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Methods:Celiac injection of Acetamide hyposulfite 300mg/for 2days to rat was used as an animal model of hepatorenal syndrome.

给大鼠腹腔注射硫代乙酰胺300mg/,共2天,制造肝肾综合征模型。测定大鼠血中ALT/GPT、CRE、UREA、TBL、NO、内毒素、ET及ATⅡ的量。同时测定16h尿量,并计算肌酐清除率。

Objective To evaluate relationship between urine NAG isoenzyme and acute cerebrovascular disease. Methods The activity of urine NAG isoenzyme, NAG/Cr and blood NAG isoenzyme in 47 patients with acute CVD (15 patients with brain hemorrhage and 32 patients with brain infarction) were examined by p-nitrobenzene chronometry.

目的 探讨尿液N-乙酰-β-D-氨基葡萄糖苷同工酶与急性脑血管病的关系方法采用对硝基酚比色法,分别测定了47例急性脑血管疾病患者(其中脑出血15例,脑梗死32例)的尿液NAG同工酶谱、尿NAG与尿肌酐的比值、血清NAG活力。

Water,Hydrogenated Polyisobutene,Cyclohexasiloxane,Glycerin,Alcohol Denat,Cetearyl Alcohol,PEG-20,Petrolatum,C13-14 Isoparaffin,Zea Mays Oil,Tocopheryl Acetate,Hydroxypropyl Tetrahydropyrantriol,Hydrolyzed Soy Protein,CI 14700/Red 4,Phenoxyethanol,Adenosine,PEG-100 Stearate,Ethylparaben,Triethanolamine,Polyacrylamide,Malus Domestica Stem Cell Culture,CI 19140/Yellow 5,Dimethyl Isosorbide,Dimethicone,Dimethiconol,Limonene,Xanthan Gum,Pentaerythrityl Tetra-Di-T-Butyl Hydroxyhydrocinnamate,Linalool,2-Oleamido-1,3-Octadecanediol,Capryloyl Salicylic Acid,Acrylates/C10-30 Alkyl Acrylate Crosspolymer,Passiflora Edulis Seed Oil,Disodium EDTA,Castanea Sativa Seed Extract,Butyrospermum Parkii· Cetyl Alcohol,Butylene Glycol,Octyldodecanol,Cetearyl Glucoside,Methylparaben,Citronellol,Prunus Armeniaca Kernel Oil,Laureth-7,Coumarin,Oryza Sativa Bran Oil,Glyceryl Stearate,Fragrance

水,甘油,氢化聚异丁烯,液体石蜡/矿油,丁二醇,环己硅氧烷,鲸蜡醇,甘油硬脂酸酯,棕榈油,玉米胚芽油,PEG-100硬脂酸酯,白蜂蜡/蜂蜡,肉豆蔻醇肉豆蔻酸酯,石蜡,香精,腺苷,苧烯,山梨醇,CI 14700,CI 19140,稻糠油,杏仁油,EDTA二钠,羟丙基四氢吡喃三醇,苯氧乙醇,聚乙二醇-14M,异十六烷,氢氧化钠,辛基十二醇,季戊四醇四(双-t-丁基羟基氢化肉桂酸)酯,山梨坦三硬脂酸酯,水解大豆蛋白,卡波姆,鸡蛋果籽油,苹果果实提取物,欧洲栗籽提取物,异山梨醇酐二甲醚,聚山梨醇酯-80,辛酰水杨酸,2-油酰胺基-1,3-十八烷二醇,氯苯甘醚,麦芽糖醇,香豆素,黄原胶,微晶蜡,丙烯酰胺/丙烯酰基二甲基牛磺酸钠共聚物,丙二醇,芳樟醇,香茅醇,玉米油,羟苯丙酯,羟苯甲酯

Urinary microalbumin was determined with immunoturbidimetry, urinary NacetylD-glucosaminidase,βDgalactosidase(GAL and glycyl proline dipeptidyl aminopeptidase were determined with rate, urinary creatinine was determined with Jaffe rate.

对127例糖尿病患者,采用免疫透射比浊法检测尿mA,速率法检测N乙酰βD氨基葡萄糖苷酶、βD半乳糖苷酶、甘氨酰脯氨酸二肽氨基肽酶,Jaffe速率法测尿肌酐。

Macerate 1.0g of the powdered sample with 20.0 ml of chloroform plus 0.3ml of 25% NH_4 OH in a glassstoppered flask overnight.

本文报道用不含粘合剂的氧化铝薄层,以二甲苯-丙酮-无水乙醇-二乙胺(50:40:10:0.6)为展开剂分离茄科植物中的莨菪碱、东莨菪碱、山莨菪碱、樟柳碱及红古豆碱等五种莨菪烷生物碱,用改良Dragendorff试剂-Wagner试剂(1:1)显色,定量收集莨菪碱、东莨菪碱及山莨菪碱的斑点,莨菪碱和东莨菪碱用氨甲醇洗脱,蒸干洗脱液后分别用pH 5.6及pH 4.5的溴甲酚绿溶液作比色测定;山莨菪碱用4%醋酐氯仿洗脱,蒸干洗脱液后用pH 5.6的溴甲酚绿溶液作比色测定。

Jiangmen City, Czech Run Chemical Trading Co., Ltd. operating chemical raw materials, mainly toluene, xylene, a rough, crude dimethyl, mixed aromatics, mesitylene, crude Sanjia, mixed dimethoxy, methylal, n-butyl, B ester, n-butyl alcohol, isobutyl alcohol, vinyl acetate, styrene, butyl ether, cyclohexanone, 6 #, 120 #, 200 #, titanium dioxide, phthalic anhydride, DOP, isopropanol for Main Product, Quality Assurance , the price advantage of abundant supply.

江门市捷润化工贸易有限公司经营化工原料,主要为甲苯、二甲苯、粗甲、粗二甲、混合芳烃、三甲苯、粗三甲、混二甲、甲缩醛、正丁酯、乙酯、正丁醇、异丁醇、醋酸乙烯、苯乙烯、丁醚、环己酮、6#、120#、200#、钛白粉、苯酐、DOP、异丙醇为主营产品,质量保证,价格优势,货源充足。

The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4,5-二羧酸咪唑为原料的较佳工艺:1 脱羧反应:4,5-二羧酸咪唑40g,醋酐1200ml,回流10h,过滤并将滤液浓缩至干,所得固体加至50%的乙醇溶液回流,过滤并将滤液自然冷却过夜,过滤得固体;2 酯化反应:4(5)-羧酸咪唑50g,乙醇1000ml和浓硫酸60ml,加热回流2h,5%浓度NaOH溶液调节至pH=8,减压浓缩至干,加入少量水回流,自然冷却过夜并过滤得固体;3 还原反应:LiAlH410g,乙醚300ml和4(5)-羧酸咪唑乙酯28g,常温反应1.5h,小心滴加25ml水后过滤,滤渣溶于300ml甲醇中并过滤,收集所得乙醚和甲醇滤液浓缩至干,将所得固体溶于300ml乙醇中加热回流,后将溶液浓缩至约30ml,冷却并过滤得固体,该路线总收率为49.6%。

Amino to acetyl phenol, in have technology of two kinds of production domestic and internationally, acetic anhydride craft of the United States, acyl changes temperature to have 75 ℃ only, acyl changes mother liquor not apply mechanically, deputy reaction is little, of production thick tasting is kind of white almost, purificatory craft is very simple, activated carbon dosage only 2~3%, the Kun that its product does not have glow material almost in different third alcohol inferior the sealed impurity of amine impurity and minim, settleclear lightness it may not be a bad idea, the product quality that acetic anhydride craft produces is good, but close rate low, cost is high.

对乙酰氨基酚,在国内外有两种生产工艺,美国的醋酐工艺,酰化温度只有75℃,酰化母液不套用,副反应少,生产的粗品几乎是类白色,精制工艺就非常简单,活性炭用量仅2~3%,其产品在异丙醇中几乎无红光物质的醌亚胺杂质及微量的未知杂质,澄明度也好,醋酐工艺生产的产品质量好,但收率低、成本高。

By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料,经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸;并进一步改进和优化了合成工艺条件:即在催化剂三氯化铝过量50%并有三乙胺存在的条件下,中间体2-(4-十二烷基苯甲酰基)苯甲酸收率为72.45%;关环反应采用氯仿作溶剂,利用类似分水器的装置有效控制反应温度以减少碳化,2-十二烷基蒽醌的收率为68.1%。

Catecholamine requirements were significantlyless in the treated than in the nontreated patients.

记录基础值、体外循环开始前后、监护室直至术后第一天的血流动力学、内脏灌注压(胃动脉 CO2间隙)、肝功能(血浆谷胱甘肽α转换酶浓度)、肾功能(肌酐清除率、尿中 N-乙酰基-β-D-氨基葡萄糖酶)、心肌缺血(血浆肌酐激酶 MB 和肌钙蛋白 T 的浓度)、炎性反应(弹性蛋白酶、白介素-6和-8的血浆水平)和内皮细胞的完整性。

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