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The results show that the two free secondary amines of TAIW are nitrated firstly and then the four acetyl groups of TAIW are nitrolysed one after one under conditions of elevating the reaction temperature.

试验结果表明:TAIW笼底的两个游离仲胺基很容易首先发生硝化作用,在升温条件下,四个乙酰基再逐个发生硝解。

Results:It is suggested that the drug significantly protectes liver from CCl4,thioacetamide and galactosamine in mice and rats,lowers the activity of enzyme ALT in serum,shorten the sleep duration of CCl4-damaged mice induced by embuter,inhibites HBsAg in vitro,and potentiates non-specific immunity in mice and rats.

结果:研究表明,该药对四氯化碳、硫代乙酰胺和氨基半乳糖引起小鼠及大鼠的急性肝损伤有明显的保护作用,能降低谷丙转氨酶;缩短CCl4肝损伤小鼠戊巴比妥钠的睡眠时间;抑制体外乙肝病毒表面抗原;对非特异性免疫有一定增强作用。

The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water(10∶60∶30)(including 0.14%n-butyamine 0.1%acetic acid)at a flow rate of 1 mL*min-1 and detected at 220 nm during 1~7 min and at 273 nm during 7~16 min.

氮气吹干有机层,残留物用流动相重新溶解后,用Hypersil BDS C18柱分析,流动相为乙腈-甲醇-水(10∶60∶30),内含正丁胺0.14%和冰醋酸0.1%,流速为1 mL*min-1,检测波长:1~7 min用220 nm,7~16 min用273 nm。

Although CdS and NiSe belonged to the same crystal system, they had a great difference in the morphology of products produced in ethylenediamine by a solvothermal process. By making a crytallographic comparison between CdS and NiSe, I thought that fourcoordinated crystals were more prone to grow one-dimensionally in the stacking direction of tetrahedrons. This hypothesis could also be embodied in many examples.

硫化镉和硒化镍的晶体结构都为六方晶系,但在以乙二胺为溶剂的溶剂热条件下合成出的产物形貌有很大的差别,我们通过对两类晶体结构的结晶学比较,我们认为4配位的晶体更趋向于生成一维纳米材料,并提出生长方向即为四面体堆积方向,这一假设也能得到许多例子的证实。

Keratin mutation predisposes to mouse liver fibrosis and unmasks differential effects of the carbon tetrachloride and thioacetamide models.

角蛋白突变诱发小鼠肝脏纤维化,揭示四氯化碳和硫代乙酰胺模型的的差别效应

Theanine, the ethyl amide of glutamic acid, is the main amino acid in the fresh leaf and contributes 1 to 2 percent of the dried weight, but other amino acids arise during the early part of the processing.

茶氨酸是谷氨酸的乙酰胺,它是鲜茶叶中的主要氨基酸,占干茶叶重量的1~2%,其它氨基酸则是在加工早期出现的。

The main by-product s and their separation and recovery technologies were discussed for cyclohexanone gas-phase Beckmann rearrangement.

探讨环己酮肟气相Beckmann重排主要副产物及其分离回收方法,研究1-氮杂-2-乙氧基-1-环庚烯、1,3,4,5-四氧吖庚因-2-酮及其同分异十句体等副产物回收利用生成已内酰胺的方法。

ABSTRACT:Objective To investigate the effect of calmodulin antagonist 0-(4-ethoxiyl-butyl)-berbamine on proliferation of human breast cancer cell MCF-7 and its possible mechanism.

目的 探讨钙调素拮抗剂O-4-乙氧基-丁基-小檗胺对人乳腺癌细胞系MCF-7生长的影响及其作用机制。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生,用WatersHPLC仪,AccQ-TagTM专用C18柱(3.9mm×15cm),以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A,乙腈为溶剂B,超纯水为溶剂C,进行梯度洗脱,检测波长为248nm,35min测试完毕。

The amount of Na(superscript +), NH4(superscript +), K(superscript +), Mg(superscript 2+), Ca(superscript 2+), Zn(superscript 2+) in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography. And pyridine-2, 6-dicarbexylic was used as mobile phase to separated monovalent cations and pyridine-2, 6-dicarbexylic-ethylenedi-amine-oxalic acid was used as mobile phase to separated divalent cations.

采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na、NH4、K、Mg(上标 2+)、Ca(上标 2+)、Zn(上标 2+)的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。