乙酯

It,s allelchemicals were isolated through extraction, thin-layer chromatography, and column chromatograpathy. After the white clover was infused in ethanol and evaporation, the leavings was dissolved by water. The aqueous extract was extracted by petroleum,chloroform, ethyl acetate and n-Butanol successively, and the bioassay showed that the chloroform phase has obvious inhibitory effect, the inhibitory rate was 44.32%,88.08% on Abutilon theophrasti M., seedling length and root length, 82.08%,92.16% on Echinochloa crusgalli L., seedling length and root length, and the Amaranthus retroflexux L., germination rate is 0, the secondly was ethyl acetate phase.

运用萃取、薄层层析、柱层析等方法对白三叶草地上部分的化感物质进行初步分离，结果表明，白三叶草经乙醇浸提旋转蒸发后用蒸馏水溶解，依次用石油醚、氯仿、乙酸乙酯、正丁醇萃取，生物测定表明氯仿组分对杂草的抑制作用最强，对苘麻芽长和根长抑制率分别为44.32%、88.08%，对稗草芽长和根长的抑制率分别为82.08%、92.16%，反枝苋的发芽率为0；其次是乙酸乙酯相。

Product has mainly engaged in alcohol-benzene toluene xylene butyl acetate ester, such as acetone acetophenone ring.

主要经营产品有甲苯二甲苯醇苯醋酸丁酯乙酯丙酮环乙酮等。

Orthogonal test was performed to examine the influences of reaction conditions on microwave-assisted synthesis of 2'-oxo-cyclopentanecarboxylic acid ethyl ester from diethyl adipate.

以己二酸二乙酯为原料，在微波辐射下经Dieckmann缩合反应合成2'-羰环戊基甲酸乙酯。

Content of butanoic acid, methyl ester; butanoic acid, ethyl ester; hexanoic acid, methyl ester; DMHF; DMMF identified in strawberry cultivated from green house were higher than that cultivated in the open field of the correspongding nitrogen levels , and the hexanoic acid, ethyl ester could only identified in green house strawberries.

不同氮素水平温室草莓果实中丁酸甲酯、丁酸乙酯、己酸甲酯、DMHF、DMMF的相对含量和总量均比相应氮素水平的露地草莓的高，且己酸乙酯只是在温室草莓中检测到。

The obtained results show that the primary and secondary alcohols areconverted in good yields, whereas tertiary alcohol and phenol are unreactive.

当原料分别为乙醇、正丁醇、仲丁醇、苯甲醇和苯乙醇时，目标产物碳酸二乙酯、正丁基乙基碳酸酯、仲丁基乙基碳酸酯、苯甲基乙基碳酸酯和苯乙基乙基碳酸酯的产率分别为67.3、52.3、56.7、37.6和32.8％。

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

The costuslactone and dehydrocostuslactone in the supercritical CO 2 extract of aucklandia were identified by TLC using a mobile phase of petroleum ether,ethyl acetate and benzene (70∶5∶15) and the colour developing reagent of 5% vanillic aldehyde dissovled in sulfuric acid.

用薄层色谱法，以ψ(石油醚∶乙酸乙酯∶苯)=70∶5∶1 5为展开剂，质量分数为 5 %香草醛硫酸为显色剂对木香超临界萃取物中的木香烃内酯与去氢木香内酯进行鉴别；并建立高效液相色谱法同时测定木香烃内酯与去氢木香内酯的含量方法。

Two series of polyurethane acrylate grafted acrylic resins (Acr-g-TPU-PETA and Acr-gPPU-PETA) self-emulsifying systems are obtained by grafting -NCO group modified polyurethane acrylates with acrylic copolymer prepared from n-butyl acrylate, styrene,βhydroxyethyl methacrylate and acrylic acid The self-emulsifying systems showed Newtonian fluidity with viscosity closed to that of water, the solid contents were around 30% The T〓 of 15～4℃ for dried film before photocuring favored film formation at room temperature DSC and DMA results showed that PU-PETA is compatible with acrylic resin in the grafted resin The TG and dTG curves for Acr-g-PU-PETA samples were substantially different from the corresponding blends, and the brodened dTG peaks for photocured grafted resin suggest that there might be multiple interactions among chain segments The photocued film of the grafted resins self-emulsifying system exhibited good overall properties with polyurethane acrylate grafts ranging from 30% to 50%, and Acr-g-TPU-PETA series showed better properties than Acr-gPPU-PETA series The adhesion of the photocured film was 1～2 grade, impact strength was 50kg-cm and flexibility was 1mm The Shore hardness and the adhesion of the film decreased markedly if PETA was replaced by HEMA as photoactive group due to the lower C=C double bond content in the grafted resin The polyhydroxy amine-linked thioxanthones photoinitiators can be evenly dispersed in self-emulsifying system without color spot appearing in the dried film The films photocured with IV〓～IV〓 generally exhibited higher Shore hardness, gloss and solventresistance than that cured with Irgacure 2959 and did not induce the rusting of the iron substrate Pigmenting with titanium oxide had no effect on the photocuring The polyhydroxy amine-linked thioxanthone IV〓 and IV〓 can be new candidates for the formulation of titanium oxide pigmented photocurable water-borne coatings for their pale-yellow appearance and slight interference with the color of the coatings WB 4759 with high water-solubility coalesced and separated from the dried resin film, and even induced the rusting of iron substrate.

以丙烯酸丁酯，甲基丙烯酸-β-羟乙酯，丙烯酸及苯乙烯合成厂丙烯酸共聚树脂，并与含-NCO端基的聚氨酯丙烯酸酯接枝反应，经水性化后，得到两个系列（Acr-g-TPU-PETA和Acr-g-PPU-PETA）各5个不同配比的丙烯酸树脂接枝聚氨酯丙烯酸酯自乳化体系，粘度与水相近，为牛顿流体，固含量30％左右。光固化前干燥涂膜的玻璃化转变温度在-15℃～4℃之间，有利于室温下成膜。DSC及DMA谱表明两种树脂基本相容。Acr-g-PU-PETA的热失重行为明显不同于共混材料，接枝样dTG峰明显宽化，表明接枝样中链段之间的相互作刚有多重性，丙烯酸树脂与聚氨酯之间有一定的相容性。接枝树脂自乳化体系光固化涂层的综合性能以聚氨酯丙烯酸酯成分为50％～30％者相对较好，且以Acr-g-TPU-PETA系列更理想。光固化膜的附着力为1～2级，冲击强度为50kg·cm，柔软性多为1mm。以HEMA代替PETA作为接枝树脂的活性基团，碳—碳双键密度太低，光固化膜交联点太少，硬度和附着力均较差。多羟基胺连硫杂蒽酮光引发剂能均匀分散于树脂自乳化体系和接枝树脂干膜中，不出现色斑，光固化膜肖氏硬度一般高于以Irgacure 2959为光引发剂的光固化膜，光泽度及耐丁酮溶剂性能均有所提高，不会诱导铁基生锈，钛白着色对光固化结果几乎没有影响。本论文所合成的多羟基胺连硫杂蒽酮光引发剂IV〓与IV〓为浅黄色，对光固化涂层的颜色干扰较小，为配制钛白着色光固化水性涂料提供了新的光引发剂。水溶性太强的WB 4759在干膜中易聚结析出，且对所附着的铁基有诱导锈蚀作用。

D-Pantothenyl alcohol, also called ortho-vitamin 85, is an important nutrition suppled substance. It has been widely applied in the field such as medicine, cosmetic, foodstuff, feed additive, and so on. The preparation of D-pantothenyl alcohol and the optimization of key factor are discussed mainly in this paper. It mainly includes three section.In the first section, with formaldehyde, isobutyl aldehyde and diethyl oxalate as the starting materials, D-pantolactone is prepared via three steps including condensation, catalytic hydrogenation and physical resolution. The specific rotatory power of the product is consistent with imported product.

D-泛醇，俗称原维生素B_5，属维生素B旋类营养增补剂，广泛应用于医药、化妆品、食品、饲料等领域，本文着重探讨了其制备及关键因素的优化，主要内容可分三部分：第一是D-泛内酯的制备，先以甲醛、异丁醛和草酸二乙酯为起始原料合成酮基泛内酯，再经催化氢化得到DL-泛内酯，然后通过物理拆分获得D-泛内酯，得到产物的比旋光度与进口产品基本一致。

Polyurethane-acrylics hybrid latexes were prepared using isophorone diisocyanate, dimethylol propanoic acid and polypropylene oxides of different molecular weights as main materials for PU component, and butyl acrylate, methyl methacrylate and a crosslinker, trihydroxymethyl propanetriacrylate as main acrylic monomers. Hydroxyethyl acrylate was used as the coupling agent between PU and AC.

以异佛尔酮二异氰酸酯、二羟甲基丙酸和聚丙醚二醇等为聚氨酯原料，丙烯酸丁酯、甲基丙烯酸甲酯、三羟甲基丙烷三丙烯酸酯为丙烯酸酯类单体，丙烯酸羟乙酯为聚氨酯和聚丙烯酸酯间的偶联剂合成了丙烯酸酯改性水性聚氨酯乳液。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。