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乙酯

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It was discovered that trimalonic acid C60、fullerol、dimalonic[60]fullerene hydrolysate、tetraethyl methano[60]fullerenediphosphonate、methano[60]fullerenediphosphonic acid and dimalonic acid C60 exhibited different inhibitory effects on Taq DNA polymerase.

实验发现,6种富勒烯衍生物三丙二酸富勒烯、富勒醇、富勒烯丙二酸水解物、亚甲基富勒烯二膦酸四乙酯、亚甲基富勒烯二膦酸四乙酯的完全水解物和二丙二酸富勒烯对Taq DNA聚合酶存在不同程度的抑制作用。

In the reaction, industrial chlorinating agent and brominating agent with low cost and easy acquisition are used as oxidants to oxidize the ethyl lactate into the ethyl pyruvate.

反应中使用了廉价易得的工业用氯化剂、溴化剂作为氧化剂,将乳酸乙酯氧化为丙酮酸乙酯

Result: The anticancer active component includes: taxol 9.45%、cephalomanine: 9.63%、10- deacetylbaccatinⅢ: 22.64%、total flavonoids: 19.15%. 3. The preparation of Seiadopitysin control Methods: Take dry Ginkgo leaves and extracted three times by sonication with 95% EtOH, solutions were concentrated under vacuum, after defatting by petroleum benzin, the sample was extracted with EtOAc and the solutions were concentrated under vacuum.

金松双黄酮对照品的制备方法:取干燥银杏叶以95%乙醇超声提取3次,提取液合并,减压浓缩,石油醚脱脂后,用乙酸乙酯萃取,萃取液减压浓缩,经硅胶柱(6cm×80cm)层析,石油醚-乙酸乙酯(9∶1~5∶5)梯度洗脱,产物用甲醇多次冲淋,再以二甲基甲酰氨溶解,反复重结晶,得黄色粉末结晶。

Under the optimal reaction conditions the acid value of the esterified production is the lowest,and the esterified degree is complete.

在最优条件下,鱼油的乙酯化产品酸值最低,乙酯化程度最高。

The similar nicotinoyltrifluoroacetones are synthesized from acetylpyridine and ethyl trifluoroacetate through Claisen reaction.The influnences of alcoholic natrium,reaction temperature and solvent on reaction yield is studied.The subliming method is improved.

本文以乙酰吡啶和三氟乙酸乙酯为主要原料,利用克莱森酯缩合反应,合成了三种相似结构的吡啶甲酰三氟丙酮化合物,考察了碱性试剂醇钠、反应温度和溶剂等因素对反应产率的影响,改进了纯化产物的方法。

Benzoyl chloride, phthaloyl dichloride, isophthaloyl dichloride and terephthaloyl dichloride were reacted with cinchona alkaloids to form 16 esters type catalysts 4a-d, 5a-d, 6a-d and 7a-d.

1对于溴乙酰甲酸乙酯为底物的反应,这类以酯键形成的金鸡纳生物碱衍生物表现出的不对称诱导作用不令人满意(22-75%ee)。

L-Phenylalanine was then obtained by alkylation of N- glycine ethyl ester with benzyl bromide in the presence of an asymmetric phase-transfer catalyst-N-benzyl-cinchonine chloride, followed by hydrolysis of the resulting product.

以甘氨酸乙酯盐酸盐和二苯甲酮为起始原料合成了N-二苯亚甲氨基乙酸乙酯,后者在手性相转移催化剂-N-苄基氯化辛可宁诱导下与烷基化试剂溴化苄发生不对称相转移催化烷基化反应,水解得到L-苯丙氨酸。

Methyl-l, 3-oxazine-2,4-dione are prepared from ethyl acetoacetate and ethyl carbamate at 140 for 6h, catalysted by zinc acetate, giving to 48.8% yields which is 33% more than the literature value.

选用醋酸锌作催化剂,使乙酰乙酸乙酯与氨基甲酸酯在140℃反应6h,合成6-甲基-1,3-噁嗪-2,4-二酮,产率达48.8%,较文献报道值高出了33%。

The extracts from evening primrose flower could significantly enhance the cellular immune function in immunosuppressed mice. Effects of ethylacetate extract was better than those of water extract.

月见草花乙酸乙酯提取物和水提取物均可明显增强环磷酰胺免疫抑制小鼠的细胞免疫功能,其中乙酸乙酯提取物的作用优于水提取物。

In order to improve the thermal stability of yellow iron oxide pigments, a new balance precipitant coating silicon method with ethyl acetate as potential acid by controlling the dehydrolysis velocity of ethyl acetate was used.

为了改善铁黄颜料的耐热性,运用乙酸乙酯作为潜伏性酸试剂,研究了一种新的铁黄表面均匀包覆二氧化硅的方法,即通过控制乙酸乙酯的水解速率来实现在铁黄表面均匀包覆二氧化硅。

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