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乙酯

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It is a convenient and efficient method of preparation of diethyl N--L-glutamate.

利用上述方法可以方便高效地制备N-[4-苯甲酰基]-L-谷氨酸二乙酯

The catalyst used diethyl 2,3—di—i—propylsuccinate as internal donor particles were also synthesized.

采用 2,3-二异丙基琥珀酸二乙酯为内给电子体合成了负载型聚丙烯催化剂。

Urinary sample was acidified by 2 mol/L hydrochloric acid and pretreated by liquid-liquid extraction using diethyl ether.

尿样经2 mol/L盐酸酸化后用乙酸乙酯进行萃取。

Pharmaceutical characteristics of dimethylamino ethyl(4-chlorophenylmethfoxy )acetate hydrochloridein rabbit was studied and several parameters at different timeand way of medicine administration were determined.

研究了4-氯代苯甲氧基乙酸二甲氨基乙酯盐酸盐在家兔体内的药代动力学,测定了不同时间不同给药方式家兔体内的血药浓度及动力学参数。

Dimethylamino)ethyl methacrylate was polymerized using PS-CH_2Cl as macroinitiator and CuCl/ 2,2 '-Bipyridyl as catalyst in toluene to acquire amphiphilic brush-type copolymers of PS-g-PDMAEMA.

再以氯甲基化的聚苯乙烯(PS-CH_2Cl)为大分子引发剂,在CuCl和2,2′-联吡啶(2,2′-Bipyridyl,bpy)存在下,以甲苯为溶剂,进行甲基丙烯酸N,N-二甲胺基乙酯2-(Dimethylaminoethyl methacrylate,DMAEMA的ATRP聚合,得到两亲性的梳状共聚物PS-g-PDMAEMA。

This dissertation is mainly focused on the reactivity of methylenecyclopropanes and comprises six parts. 1 The reactions of methylenecyclopropanes with phenylsulfenyl chloride, phenylselenyl chloride and diphenyl diselenide; 2 The coupling reactions of the ring-opening products derivated from methylenecyclopropanes; 3 The palladium-catalyzed ring-enlargement of mono-aryl group substituted methylenecyclopropanes to cyclobutenes. 4 The gold-catalyzed domino ring-opening and ring-closing hydroamination of methylenecyclopropanes with sulfonamides; 5 The Lewis acid-catalyzed reactions of mono-aryl group substituted methylenecyclopropanes with diethyl ketomalonate in the presence of water; 6 The iodobenzene diacetate mediated novel 1,3-dipolar cycloaddition of methylenecyclopropanes, vinylidenecyclopropanes, and methylenecyclobutane with phthalhydrazine.

本论文主要研究了亚甲基环丙烷类化合物的一些化学反应性能,共由以下六部分组成:1、亚甲基环丙烷类化合物与苯硫氯、苯硒氯及二苯基二硒的反应;2、亚甲基环丙烷类化合物开环产物的偶联反应;3、单芳基取代的亚甲基环丙烷类化合物在钯催化剂作用下的扩环反应;4、金化合物催化磺酰胺对亚甲基环丙烷类化合物的串联开环关环氨氢化反应;5、路易斯酸催化亚甲基环丙烷类化合物与丙酮二羧酸二乙酯在有水存在下的反应;6、醋酸碘苯促进的亚甲基环丙烷类化合物、亚乙烯基环丙烷类化合物及亚甲基环丁烷类化合物与邻苯二甲酰肼的新型1,3-偶极环加成反应。

As a part of a search for new antitumor agents from Chinese medicinal plants, the roots of Salvia prionitis, collected in Jiangxi Province, was investigated. From the roots of this plant, a new diterpene, saprirearine (95), a new anhydride-type compound, saprionide (96), a new 7, 8-seco-abietane diterpene derivative, 7, 8-seco-paraferruginone (99), and a new 4, 5- seco-5, 10-friedo-abietane diterpenoids, 3-keto-4-hydroxysaprorthoquinone (102), have been isolated along with 6 known compounds. Their structures were established by spectroscopic methods and chemical transformation.

在对红根草的乙酸乙酯提取物进行分离,纯化和结构研究中,共得到10个化合物,其中4个是新化合物,3个新化合物具有新颖的重排松香烷型二萜骨架,新化合物99为首次从本属植物中分得的7,8-开环的松香烷型二萜醌类化合物。

Diethyl maleate was synthesized from maleic anhydride and ethyl alcohol in the presence of ammonium ferric sulfate dodecahydrate.

在十二水合硫酸铁铵存在下,由马来酸酐与乙醇合成了马来酸二乙酯,研究了反应的影响因素和催化剂的重复使用性能。

The synthesis methods of ethyl lactate catalyzed by P-toluene sulfonic acid, cationic exchange resin, ferric chloride hexahydrate, stannous chloride, Aluminium chloride, modified zirconium oxid, ferric-potassium vitriol, ammonium ferric sulfate dodecahydrate, rave earth sulfate, sodium bisulfate monohydrate, complex solid superacid, heteropoly acid, molecular sieve, ionic liquid and lipase etal.

评述了对甲苯磺酸,阳离子交换树脂,六水三氧化铁,氯化亚锡,三氯化铭,改性氧化锆,铁钾矾,十二水合硫酸铁铵,稀土硫酸盐,一水硫酸氢钠,复合固体超强酸,杂多酸,分子筛,离子液体和脂肪酶等催化剂催化合成乳酸乙酯的合成方法。

With 50% ethanol to elute to icarrin and then with Ethyl Acete and 60% ethanol to crystallize, the purity of icariin reached 90.02%.

用50%乙醇洗脱淫羊藿苷,经乙酸乙酯和60%乙醇重结晶后,干燥物中淫羊藿苷的含量达90.02%。

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