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The effects of different doses of urethane,chloral hydrate and pentobarbital sodium on the electrophysiological characteristic of sciatic nerve of toad in vitro were investigated by means of the extracellular recording action potential.

使用BL-420生物机能实验系统,采用细胞外记录神经干动作电位的方法,观察了氨基甲酸乙酯、水合氯醛和戊巴比妥钠3种麻醉剂对蟾蜍离体坐骨神经电生理特性的影响。

Scattered into ethanol, ethyl silicon is medium tetraethyl ortho-silicate in ammonia catalytic hydrolysis, formed under the condition of the negatively charged with PS silica microspheres due to charge effect between by adsorption to PS microspheres surface, core-shell structure.

将其分散到乙醇/水介质中,正硅乙酸乙酯在氨水催化条件下水解,形成带负电性的二氧化硅与PS微球之间由于电荷作用而被吸附到PS微球表面,形成核-壳结构。

First use soap-free emulsion preparation for polystyrene spheres, and the kernel, Reuse are silicon acetic tetraethyl ortho-silicate in ammonia catalytic hydrolysis, formed under the condition of silica, charged by six water or their cerium, six of methylene amine solution HMT (4) into the negatively charged, uniform cerium oxide coated surfaces to PS microspheres, core-shell structure of PS - CeO2 and PS - SiO2 composite microspheres.

首先用无皂乳液制备了聚苯乙烯微球,并以此为内核;再利用正硅乙酸乙酯在氨水催化条件下水解,形成带负电性的二氧化硅,或者利用六水亚硝酸铈、六亚甲基四胺水溶液分解出带负电性的氧化铈,均匀的包覆到PS微球表面,形成核-壳结构的PS-CeO2和PS-SiO2复合微球。

In the present dissertation, a surfactant-templated mesoporous silica molecular sieve with high pore volume, high porosity and narrow bimodal mesopore size distribution was synthesized for the first time in a reaction system, which was used usually in the synthesis of mesoporous MCM-41 molecular sieves, by a judiciously controlled two-phase sol-gel processing under basic conditions.

在本论文中,我们通过对一个通常用于制备介孔MCM-41分子筛的反应体系中正硅酸乙酯水解与缩合反应相对速率的精确调控,首次在弱碱性体系中合成了一种具有高孔隙率、大孔体积和双介孔孔分布特征的新型二氧化硅分子筛材料,简记为BMS,并对BMS二氧化硅分子筛中双介孔结构形成的原因及各种可能对其结构和性质产生影响的合成因素如Ammonia/silica摩尔比、组分浓度的变化、表面活性剂烷基链长度的调节、辅助有机物均三甲苯的引入、催化剂的结构和性质、溶剂和助溶剂的极性和用量、老化和干燥条件的变化及合成后水热处理等,利用不同的测试手段如XRD,SEM,TEM,〓Si MAS NMR,TG-DTA,N〓吸附测试等进行了系统的表征研究。

Optimization technology was acetidin: N-hexane (3:7) as low-pole solvent system, methanol: dichloromethane (1:9) as polar solvent system, 20% glycerol filter paper as moisturizer, 14 h age Bacillus subtilis as indicating strain seed on thin layer plate cultivated for 14~18 h, 1% TTC staining time 1~2 h, bacterial mix method suitable to 0.2%~0.6% agar semisolid bouillon culture-medium, bacterial spread method suitable to 1% agar semisolid bouillon culture-medium.

结果:该方法展开系统筛选简单,抑菌斑位置准确、斑点清晰,其优化条件为:以乙酸乙酯:正己烷(3:7)为弱极性展开系统,甲醇:二氯甲烷(1:9)为强极性展开系统,用20%甘油滤纸对湿室保湿,以14h菌龄的枯草芽孢杆菌为指示菌种子液,自显影薄层板36℃培养14~18h,1%TTC显色时间为1~2h,含0.2%~0.6%琼脂的半固体肉汤培养基应使用混菌法生物自显影,含1%琼脂半固体肉汤培养基应使用涂布法生物自显影。

The results showed when the weight ratio of linseed oil to rosin was less than 1.2, the product with following characters could be prepared i.e. molecular weight (averageM 6000~10000, PDI less than 4, n-heptane tolerance in the range of 5~20mL/2g, softening point more than 110℃ and good solubility in mineral oil, vegetable oil, aromatic hydrocarbon, MEK and ethyl acetate and so on. The product might be a new polymer for manufacturing rotary printing inks.

实验表明:m:m<1.2时,所得产品分子量(平均值M6000~10000,分子量分布范围,庚烷容纳度在5~20mL/2g,软化点>110℃,可溶于矿物油、植物油、芳香烃、丁酮和乙酸乙酯等溶剂中,是轮转油墨用的一种新型高分子聚合物。

This paper presents a new method for analysis of total organic acids in wine as follows:organic acids in wine were separated and enriched with strong anionexchange resin and were esterified directly on the resin with BF 3diethylether and alcohol for 60min under the temperature of 90℃.

界面衍生化气相色谱法测定葡萄酒中总有机酸⒇邓丛蕊(济南大学化学系济南250002)提要利用离子交换树脂分离、富集葡萄酒中总有机酸并直接在树脂界面上乙酯化,结合气相色谱/质谱法,鉴定并分析了葡萄酒中21种有机酸。

IP53 is a quick-drying, zinc phosphate primer, based on long oil alkyd resin and urethane alkyd resin.

IP53是长油醇酸树脂和氨基甲酸乙酯醇酸树脂配制而成的快干磷酸锌底漆。

The reversible addition fragmentation chain transfer radical polymerization of vinyl acetate was carried out in ethyl acetate.

在乙酸乙酯溶剂体系中考察了RAFT试剂结构、/、单体浓度对VAcRAFT溶液聚合规律的影响。

The R f value of the glucosamine sulfate was 0.36 measured by paper chromatography with the solvent system of pyridine, ethyl acetate, water and glacial acetic acid (5∶5∶3∶1 in volume).

经纸层析鉴定,以吡啶、乙酸乙酯、水和冰醋酸按体积比 5∶5∶3∶1组成的溶剂系统进行展层,氨基葡萄糖硫酸盐的Rf 值为 0 。36。

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