乙腈

Methods tetrahydrofuran: 0.2% citric acid (14∶1∶85) was used as mobile phase at a velocity of 1 ml·min-1 and the detection wavelength was set at 360nm. ResultsRutin was found in SFE extract of Sparganium Stoloniferum.

方法在聚酰胺膜上点样，以80%乙醇作为展开剂鉴别芦丁，采用Symmetry C18色谱柱，以乙腈-四氢呋喃-0.2%枸橼酸（14∶1∶85）为流动相，柱温25℃，在流速为1.0 ml·min-1，360 nm的检测波长下，测定芦丁含量。

In the third chapter, the photoabsorption of NO, CO, acetonitrile, acrylonitrile, benzene and toluene of benzene series have been measured by using a homemade experimental apparatus of cylindrical multi-stage ion chamber with high flux SR source. The ionization energies of some electron states are given. Their superexcited states, autoionization Rydberg states have been analyzed. By the analysis and comparison, our results are accurate and credibility.

在第三章中，利用高通量的同步辐射光源和自制的多级光电离吸收池装置，测量了NO、CO、乙腈、丙烯腈、苯系物中的苯和甲苯的光吸收谱，给出了部分电子态的电离能，分析了其中的自电离Rydberg态结构和一些振动能级，对部分结构做了精确指认，经过分析和比较，我们所得的结果比较精确和可靠。

By using isopropyl benzene as the internal standard material, using Agilent 1100 HPLC, using methanol-acetonitrile-water as mobile phase ,using three-component grade elution program, the components that contain benzene such as TALD,PT,4-CBA,TA,BA,PX and internal standard material isopropyl benzene in liquid phase product was analysed. Shimazu6A GC was used to analyse the solvent acetic acid and internal standard material isopropyl benzne in liquid phase.

以异丙苯为内标物，应用Agilent1100高效液相色谱仪，用甲醇－乙腈－水为流动相，采用三元梯度洗脱程序分析液相产物中的含苯环组分对甲基苯甲醛、对甲基苯甲酸、对羧基苯甲醛、对苯二甲酸、苯甲酸、对二甲苯和内标物异丙苯，应用Shimazu6A气相色谱仪分析液相中的溶剂醋酸和内标物异丙苯。

By using acetonitrile-water (pH=3.85) as the mobile phase, with a flow rate of 1.0mLmin^(-1), detected at 294nm, washed by gradientelution, the mian alkaloids can be separated in HPLC. The figure was applied to qualitative analysis, and quality control of alkaloids in thesium chinese turcz.in some extent.

在流动相为乙腈－水(pH=3.85)，流速为1.0mLmin1，检测波长为294nm的条件下，进行梯度洗脱，在HPLC图谱上百蕊草提取液中主要生物碱可得到理想分离，图谱可为定性分析提供依据，并可在一定程度上进行百蕊草生物碱物质的质量控制。

It was found that NBD-C is an efficient gelator of acetonitrile, and the gel system possesses very smart thixotropic property.

实验结果表明，NBD-C对乙腈具有很强的胶凝作用，且该凝胶体系具有显著的剪切触变性。

The experimental results showed that the transmissivity of in the range of 190 to 300 nm is comparable to that of and.

实验结果表明，在190～300nm波长范围内，乙腈的透过率与、的相当，而的透过率略低于、，在190～210nm波长范围内透过率最差。

Acetonitrile-sodium chloride, trichloromethane and acetone-dichloromethane were used to extract organophosphorous pesticides respectively. Pulsed-flame photometer detector was used to analyze the extraction rate of these three solvents. Flame ionization detector was used to analyze the content of impurity in the samples extracted by those three solvents.

分别采用乙腈－氯化钠法、三氯甲烷法和丙酮－二氯甲烷法提取蔬菜样品中残留的有机磷农药，使用带脉冲式火焰光度检测器的气相色谱法比较了三种提取方法有机磷农药的提取效率，使用带火焰离子检测器的气相色谱法分析了三种提取方法杂质溶出量。

The clenbuterol and ractopamine of specimen was extracted by 0.5% tungstenic acid: methanol (80:20). It was then purified by Oasis MCX. The mobile phase was 4 mmol/L ammonium acetate: acetonitrile (80:20). PDA detector was used for separation and detection.

采用0.5%钨酸：甲醉(80：20)提取试样中的盐酸克伦特罗和莱克多巴胺，用Oasis MCX小柱净化，4mmol/L乙酸胺溶液：乙腈(80：20)为流动相，用PDA检测器分离测定。

This is the first report of pectenolone and pectenoxanthin, two types of carotenoid, in the muscle of the Yesso scallop.3 Roles of the carotenoids composition and accumulation in Yesso scallopThe method for detecting carotenoids using reverse phase high performance liquid chromatography was developed. The conditions of RP-HPLC analysis were an analytical scale (200×4.6 mm, inner diameter 5μm) Eclipse XDB-C18 column of Agilent corporation; 10μl injection volume; 25°C column temperature; acetonitrile, methanol and methylene dichloride mobile phase (40:56:4, V/VV) with 0.1% BHT; 1.0 ml per minute flow rate; 450 nm UV-VIS detector; 8 minutes elution.The carotenoids from orange muscle of Yesso scallop of 7, 10, 12, 15, 18, 22 months old was detected using the method refered above.

通过柱层析、高效液相等手段对橘红色闭壳肌中的主要类胡萝卜素进行了提取分离，分离提纯得到两种类胡萝卜素，并通过MS、~1H-NMR和~(13)C-NMR对其进行结构鉴定，结果表明(3S，3\'R)-3，3\'-dihydroxy-7\'，8\'-didehydro-β，β-Caroten-4-one和(3S，3\'S)-7，7\'，8，8\'-tetradehydro-β，β-Carotene-3，3\'-diol，俗称pectenolone和pectenoxanthin是橘红色闭壳肌中的主要类胡萝卜素，这是国内外首次对虾夷扇贝闭壳肌中的类胡萝卜素进行提纯及结构鉴定。3虾夷扇贝类胡萝卜素的种类组成和累积变化规律建立了橘红色闭壳肌中类胡萝卜素的HPLC分析定量检测技术：色普柱为Agilent公司的Eclipse XDB-C18柱200mm×4.6mm，i.d.5μm进样体积，5μl ；流速1ml/min；检测波长450nm；柱温25℃；流动相为乙腈：甲醇：二氯甲烷(V/V/V=40：56：4并加入0.1%的BHT；分离时间为8min。

Thus, the thermodynamic equilibrium was shifted and the yield of cyclic carbonates was improved.

在乙腈体系中，以不同的乙酸盐作催化剂，研究了CO2与二醇合成环状碳酸酯的反应。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。