乙腈

Methods Using Diamonsil ODS1 C18 Column, acetonitrile- 0.033mol/L Potassium Phosphate Monobasic acid(35:65) as the mobile phase,detection wavelength as 265nm and flow rate was 1.0ml/min.

HPLC用外标一点法，Diamonsil ODS1 C18柱，乙腈- 0.033mol/L磷酸二氢钾溶液(35：65)为流动相，流速为1.0ml/min，λ=265nm。

Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.

用甲苯作溶剂，使三乙烯四胺和N，N-二甲基甲酰胺二甲基缩醛在85℃反应2 h，得到中间体双咪唑啉，产率90.4%，在乙腈溶剂中，碳酸钾存在下，双咪唑啉和1，2-二溴乙烷进行扩环反应，得到环状中间体一溴盐，产率78.7%，一溴盐经碱性水解2 h，得到1，4，7，10-四氮杂十二烷，产率74.2%。

The spectroscopic characteristics of C60 on Ag electrode s in nonaqueous solution were studied by surface-enhanced Raman scattering technique.

采用表面增强拉曼光谱技术研究了乙腈溶液中C60的悬液在银电极表面的光谱特征，得到了银电极表面C60团簇和表面吸附C60分子的光谱信息。

This thesis is constituted by four parts: In the first part a summarization is given on the main total synthetic methods of isoflavones, for example, deoxybenzoin method which generally involves two steps wherein a phenol is reacted in the presence of a Lewis acid with phenylacetic acid to generate an intermediate deoxybenzoin which is then cyclized with a one carbon electrophile.

本论文主要工作包括四部分：第一章综述了近年来全合成异黄酮的主要方法：脱氧安息香法，是以多羟基苯酚与苯乙酸或苯乙腈在Lewis酸存在下，反应生成中间体脱氧安息香，然后再与亲电碳试剂进行关环反应生成异黄酮。

Results The optimum condition was μ-Bondapak C18 column with acetonitrile-water-0.05% phosphonic acid gradient elution system, 1.0ml min^(-1) flow rate, 267 nm. detection wavelength and 23~26℃ temperature. The analysis ended within 45 min.

结果 在色谱柱为μ-Bondapak C183.9mm×300mm，10μm；流动相A相为乙腈，B相为0.05%的磷酸水溶液；流速为1.0ml/min；检测波长是267nm及温度为23~26℃的条件下；经45min梯度洗脱，成功的分离分析了桂枝汤中的4个成分。

The nickel, lead, cadmium and mercury ions were pre-column derived by tera-(2-aminophenyl)-porphine (T2APP). These chelates were enriched by solid phase extraction with C18 cartridge and the enrichment factor of 50 was achieved.

中草药样品用微波消化，样品消化液中的镍、铅、镉、汞用四－－卟啉(T2APP)柱前衍生，然后用ZORBAX RP18固相萃取小柱萃取富集镍、铅、镉、汞的T2-APP络合物，富集倍数为50倍；经富集后的络合物用乙腈和0.05mol？

Methods:The RP-HPLC method was applied and protocatechuic aldehyde was used as the internal standard substance.

采用RP-HPLC法，以原儿茶醛为内参照物，色谱柱：Luna C_(18)柱(250mm×4.6mm，5μm)，流动相：0.05%磷酸水溶液-乙腈，梯度洗脱程序为：0min时A-B(100∶0)，80min时A-B(67∶33)，85min时A-B(60∶40)，100min时A-B(60∶40)，流速：1.0mL·min~(-1)，检测波长：280nm。

The determination of quercitin was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using methanol-water-phosphoric acid (V:V:V=60.00:40.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 360 nm. The determination of gallic acid was performed on Century SIL C18 BDS (250 mm×4.6 mm, 5μm) column, using acetonitrile-water-phosphoric acid (V:V:V=5.00:95.00:0.02) as mobile phase at a flow rate of 0.8mLmin^(-1) and UV detection at 272 nm.

槲皮素的测定条件为：Century SIL C18， BDS(250.0mm×4.6mm， 5μm)色谱柱，流动相为甲醇－水－磷酸（体积比为60.00：40.00：0.02），流速为0.8mLmin^(-1)，检测波长为360nm；没食子酸的测定条件为：Century SIL C18 BDS (250.0mm×4.6mm， 5μm)色谱柱，流动相为乙腈－水－磷酸（体积比为5.00：95.00：0.02），流速为0.80mLmin^(-1)，检测波长为272nm。

Two solvent systems which were MeOH -50% MeOH and 95% alcohol - water were studied by the content of salvianolic acid B and salviol ⅡA and the icon of Salvia miltiorrhiza Bge..

采用C18柱，乙腈-0.35%冰醋酸溶液梯度程序洗脱，以丹参酮ⅡA和丹酚酸B含量为指标并结合图谱，综合考察甲醇-50%甲醇、95%乙醇-水两套溶剂系统提取丹参药材的效果。

Methods The determination was carried out over a Symmetry C18 column at 25℃. Methods tetrahydrofuran: 0.2% citric acid (14∶1∶85) was used as mobile phase at a velocity of 1 ml.min-1 and the detection wavelength was set at 360nm. ResultsRutin was found in SFE extract of Sparganium Stoloniferum.

方法在聚酰胺膜上点样，以80%乙醇作为展开剂鉴别芦丁，采用Symmetry C18色谱柱，以乙腈-四氢呋喃-0.2%枸橼酸（14∶1∶85）为流动相，柱温25℃，在流速为1.0 ml.min-1，360 nm的检测波长下，测定芦丁含量。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？