乙酯

Methods A mixture of 10 mol/L potassium dihydrogen phosphate solution and acetonitrile(60 ∶ 40) was used as the mobile phase.

方法以乙腈-10mmol/L磷酸二氢钾(40∶60)为流动相，炔雌醇为内标，血浆样品经乙酸乙酯萃取。

Silicone/SiO2 organic-inorganic hybrid sol have been prepared from tetraethyl orthosilicate as inorganic precursor, methyl triethoxysilane and diphenyl dimethoxy silane as organic precursor, the hydrochloric acid and water as catalysts, by sol-gel method through the hydrolysis-polycondensation reaction.

采用溶胶－凝胶法，以正硅酸乙酯为无机相前驱体，甲基三乙氧基硅烷和二甲基二甲氧基硅烷为有机相前驱体，盐酸和水为催化剂，通过水解－缩聚反应制备了有机硅／SiO2有机－无机杂化溶胶。

College of Veterinary Medicine, China Agricultural University, Beijing 100094, China Abstract: A method has been developed to determine residual stilbenes such as diethylstilbestrol, dienestrol and hexestrol in animal tissues using solid phase extraction and gas chromatography-mass spectrometry.

动物组织样品在碱性条件下用乙酸乙酯提取，经碳酸钠溶液液-液分配净化，再用硅胶柱固相萃取净化，洗脱液均分成两份后经氮气吹干，分别用双三甲基硅基三氟乙酰氨和七氟丁酸酐衍生，采用选择离子监测模式进行测定，外标法定量。

The process was methanolysis α-imino ether acid hydrogen chloride salt from methyl-cyanide.

研究了以乙腈为原料经α-亚氨基乙醚盐酸盐醇解制备原醋酸二乙酯的工艺方法，对醇解的投料比、反应时间及中和pH值等工艺条件进行了研究，得出较优惠的工艺条件。

The wholly aromatic four-component copolyesters were prepared from p-acetoxy-benzoic acid, hydroquinone diacetate, 2,6-naphthalene dicarboxylic acid and isophthalic acid by melting polycondensation.

由对乙酰氧基苯甲酸、对苯二酚二乙酯、2，6-萘二甲酸及间苯二甲酸四种单体通过熔融缩聚反应，合成了全芳香族四组分共聚酯。

In the presence of catalytic rhodium acetate, ethyl 2-diazo-3-oxo-per fluoroalkanoates, reacted readily with nitriles to give a series of 5-fluoroalkyl substituted 1, 3oxazoles with high regio-selectivity through a metal carbenoid intermediate. The reactions of carbenoids with noncyclic vinyl ethers or cyclic vinyl ethers afforded dihydrofuroates in good to excellent yields. Interestingly, only vinyl C-H insertion compound was obtained concerning of the reaction of carbenoids with 2, 5dimethylfuran due to the steric hindrance of methyl group

醋酸铑分解2-重氮-3-氧代-全氟羧酸乙酯形成的金属卡宾作为1，3-偶极体，可以与一系列芳基或烷基取代的腈反应，高度区域选择性地生成一系列4-乙氧羰基-5-氟烷基取代的噁唑化合物；也可以与富电子的链状和环状的烯基醚反应，以优良的产率得到一系列氟烷基取代的二氢呋喃类化合物；而与2，5-二甲基呋喃的反应，由于甲基的位阻作用，只得到金属卡宾对呋喃3-位烯基碳氢键插入产物。

Through condensing o-aminobenzoic acid, ethyl oxalyl chloride and ethylenediamine(or 1,2-propylenediamine), two new ligands N-benzoato-N′-(2- aminoethyl)oxamido(H3oxbe) and N-benzoato-N-(2-amino-2-methylethyl)oxamido(H3oxbt) have been synthesized. Their mononuclear complexes Na·1.5H2O and Na·1.5H2O have also been obtained.

2以邻氨基苯甲酸、草酸乙酯酰氯和乙二胺(或1，2-丙二胺)缩合制得了两种具有不对称草酰胺结构配体N-(2-苯甲酰基)-N&-(2-氨乙基)草酰胺(H3oxbe)和N-(2-苯甲酰基)-N&-(2-氨丙基)草酰胺(H3oxbt)，并得到了它们的单核配合物：Na·1.5H2O和Na·1.5H2O。

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ，N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

Alumina sols of different content were prepared by using Al3 as precusor, water as solvent, nitric acid as peptizer, ethylacetoacetate and polyvinylpyrrolidone as modified menstruum. We used dip-coating method and spin-coating method prepared of alumina films on the plane glass and used dip-coating method and rising liquid method inside the wall of the fiber.

以仲丁醇铝为前驱物、水为溶剂、硝酸为胶溶剂、同时加入乙酰乙酸乙酯和聚乙烯吡咯烷酮作为改性剂制备了不同浓度的氧化铝溶胶用提拉法和旋覆法在平板玻璃上镀膜，同时用提拉法和液面上升法在石英毛细管内壁上镀膜。

A(C2H5)3N·HCl-induced palladium complex PdL2Cl2 and CuCl2 catalyzed cyclotrimerization reaction of Ethyl Propiolate has been reported for the first time.

报道了一类三乙胺盐酸盐存在下钯PdL2Cl2-CuCl2催化体系催化的丙炔酸乙酯(Ethyl Propiolate，简称EP)环三聚反应。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。