乙酯

D limonene was distributed among the culture flasks (200 mg/L). The flasks were incubated at 28oC on a rotary shaker (r/min=120) for 5 days. On completion, the culture broth were successively extracted with EtOAc. The extract was quantitatively measured by gas chromatography mass spectrometry analysis, The results showed that biocatalytic reactions were comprised of oxidation, including hydroxylation and ketonization which occurred at different positions of the D limonene, as well as hydrogenation, hydrolyzation, esterification and cyclic cleavage. These bacteria strains possess the distinctive biocatalytic capacities towards the D limonene. A series of terpenoids, including sesqui , di and tri terpernoids were also observed,which was accounted for D limonene had influence on the metabolites of marine bacteria.

以2216E为培养基，添加200mg/L的柠檬烯，在28℃，以120 r/min摇瓶培养5 d，用乙酸乙酯提取培养液，经GC MS分析其转化产物，结果显示，这些细菌能在柠檬烯的不同位置进行羟基化、羰基化等，并伴随有还原、水解、酯化、开环等反应，但转化能力和转化程度不同；在产物中，还检测到系列结构不同的其它萜类：包括倍半萜、二萜以及三萜等，这些萜类化合物的产生跟柠檬烯的加入有关，说明柠檬烯能影响细菌代谢产物的产生。

The free fatty acids were extracted with petroleum ether and were separated on silicon gel column chromatography. The ethyl acetate-soluble lipid fraction and water-soluble lipid fraction were subjected to hydrochloric acid-catalyzed methanolysis, then were extracted with petroleum ether, respectively.

用石油醚提取低极性组分，经硅胶柱层析分离得到游离脂肪酸；用乙酸乙酯提取酯溶性神经酰胺及其衍生脂类，提取物和残余的水溶性脂类分别经盐酸甲醇解，水解产物再用石油醚提取。

By using gas chromatography technique nine kinds of fragrance components(acetic aldehyde,ethyl acetate,ethanol,propyl acetate,3-hydroxy-2-butanone,acetic acid,furfural,metacetonic acid,2,3-butylene glycol)were measured quantitatively in different kinds of Shanxi overmature vinegar and the other kinds of vinegar.

应用气相色谱方法对山西老陈醋和其他种类醋的9种香气成分(乙醛、乙酸乙酯、乙醇、乙酸丙酯、3-羟基-2-丁酮、乙酸、糖醛、丙酸、2，3-丁二醇)进行了定性、定量测定，并用聚类分析、模糊综合评判、方差分析、回归分析的方法对实验结果进行了数理分析。

Esterification of phenethyl alcohol with acetic acid was studied using lanthanum chloride supported on activated carbon as heterogeneous catalyst.

以活性炭负载三氯化镧为非均相催化剂，对乙酸与苯乙醇之间的酯化反应进行了研究，考察了催化剂用量、醇酸摩尔比、反应时间对乙酸苯乙酯收率的影响。

Due to the key challenge for complicated techniques and preparation, there were few reports about ternary systems. A series of polyimide/SiO_2-TiO_2 hybrid films with different contents of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor in situ with sol-gel method and both phases in situ. Chemical structure and micro-morphology of hybrid films were studied by means of IR, SEM and XRD.

本文以正硅酸乙酯和钛酸四丁酯为前驱体，采用原位溶胶-凝胶法和两相原位同步法制备了一系列不同含量的聚酰亚胺/SiO_2-TiO_2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性、电击穿场强和耐电晕性。

A series of polyimide/SiO2-TiO2 hybrid films with different contents and weight ratio of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor by situ method. Chemical structure, micro-morphology and thermal stability of hybrid films was studied by means of SEM, IR and XRD, TGA was also tested.

以正硅酸乙酯和钛酸四丁酯为前驱体，采用两相原位同步法制备一系列不同含量及重量比的聚酰亚胺／SiO2-TiO2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性。

A series of polyimide/SiO2-TiO2 hybrid films with different contents and weight ratio of inorganic particle were fabricated using tetraethoxyl silicane and tetrabutyl titanate as precursor by situ method .

以正硅酸乙酯和钛酸四丁酯为前驱体，采用两相原位同步法制备一系列不同含量及重量比的聚酰亚胺/SiO2-TiO2杂化薄膜，利用红外光谱、扫描电镜和XRD观察了薄膜的化学结构和微观结构，并测试了薄膜的热稳定性。

The esterification of mixing binary acid with ethanol was carried out under silicotungstic acid as catalyst in this experiment.

以混合二元酸为原料酸，硅钨酸为催化剂，与无水乙醇进行酯化反应制备混合二元酸二乙酯。

Twelve new Schiff bases of 5-amino-1H-1,2,3,4-tetrazolyl were synthesized. These Schiff bases were further converted into α-(5- tetrazolyl)-aminoalkyl phosphonates.

合成了12个新的5—氨基—1H—1，2，3，4—四唑的Schiff碱，而后与亚磷酸二乙酯反应，合成出了12个新的含四唑基的α-氨基烃基膦酸酯，通过IR，^1H NMR，^31P NMR和元素分析证实了它们的结构。

In this study, new benzo[l,2,3]thiadiazole derivatives were designed according to relationship of structure and efficacy. The 9 novel compounds were synsthesized with following reactions. The chlorine atom in 2-chloro-3,5-dinitro-benzoic acid as beginning raw material was substituted by 2-methylpropane-2-thiol, esterified then with bromoethane, reduced by iron powder and cyclized to obtain ethyl benzo[l,2,3]thiadiazole-7 after diazonation reation.

本论文根据苯并噻二唑诱导剂的构效关系设计了新的苯并噻二唑的结构，并合成了9个未见文献报道的化合物，合成步骤如下：采用2-氯-3，5-二硝基苯甲酸为起始原料，苯环上的氯原子被叔丁基硫醇置换，羧酸由溴乙烷酯化，硝基由铁粉还原，随后经重氮化关环生成苯并[1，2，3]噻二唑-7-羧酸乙酯。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。