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The major results obtained are: PCR-RFLP method is suitable for molecular identification of Shihu; 205 compounds were isolated from 10 species of Dendrobium, including 21 new compounds, and 28 compounds isolated from genus Dendrobium for the first time. Each of the extracts and compounds were screened for anticoagulant and antitumour activities separately. The results indicated that the ethyl acetate extract from Dendrobium chrysanthun has significant anticoagulant function; the antitumour function of the 4 bibenzyl components from Dendrobium chrysotoxum is stronger than that of phenanthrene, of which the erianin has significant anti-angiogenic effect both in vivo and in vitro; components with moderate or stronger antitumour activities were found in the extracts of D. thyrsiflorum, D. chrysanthun and D. trigonopus; quality standard for 5 species of Dendrobium was drawn up use active or indicative components as control.

重要研究结果有:经方法学研究,认为PCR-RFLP法适于作为石斛属药材分子标记鉴定方法;对10种石斛进行化学成分分离鉴定,共分得205个化合物,其中新化合物21个,首次从石斛属分得的28个;对提取物和各单体化合物分别作抗凝血、抗肿瘤等活性筛选,结果说明束花石斛乙酸乙酯部位有显著的抗凝血作用,鼓槌石斛的4个联苄类成分抗肿瘤作用强于菲类,联苄类毛兰素在体内外有显著抗血管生成活性,球花石斛、束花石斛及翅梗石斛均筛到中等或较强抗癌活性的成分;选择有活性或指标性成分作对照品,对5种石斛草拟了质量标准。

Chemical constituents in ethyl acetate fraction of alcoholic extract from the flower of Bombax malabaricum DC .

采用GC-MS对木棉花醇提物乙酸乙酯溶解组分的化学成分进行了研究,共鉴定出46种成分。

The turbidity was induced mainly by inorganic salt in seriflux and the ethyl fatty acid in brut liquor.

低度白酒浑浊及货架期沉淀的原因主要是由加浆水中的无机盐和原酒中的高级脂肪酸乙酯引起的。

ResultThe Buxus Microphylla leaf ethyl acetate extraction (high-dose and low dose) have obvious effect on reducing the serum total cholesterol and triglyceride, moreover, the high-dose ethyl acetate extract reducing blood lipid was better than the other extracts.

结果 小叶黄杨叶乙酸乙酯提取物的高、低两个剂量组均有显著的降低血清总胆固醇和三酰甘油的作用,小叶黄杨叶的水提取物和石油醚提取物均有显著的降低血清中总胆固醇的作用,小叶黄杨叶氯仿提取物及正丁醇提取物均无降血脂的作用。

Result: Seven phenolic compounds were identified as rosmarinic acid(1),gallic acid(2),gentisic acid 5-O-(6′-O-galloyl)-β-D-glucopyranoside(3),caffeic acid(4),p-coumaric acid(5),ethyl caffeate(6) and acteoside(7),respectively.

结果:分离得到7种酚类化合物,经结构鉴定为:迷迭香酸(1),没食子酸(2),龙胆酸5-O-(6′-O-没食子酰基)-β-D-吡喃葡萄糖苷(3),咖啡酸(4),对香豆酸(5),咖啡酸乙酯(6)和acteoside(7)。

Their chemical structures were characterizd on the basis of spectral and chemical evidences to be: Sarracenin (1), 2-methyl-5-hydroxy-7-O-ethyl caffeate chromome (2), Naringenin(3), 2-methyl-5, 7-dihydroxychromome (4), 2-methyl-6-hydroxyl-cinnamic acid methyl ester (5), eriodictyol (6), quercetin (7), Naringenin-7-O-β-D-glucoside( 8 ), eriodictyol-7-O-α-D-glucoside (9), quercetin-3-O-β-D-glucoside(10). In addition, one compound was abtained from the n-butanol frationk, which was finally identified as Morrosiside(11) by spectral and chemical evidences.

以波谱数据及其理化性质鉴定为:Sarracenin(1),2-甲基-5-羟基-7-O-咖啡酸乙酯色原酮(2),柚皮素(3),2-甲基-5,7-二羟基色原酮(4),2-甲基-6-羟基苯丙烯酸甲酯(5),圣草酚(6),槲皮素(7),柚皮素-7-O-β-D-葡萄糖苷(Naringenin-7-O-β-D-glucoside)(8),圣草酚-7-O-α-D-葡萄糖苷(eriodictyol-7-O-α-D-glucoside)(9),槲皮素-3-O-β-D-葡萄糖苷(quercetin--3-O-β-D-glucoside)(10);另外从正丁醇萃取部位分离得到1个化合物,以波谱数据和文献对照鉴定为:Morroniside(11)。

The ethanol extract and ethyl acetate extract of Capparis Spinosa have the effect against skin fibrosis.

槌果藤乙酸乙酯提取物、乙醇提取物具有抗皮肤纤维化作用。

Results On week 2, 4, 6, the thickness of dermis was 23.22, 24.94, 19.97 μm respectively in mice treated with ethanol extract of Capparis Spinosa, 27.66, 26.15, 22.13 μm respectively in those treated with ethyl acetate extract of Capparis Spinosa.

目的 观察槌果藤乙酸乙酯提取物、乙醇提取物对硬皮病小鼠模型真皮厚度、Ⅰ型、Ⅲ型胶原合成及转化生长因子-β1表达的影响。

Ethyl decanoate was synthesized from capric acid and ethanol by using ferric potassium alum as catalyst.

以铁钾矾为催化剂,通过葵酸与乙醇反应合成了癸酸乙酯

Caproic acid is regarded as not only an important index of determining the quality of fragrance alcohol, but also a main restricted factor of the quality of Luzhou-dagu Baijiu.

适量的已酸乙酯是决定浓香型白酒质量的一个重要指标,也是曲酒优质率的主要限制因素。

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