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The key intermediate 3-methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods,formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction,and then hydr...

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

The key intermediate 3- methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods, formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction, and then hydrolysis.

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

The effects of electrical and chemical stimulation of the vertral medial area of nucleus facialis on the myoelectric activities of genioglossus were observed in 26 urethane-anaesthetized and vagotomized rabbits.

本研究在26只氨基甲酸乙酯麻醉、断双侧迷走神经的健康成年家兔上观察了电、化学刺激面神经核腹内侧区对颏舌肌肌电活动的影响。

Effects of electrical and chemical stimulation of the dorsal and ventral medial area of nucleus facialis on myoelectric activities of genioglossus and phrenic muscle were observed in 44 urethane-anaesthetized and vagotomized rabbits.

在44只氨基甲酸乙酯麻醉、断双侧迷走神经的健康成年家兔上,观察电、化学刺激面神经核背内侧区和腹内侧区对颏舌肌和膈肌肌电活动的影响。

Effects of electrical and chemical stimulation of the dorsal and ventral areas of the nucleus raphe dorslison genioglossus and diaphragm activities were observed in 48 urethan-anasthetized and vagotomized raddits.

本实验在48只氨基甲酸乙酯麻醉、断双侧迷走神经的健康家兔上观察了电、化学刺激中缝背核背侧区和腹侧区对颏舌肌和膈肌肌电积分活动的影响。

The effects of electrical and chemical stimulation at nucleus rape dorsalis and nucleus raphe magnus on genioglossus and phrenic muscle activities and amplitude augmenting response to apnea were observed.

本实验在64只氨基甲酸乙酯麻醉、断双侧迷走神经、自主呼吸的健康家兔上进行,观察电、化学刺激中缝背核、中缝大核对颏舌肌和膈肌肌电、以及窒息增幅反应的作用。

It was difficult to extract corn pigments completely, for some of them were in a protein-bind state. It was better to use active carbon for the decolorization of GEON, the conditions were 40℃, stir time 6 hours, the ratio of carbon to hydrolyzate 1: 100 , but as to milk-like powder, it was better to extract pigments after spray drying.

最后,本文对玉米黄素的可抽提性也进行了初步研究,结果表明,部分色素与蛋白质结合而难以抽提,因而有机溶剂难以将色素抽提完全,对Gln活性肽营养液而言,可选用酶解后加活性炭进行脱色,脱色条件为40℃,搅拌6小时,炭液比为1∶100;而对黄粉蛋白乳粉而言,喷雾干燥后用乙酸乙酯脱色,可使酶解干燥后黄粉的异味减轻。

The fungicidal activity of methanol extract was higher than that of ethyl acetate extract, and the inhibition rates were higher than 90% against Alternaria longipes, Fusarium oxysporium, Gibberella zeae, Glomerella cingulata, Exserohilum turcicum under the concentration of 1000g/mL The results of the inhibition of spore germination indicated that the fermentation products exhibited obvious inhibition rate against Alternaria longipes, Exserohilum turcicum and Fusarium coeruleum, the EC50 values was 59.4g/mL, 96.5g/mL and 132.5g/mL. In the bioassay of the fermentation products against Bacillus sub tills and Bacillus cereus, by means of detection fo inhibition zone, the inhibition zone diameter was 20mm and 27mm. The results of pot tests that methanol extract showed higher than 70% of protective efficacy and therapeutic efficacy against wheat powdery mildew under the concentration of 2000g/mL.

其中,甲醇提取物的抑菌活性比乙酸乙酯提取物强,在1000g/mL浓度下对烟草赤星病菌、马铃薯干腐病菌、小麦赤霉病菌、苹果炭疽病菌、玉米大斑病菌的菌丝生长抑制率均大于90%;抑制孢子萌发法试验结果表明,2K3菌株菌丝体的甲醇提取物对烟草赤星病菌玉米大斑病菌和马铃薯干腐病菌的EC50分别为59.4g/mL、96.5g/mL和132.5g/mL;管碟法生测结果表明,2K3菌株菌丝体的甲醇提取物对枯草芽孢杆菌和蜡状芽孢杆菌的抑菌圈直径分别为20mm和27mm;盆栽试验结果表明,2K3菌株菌丝体的甲醇提取物在2000g/mL浓度下对小麦白粉病的治疗和保护作用均在70%以上。

In this paper,extraction velocity of TP during the process of TP production using Fluid Globelet Ascendingwas studied.

本文采用上升液滴法研究了有机相乙酸乙酯单液滴在萃取茶多酚过程中的速率。

The fungicidal activity of methanol extract was higher than that of ethylacetate extract. The bioassay showed that the methanol extracts of strain As fermentation products had certain degree fungicidical activity against Botrytis cinerea, Alternaria longipes, Glomerella cingulata, Curvulavia lunata, Gibberella zeae, Valsa malt under the concentration of 4000μg/mL, the inhibiting ratio against pathogen growth was ranging from 62.9%~85.1%; The results of the inhibition of spore germination indicated that the fermentation products exhibited obvious inhibition rate against Alternaria longipes, the EC50 values was 62.5328μg/mL; The bioassay showed that the methanol extracts of strain As fermentation products had certain degree fungicidical activity against Bacillus cereus , Bacillus subtilis.

其中甲醇提取物的抑菌活性较乙酸乙酯好,在4000μg/mL浓度下对番茄灰霉病菌、烟草赤星病菌、苹果炭疽病菌、玉米弯孢叫斑病菌、小麦赤霉病菌、苹果腐烂病菌6种植物病原真菌均有抑制作用,抑制率在62.9%~85.1%;抑制孢子萌发试验表明:菌丝体甲醇提取物对烟草赤星病菌的毒力较好,其EC50仅为62.5328μg/mL;抑制细菌活性表明菌丝体甲醇提取物对蜡状芽孢杆菌和枯草芽孢杆菌有一定的抑制作用,而对大肠杆菌无明显的抑制作用。

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