乙腈

The preparation method comprises the following steps in sequence:(1) metric acetonitrile is added into a dual-bottleneck distilling flask that is provided with a refluxing and condensing tube, and simultaneously, long-chain dialkyl methyl tertiary amine and relevant saturated dihalide are added thereof;(2) nitrogen is pumped for 10 to 20 minutes for deoxidizing;(3) a magnetic mixing reaction is carried through for 10 to 15 hours under the condition of 78 to 83 DEG C.

其制备方法依次包括以下步骤：(1)在装有回流冷凝管的二颈蒸流烧瓶中，加入计量的乙腈，同时按一定比例加入二长链烷基甲基叔胺与相应的二卤代烷；(2)通氮气10-20分钟，排除氧气；(3)在78-83℃条件下磁力搅拌反应10～15h。

To establish a MPLC method for the content determination of resveratrol in Polygonum cuspidatum Sieb. Et. Zucc, Analytical column SOURCE 5RPC ST 4.6/150 was used with a mixture of acetonitrile+water (30+70,volume ratio ) as mobile phase ,with a flow rate of 1ml/min and the UV detection wavelength was 306nm, The linear range was 0.6-1.6mg/ml (r=0.9919). The average recovery of prodatin was 103.0%-90.4%(RSD=7.21%). The method is convenient and accurate. Result indicated a reverse phase chromatography media based o n polystyrene/divinyl benzene has excellent resolution for resveratrol in cuspidatum. P rovide theoretical support for process development.

色谱条件采用SOURCE 5RPC ST 4.6/150预装柱，以乙腈/水(体积比30/70)溶液为流动相，流速1ml/min、检测波长为308nm，结果表明，白藜芦醇在0.6～1.6mg/ml的浓度范围内峰面积积分值与浓度的相关系数r=0.9919；所测定的虎杖饮片中白藜芦醇平均含量为0.304％，平均回收率为103.0％～90.4％；实验表明，以聚苯乙烯为基架的反相介质对于虎杖中自藜芦醇具有良好的分辨率，适合其有效成分的检测、分离，对虎杖中白藜芦醇制备的科学研究过渡到工艺开拓有很好的借鉴。

Its electroosmotic flow properties are investigated in a variety of nonaqueous media (methanol and mixtures of methanol and acetonitrile).

利用溶胶凝胶技术改进了二氧化锆涂层毛细管的制备方法，并系统的研究了非水体系中(甲醇以及甲醇和乙腈的混合溶剂)二氧化锆涂层毛细管在不同条件下的电渗流行为。

MethodsSeparation was performed on an Agilent ZORBAX SBC18 (4.6 mm×250 mm, 5 μm) analytical column with mobile phase consisting of acetonitrile and water with gradient elute at the flow rate of 1.0 ml/min and the column temperature 40℃.

色谱柱： Zorbax SBC18柱（250 mm×4.6 mm，5 μm），流动相∶乙腈水，检测波长：203 nm，柱温：40℃，流速：1.0 ml/min，分析时间：90 min。

The results show that among the acetoacetonate complexes,Co_3 has the best catalytic activity.The optimum reaction conditions were as follows:0.764 mmol of Co_3,mole fraction of ethanal 10%based on the substrate,room temperature,oxygen pressure 2 MPa,reaction time 11h and solvent acetonitrile.Under these conditions,13.3%p-chlorobenzaldehyde was obtained with 15.3%conversion and 87.2%selectivity.The oxidation can also be carried out without solvent with 8.1%conversion,89.1%selectivity and 7.2%yield respectively.

在金属配合物中Co_3的催化性能最好，在其用量为0.764 mmol、乙醛用量为反应物物质的量的10%、氧气压力为2MPa时，以乙腈为反应介质，室温下反应11h，反应的转化率和选择性可达15.3%，87.2%，对氯苯甲醛收率可达13.3%；反应也可在无溶剂时进行，此时反应的转化率、选择性及醛的收率分别为：8.1%，89.1%，7.2%。

Conductive polythiophene film was electrochemically deposited by direct oxidation of thiophene in boron thrifluoride diethyl etherate and in the mixed electrolyte of BFEE and acetonitrile.

用电化学方法分别在纯的三氟化硼乙醚离子溶液中，三氟化硼乙醚+乙腈溶液中在导电氧化锢锡ITO电极上成功聚合噻吩。

A HPLC/ESI-MS method studied on relative compounds of chloramphenicol succinate ;Column:an Agilent ODS column 250×2.1mm;Mobile phase: 0.05M ammonium formicate buffer PH4.0/acetonitrile=80/20 ,flow0.2ml/min, and λ276nm;Mass:trap ion mass;source:ESI;Scan mode:negative ion scan.

液相色谱条件为色谱柱：Agilent C18 2.1mm×250 mm；流动相：流动相0.05M甲酸铵用甲酸调pH至4.0 /乙腈=80/20，流速0.2ml/ min，检测波长276nm；质谱条件为离子肼电喷雾质谱仪，离子源：ESI；检出模式：负离子检测。

Glyoxal in cosmetic sample was extracted by the solution of acetonitrile and water.

样品用乙腈－水溶液溶解，与2，4-二硝基苯肼在弱酸条件下衍生化反应，衍生物直接用HPLC测定，用外标法定量。

Ten batches of Cortex Moutan Carbonisatum were measured by HPLC with Paeonol as a reference substance and the HPLC analysis was performed on a Hedera ODS-3 Chromatographic Column (4.6 mm×150 mm, 5 μm), with methanol to Acetonitrile (1∶1) and 0.5‰ trifluoroacetic acid solution as mobile phase in gradient mode and the detection wavelength was at 258 nm.

采用Hedera ODS-3柱(4.6 mm×150 mm，5 μm)，流动相甲醇-乙腈(1∶1)-0.5‰三氟乙酸水，梯度洗脱，检测波长258 nm。

Hydroxyacetic acid was synthesized by glycolonitrile in the presence of H2SO4 , and it was separated by applying extraction based on chemical complexation and solvent method.

以羟基乙腈为原料，在酸性条件下水解合成羟基乙酸，并采用络合萃取法和溶剂溶解法分离羟基乙酸。

My first article for Screen Power Magazine, which is to this day is the official magazine of Jackie Chan, was a DVD review of the Hong Kong actioner Gen-X Cops, starring Nicholas Tse and Daniel Wu.

我的第一篇文章为屏幕力量杂志，在对这天是Jackie Chan 正式杂志，是香港actioner Gen X 警察的DVD 回顾，担任主角Nicholas Tse 和丹尼尔吴。

His lips grazed hirs, Now what are you going to do?

他的唇使吃草了 hirs，现在你将要做什麼？