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SiO2 aerogels were produced from TEOS as silicon resources by sol-gel method and surface modification at ambient pressure.

以正硅酸乙酯为硅源,采用溶胶-凝胶法和表面修饰工艺,在常压条件下制备了SiO2气凝胶。

Moreover, the loading amount of the inorganic phase was another important factor on the properties of the hybrid membrane, and the comprehensive performance was obtained when the addition amount of TEOS was around 30% based on the polymer content.

此外,杂化膜中无机相的负载量也是一个影响杂化膜结构和性能的重要因素,当正硅酸乙酯的添加量为30%时,杂化膜的综合性能较为理想。

The analysis methods for the determination of micro or trace elements in high moisture jellyfish were developed. The fatty acid compositions in difderent parts of fresh jellyfish were determined by GC/MS method. Thirty-five fatty acids were identified, and most of them were found in R. esculentum jellyfish for the first time. Especially, two unusual very long chain polyunsaturated fatty acids that were never detected in the other jellyfish also were determined. Amino acids were abundant in R. esculentum jellyfish, especially containing sulfur amino acids, and could be supplied for human diet. The polysaccharide in umbrella part of jellyfish was composed of glucose, galactose and uronic acid, and its molecular weight was 40,000, but the polysaccharide of the oral arms part consisted of glucose, mannose and glycuronic acid, and its molecular weight was 43,000. Above-mentioned data were never reported. The ethanolic extract of oral arms part of jellyfish were extracted by different polar solvents (petroleum ether, acetic ether, n-butanol), and antibacterial activity was tested to these extracts by four species of terricolous pathogenic bacilli and three species of botanic pathogenic fungi. The result demonstrated that the petroleum ether extract had certain bactericidal activity for two species of pathogenic bacilli, and n-butanol extract had certain inhibited activity on apple rot pathogenic fungus.

建立了 高含水量的海蜇产品中微量、痕量元素成分测定的分析方法;采用 GC/MS 方法测定了新鲜海蜇不同部位的脂肪酸组成,共鉴定出 35 种脂肪酸,其中大多数脂肪酸是首次在海蜇中被检测到,尤其是两种不常见的 C24:5 超长链多不饱和脂肪酸的分析和鉴定在其它水母种属中也从未见报道;海蜇三个部位中氨基酸成分齐全,含量丰富,含硫氨基酸含量较高,可与其它食物蛋白质的氨基酸互补;其中海蜇皮多糖是由葡萄糖、半乳糖和糖醛酸组成,分子量为 40,000,海蜇头多糖是由葡萄糖、甘露糖和糖醛酸组成,分子量为 43,000,以上工作均未见报道;利用石油醚、乙酸乙酯、正丁醇三种不同极性溶剂分别萃取海蜇头乙醇浸提物,用纸碟法和生长速率法分别对四株陆源病原菌和三株植物病原真菌进行了抑菌实验,结果表明海蜇头石油醚提取物和正丁醇提取物具有一定的抑菌活性。

The analysis methods for the determination of microor trace elements in high moisture jellyfish were developed. The fatty acid compositions indifderent parts of fresh jellyfish were determined by GC/MS method. Thirty-five fatty acids wereidentified, and most of them were found in R. esculentum jellyfish for the first time. Especially,two unusual very long chain polyunsaturated fatty acids that were never detected in the otherjellyfish also were determined. Amino acids were abundant in R. esculentum jellyfish, especiallycontaining sulfur amino acids, and could be supplied for human diet. The polysaccharide inumbrella part of jellyfish was composed of glucose, galactose and uronic acid, and its molecularweight was 40,000, but the polysaccharide of the oral arms part consisted of glucose, mannose andglycuronic acid, and its molecular weight was 43,000. Above-mentioned data were never reported.The ethanolic extract of oral arms part of jellyfish were extracted by different polar solvents(petroleum ether, acetic ether, n-butanol), and antibacterial activity was tested to these extracts byfour species of terricolous pathogenic bacilli and three species of botanic pathogenic fungi. Theresult demonstrated that the petroleum ether extract had certain bactericidal activity for twospecies of pathogenic bacilli, and n-butanol extract had certain inhibited activity on apple rotpathogenic fungus.

建立了高含水量的海蜇产品中微量、痕量元素成分测定的分析方法;采用 GC/MS 方法测定了新鲜海蜇不同部位的脂肪酸组成,共鉴定出 35 种脂肪酸,其中大多数脂肪酸是首次在海蜇中被检测到,尤其是两种不常见的 C24:5 超长链多不饱和脂肪酸的分析和鉴定在其它水母种属中也从未见报道;海蜇三个部位中氨基酸成分齐全,含量丰富,含硫氨基酸含量较高,可与其它食物蛋白质的氨基酸互补;其中海蜇皮多糖是由葡萄糖、半乳糖和糖醛酸组成,分子量为 40,000,海蜇头多糖是由葡萄糖、甘露糖和糖醛酸组成,分子量为 43,000,以上工作均未见报道;利用石油醚、乙酸乙酯、正丁醇三种不同极性溶剂分别萃取海蜇头乙醇浸提物,用纸碟法和生长速率法分别对四株陆源病原菌和三株植物病原真菌进行了抑菌实验,结果表明海蜇头石油醚提取物和正丁醇提取物具有一定的抑菌活性。

In the process of laboratory study, oxycodone was prepared by oxidating thebaine at 6,14-position under oxydol, hydrodeoxidizing 7,8-position double bond and 14-position ether under palladium catalyst. Furthermore, N-methyl of oxycodone was isolated byα-chloro-ethyl chloroformate under anhydrous condition and protection of 14-position hydroxyl to obtain noroxycodone, which was further converted into methylnaltrexone by N-alkylation in presence of cyclopropyl bromomethane, then by isolating 3-position methyl of methylnaltrexone under boron tribromide, becoming hydrochloride to prepare target compound, natrexone hydrochloride.

实验室工艺方面,本文首先用双氧水氧化蒂巴因的6-位和14-位、在钯炭催化下加氢还原7-8位双键和14-位醚合成羟考酮,然后提出并优化了在无水和14-位保护的情况下,用氯甲酸-α-氯乙酯脱去羟考酮的N-位甲基合成去甲羟考酮,再用环丙甲基溴将去甲羟考酮的N-位烷基化合成甲基纳曲酮,最后采用三溴化硼脱去甲基纳曲酮的3-位甲基和成盐酸盐合成盐酸纳曲酮。

To adopt system menstruum deal with fermented products of mycelium from Tremella aurantialba, then mycelium from tremella aurantialba was studied with the clotting time of the thrombogen, the whole blood clotting time in mice and thrombosis experiment in mice.

采用系统溶剂法处理金耳菌丝发酵物,得乙酸乙酯部位、正丁醇部位及水溶部位,通过凝血酶原实验、小鼠凝血实验及小鼠体内血栓形成实验等来筛选具有抗凝血作用的有效部位。

Diethylphosphite was prepared from ethanol and phosphorus trichloride at mole ratio of 3.3:1 with the droping temperature at 5-10℃, and reacted under room temperature.

以无水乙醇和三氯化磷为3.3:1的投料量,5~10℃下滴加,室温下反应,制备亚磷酸二乙酯

If you are using urethan enhanced printing, coating after 8 h of natural drying, you can use water-based ink business card printing and membership card.

如果用氨基甲酸乙酯强化印版,涂布后经过8h的自然干燥,即可使用水性油墨制卡和会员卡制作。

Because you want to use water-based ink, paint, or urethan, phenol-formaldehyde resin on the printing plate for water resistance.

因要使用水性油墨,所以要用漆或氨基甲酸乙酯、酚醛树脂对印版进行耐水强化处理。

Urethan resin for better stability, but business card printing and membership card making suitable to their needs and less soluble Li anzhai and other styryl modified monomaleate resin, water-based Amino resins, and polyvingl acid and carboxymethly celluiose, and so on, these polymer resin generally with the-COOH,-OH,-NH

氨基甲酸乙酯树脂的稳定性较好,但制卡和会员卡制作适性和可溶性要略差一些,其它还有用苯乙烯改性马来酸树脂、水性氨基树脂以及聚乙烯酸和羧甲基纤维素等,这些高分子树脂一般均含有-COOH、-OH、-NH

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