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乙酯

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A new synthesizing route for ethyl-2-(p -ethoxyphenyl) propenoate preparation was proposed, in which, the ethyl-2-(p-ethoxyphenyl) propenoate was synthesized from phenetole via Friedel-Crafts reaction and Wittig G reaction.

设计了一条以苯乙醚为起始原料,经过Friedel-Crafts反应、WittigG反应合成2-对乙氧基苯基丙烯酸乙酯的新路线。

L-Phenyl-3-methyl-5-pyrazoIone was synthesized by the reaction of ethyl acetoacetate and phenyl hydrazine in ethanol.

在无水乙醇的存在下,乙酰乙酸乙酯和苯肼为原料合成标题化合物。

Benzyloxy benzoyldimethylsulfoxide was prepared by the reaction of ethyl 4-benzyloxybenzoate and dimethyl sulfoxide in the presence of sodium hydride, followed by Pummerer reaction with concentrated hydrochloric acid to afford eo-hydroxy-co-thio-methyl-(4/-benzyloxy) acetophenone, which reacted with urea, thiosemicarbazide, semicarbazide hydrochloride and o-phenylenediamine to give imidazolidine-2,4-dione, l,2,4-triazine-3- one and quinoxaline derivatives, respectively.

本文用4-苄氧基苯甲酸乙酯和二甲亚砜为原料,在氢化钠存在下反应,合成了(4′-苄氧基)-苯甲酰基-二甲亚砜。研究了该亚砜在浓盐酸的存在下发生的Pummerer重排反应,用重排产物ω-羟基-ω-甲硫基-(4′-苄氧基)-苯乙酮分别与尿素、氨基脲、氨基硫脲和邻苯二胺反应合成了2,4-咪唑啉-二酮、1,2,4-三嗪-3-酮、喹喔啉等含氮杂环化合物。

A sol containing SiO_2 particles was prepared by the base catalyzed hydrolysis and polycondensation of tetraethoxysilane through sol-gel process. A solution containing double-chain polymer of methyltriethoxysilane was also prepared under acid condition, as the introducer of water repellence.

通过溶胶-凝胶法,在碱性条件下水解缩聚正硅酸乙酯获得含有SiO2颗粒的溶胶;以甲基三乙氧基硅烷在酸性条件下水解缩聚获得双链聚合物溶液,作为疏水基团的引入剂。

Methods Technetium 99m (99mTc) ECD single photon emission computed tomography was performed in 67 newborns with HIE.

采用锝(99mTc)乙撑双半胱氨酸二乙酯单光子发射型计算机断层摄影术对67例HIE患儿进行脑血流灌注断层显像。

The porous SiO2 xerogels with controlled structure were obtained from TEOS in the presence of PEG by sol-gel method.

采用溶胶-凝胶法,以正硅酸乙酯为前驱体,以不同分子量的聚乙二醇为改性剂,制备结构可控的多孔SiO2干凝胶。

Dehydroacetic acid was synthesized from acetacetic ether, and the influent factors of productive rate were investigated.

研究了以乙酰乙酸乙酯为原料合成脱氢醋酸过程中,催化剂的种类、用量以及反应时间对产物得率的影响。

With 1,4-bezenoquinone and ethyl acetoacetate as the starting materials, it had been prepared in a novel six-step procedure in overall yield of 34.6%.

以1,4-苯醌和乙酰乙酸乙酯为起始原料,经新的六步反应过程,合成阿比朵尔,总收率为34.6%。

KF/NaZnPO4 was used as the catalyst for Michael addition reaction of ethyl acetoacetate and acrylonitrile.

以磷酸锌钠负载KF为催化剂,催化乙酰乙酸乙酯与丙烯腈进行Michael 加成反应。

The synthesis of celery ketone from butyl aldehyde and ethyl acetoacetate was improved with higher yield by using solid superbase(K2O/γ-Al2O3) for the first time.

在正丁醛和乙酰乙酸乙酯为原料合成芹菜酮的合成过程中,对其催化方法进行改进。

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