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乙酯

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Thiobarbituric acid was synthesized by sulfourea and diethyl malonate in sodium alcohol and 5-Arylidene thiobarbituric acid was prepared by the Knoevenagel condensation reaction from benzaldehyde and thiobarbituric acid.

采用丙二酸二乙酯和硫脲在乙醇钠存在下合成了硫代巴比妥酸,再分别采用固相反应和水相反应,由硫代巴比妥酸和苯甲醛经Knoevenagel缩合反应,制备了5-亚苄基硫代巴比妥酸。

In the presence of a catalyst, ethyl silicate was mixed with ethanol-water solution to form silica sol, which was impregnated into Alnus nepalensis and Tilia amurensis wood as soon as possible.

文章摘要:在催化剂存在下,使正硅酸乙酯与乙醇-水溶液混合制备硅醇溶胶,迅速将其分别注入到西南桤木和紫椴木材中,令其在室温下反应100min左右得到木材-凝胶,然后采用超临界干燥技术制备木材-SiO2气凝胶。

A strain NK13 was screened for a certain extent asymmetric hydrolyze the rac-ketoprofen Chloroethyl ester and identified as Bacillus megaterium. For the preparation of gene libraries, a positive clones was obtained from the tributyrin flat. The sequence of this esterase gene had been analysised, and contained the whole ORF of an esterase gene with the length of 933bp.

以本实验室筛选出的一株具有不对称拆分消旋酮基布洛芬氯乙酯的菌株NK13为材料,经初步鉴定为巨大芽孢杆菌,通过构建其基因文库,从中筛选得到一阳性克隆重组子pUC-NK。

In chapter 3, 83 volatile chemical constituents have been identified from the petroleum ether extracted part of ethanol extract of Debregeasia longifolia Wedd., and the relative percentages of the compounds are determined by GC method. From the extract of trichloromethane and ethyl acetate, 8 compounds have been isolated.

第三章首次对长叶水麻乙醇提取物的石油醚萃取部分分离并鉴定出83种成分,并用毛细管气相色谱面积归一化法测定了各组分的相对百分含量;从氯仿和乙酸乙酯萃取部分分离得到了8种化合物,用波谱学方法鉴定了其中2种成分。

Five species of solvents, namely, acetone, ethyl acetate, ether, trichloromethane and petroleum ether were selected to obtain extracts from Portulaca oleracea L. with microwave assistance and the biological activities of each extract was tested against Plutella xylostella L.

在微波加热条件下,以丙酮、乙酸乙酯、乙醚、三氯甲烷和石油醚为溶剂对马齿苋干粉进行提取,试验了各溶剂提取物对小菜蛾幼虫的触杀、胃毒及拒食活性,确定了石油醚提取物触杀作用的LD50。

Triethyl citrate was synthesized from citrate acid and ethanol using FeCl3 as catalyst and ethanol as dehydrating.

以三氯化铁为催化剂,乙醇为带水剂,用柠檬酸和乙醇为原料合成了柠檬酸三乙酯

The dehydrating agent and the dehydrating condition on removal of trace water in the synthetic solution of triethyl orthoformate were investigated.

研究了原甲酸三乙酯一步法合成反应中脱除微量水分的脱水剂和脱水条件,通过正交实验确定了脱水的最优化工艺条件。

A phosphorus-containing triazine oligomer was synthesized from triethyl phosphite, cyanuric chloride ,pentaerythritol and morpholine through three steps.

以亚磷酸三乙酯、三聚氰氯、季戊四醇和吗啉为原料,经3步反应合成了含磷三嗪环低聚物,考察了反应条件对中间体及产物收率的影响,对中间体及产物的结构和热性能进行了表征。

Properlies It is yellow Powder with little osmyland taste bitter. The density is 1.42-1.52. Soluble in ethylacatate, ethanol,solution of NaOH and Na2co3, unsoluble in benzene, water and gasoline.Good storage stablility.

性状 淡黄色粉末,微臭,有苦味,无毒,比重1.42-1.52,熔点170以上,易溶于乙酸乙酯,丙酮,氢氧化钠及碳酸钠的稀溶液中,溶于乙醇,不易溶于苯,不溶于水和汽油,贮存稳定。

The inhibition effect of chloroform fraction was the most potent, with the inhibition rate about more than 83% to 5 plant pathogenic fungi under the concentration of 15mg/mL. Under the concentration of 15mg/mL, the ethyl acetate fraction and n-butanol fraction thoroughly inhibited the growth of Alternaria solani and Valsa mali, with the inhibition rate up to 100%. The n-butanol fraction showed the highest potent virulence, with EC50 to Alternaria solani and Valsa mali about 0.09 and 0.279 mg/mL respectively.

其中氯仿部分的抑菌效果较好,当质量浓度为15mg/mL时,其对5种植物病原菌的抑制率均在83%以上;15mg/mL乙酸乙酯部分和正丁醇部分分别对番茄早疫病菌和苹果腐烂病菌有强烈且稳定的抑制作用,抑制率达100.00%,正丁醇部分对这两种菌丝生长抑制毒力最好,EC50分别为0.090和0.279mg/mL。

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