained by treating 2-amino-4,6-dihydroxypyrimidinewith diazomethane at 20 °C for 24h.

本文利用硝酸胍和丙二酸二乙酯为起始原料,经环合及甲氧基化两步反应得到除草剂啶嘧磺隆的中间体:2-氨基-4,6-二甲氧基嘧啶。

The effects that isopropyl xanthogen ethyl formate is synthesized with isopropyl xanthate under differ conditions has been studied.

考察了不同条件对异丙基黄药合成异丙基黄原酸甲酸乙酯的影响。

Reduction of 2-bromodifluoromethyl substituted propargyl vinyl ether afforded the difluorovinyl propargyl ether, which rearranged to the corresponding allene bearing a gem-difluoromethene in the mid-aliphatic chain.

第三部分,在碱性条件下,α-氟烷基乙酸乙酯与炔丙醇反应制备了一系列的氟烷基取代的炔丙基烯基醚,并研究了它的Claisen重排反应,得到了2,4-不饱和的氟烷基酮。

The results show that the ethyl acetate extract of Alpinia oxyphylla Miquel possesses strongest DPPH radical scavenging activity and reducing power in a concentration-dependent manner.

在还原能力、清除DPPH自由基和羟自由基方面,乙酸乙酯提取物表现出了很强的抗氧化能力,呈现剂量依赖关系。

Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a~3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a~7c) in the presence of triethyl phosphite.The compounds 7a~7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中,在亚磷酸三乙酯存在下,采取高度稀释的方法,使4,5-二氰基-1,3-二硫杂环戊二烯-2-酮分别和多缩硫杂冠醚进行交叉偶联反应,成功地得到了不对称的2,3-二氰基四硫富瓦烯衍生物。

The swelling properties of epoxy vinyl ester resin/2-hydroxyethyl methacrylate copolymeric hydrogels were investigated.

该文研究了酚醛环氧型乙烯基酯树脂/甲基丙烯酸-β-羟乙酯共聚水凝胶的溶胀性质。

A series of hydrogels based on macromonomer novolac epoxy vinyl ester resin and hydrophilic-2-hydroxyethyl methacrylate were synthesized by bulk copolymerization.

采用大分子单体酚醛环氧型乙烯基酯树脂与亲水性单体甲基丙烯酸-β-羟乙酯为原料,以本体聚合方法制备了一系列新型水凝胶。

A novel anionic gemini surfactant,didodecyl-ethoxylate bis-sodium sulfate was prepared in three steps using lauryl alcohol,glycol-epiglyceride and chlorosulfonic acid as raw materials and BF_3-ethyl ether as catalyst.The chemical structure of the product was confirmed by IR spectrum.

以十二醇、乙二醇二环氧甘油醚和氯磺酸为原料,以BF3-乙醚为催化剂,通过三步法制备阴离子型双子表面活性剂双十二烷基乙氧基二硫酸酯钠;红外光谱对其结构进行了表征,测定了其表面活性和发泡力等性能。

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这一模式非常关注商人的网络信用基础。

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