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乙酯

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In this thesis, the design, synthesis and application of substituted 1,8-naphthalimides and napthopyrones conjugated with uridine, substituted 1,3,5-triazine, 1,2-dibromoethane, ethyl bromoacetate have been studied.

本论文研究了取代l,8-萘酰亚胺和萘并吡喃酮与尿苷、取代均三嗪、二溴乙烷、溴乙酸乙酯偶合和双l,8-萘酰亚胺之间偶合的设计、合成及应用。

Strain 7-12 was used as original strain through primary selection on plate. U\^ DES and NTG were choosed to continue to mutate them for 6 generations respectively.

通过平板初筛筛选出7-12作为出发菌株,以紫外线、硫酸二乙酯、亚硝基胍作为诱变剂,单一或复合诱变连续处理6代。

First, this paper reports measurements of surface tension of ionic liquid EMIES (1-ethyl-3-methylimidazolium ethyl sulfate) using the forced bubble method at 278.15 to 323.15 K and densities of EMIES using Westphal balance at 278.15 to

为此,本文以廉价工业原料合成的硫酸乙酯—1—甲基—3—乙基咪唑EMIES和对水、空气都稳定的离子液体BMIBF_4为主要对象,使用密度法和最大气泡法等实验方法对这两种离子液体及其EMIES的水溶液的性质作了如下研究工作:在278.15—338.15K范围内用Westphal天平测定了EMIES和BMIBF_4的密度,用最大气泡法测定了纯离子液体EMIES和BMIB_4的表面张力。

Tamarillo phenolics in EA layer also exhibited stronger or compatible inhibitory activity than DL-?

於乙酸乙酯层中树番茄酚类化合物在相同浓度及作用条件下,表现出比正对照组DL-?

The effect of structural variation of the solutes on their separation and retention was noted.

此外,还建立了手性农药喹禾灵和重要药物前体DL-苯丁氨酸乙酯对映体纯度的测定方法。

Three methods for the preparation of 1,2,4-trizolone~5 are provided. 22 compounds are prepared. 3, 4-disubstituted 1,2,4-trizolone-5 is prepared by reacting amide with ethyl hydrazine-fornate at 110癈 for 3h in the presence of phosphorus oxychloride, following neutralization and cyclization reaction, giving to 74.5 % yields,which is 30% more than the literature value.

以三氯氧磷为缩合剂,使酰胺和肼基甲酸乙酯在110℃反应3h,经碱中和、环化反应,合成3,4-二取代-1,2,4-三唑酮-5,两步反应总产率达74.5%,与文献报道值相比,高出了30%以上,在三唑酮类衍生物的合成方法中具有很大的突破性。

Different factors such as mole ratio of reactants, temperature and reaction time were studied by orthogonal test.

以硫酸氢钠为催化剂在高压釜中合成水杨酸乙酯,采用正交实验研究了醇酸摩尔比、温度、时间等因素对反应的影响。

In addition, we also can directly add n-BuLi or Mg powder into Cp2ZrCl2 THF solution, followed by addition of 1-azadiene, ethylacetate or DMF to produce pyrroles after hydrolysis.

另外,我们也可直接使用有机锂或镁粉还原Cp2ZrCl2,再加入单氮二烯,乙酸乙酯或DMF,水解后亦可直接产生比咯化合物。

Insertion of ethylacetate or DMF into 1-zircona-2-azacyclopent-3-ene complexes at 50 oC affords pyrroles in moderate yield when they quenched with KOH aqueous.

1-锆-2-氮-环戊-3-烯错合物在室温下可与乙酸乙酯或DMF进行插入反应,经由氢氧化钠水溶液水解后,可得到不错产率的比咯。

Synthesis and characterization of Octa polyhedral oligomeric silsesquioxanes and Poly and their polystyrene composites enhanced combustion properties.

使用正硅酸乙酯和四甲基氢氧化铵,采用水解缩合的方法制备笼型八八硅酸盐,将其作为聚苯乙烯树脂的添加剂,采用熔融共混的方法制备了TMN-POSS/PS复合材料。

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