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The main synthetic methods and application prospect of organic energetic dinitrate salt s,ethylenediamine dinitrate,azobisformamidine dinitrate,carbohydrazinium dinitrate,polyaminoguanidine dinitrate and tetrazine dinitrate,were reviewd with 26 references.

综述了乙二胺二硝酸盐、偶氮二甲醚二硝酸盐、碳酰肼二硝酸盐、氨基胍类二硝酸盐和四嗪类二硝酸盐等有机含能二硝酸盐的主要合成方法及应用前景。

Ten novel derivatives of 1-phenyl-5-[5-(substituted anilinocarbonylmethylthio)-4-phenyl-1,2,4- triazol-3-ylmethylthio]-tetrazole were synthesized rapidly in high yields by the reaction of N--2-chloryacetanilide (3) with 1-phenyl-5-(5-mercapto-4-phenyl-1,2,4-triazol-3-ylmethylthio)-tetrazo- le (2) under microwave irradiation and phase transfer catalysis conditions.

采用微波和相转移催化法通过1-苯基-5-(4-苯基-1,2,4-三唑-5-巯基-3-甲硫基)四唑(2)与2-氯乙酰芳胺(3)反应高效、快速地合成了10种尚未见文献报道的1-苯基-5-[5--4-苯基-1,2,4-三唑-3-甲硫基]四唑。其结构经IR,1HNMR,13CNMR和元素分析表征。生物活性实验结果表明,该类化合物在较低浓度下部分化合物对小麦芽有很好的促进作用

And titanous ion; a mixture of ferrous ion, oxygen, ascorbic acid, and ethylenetetraaminetetraacetic acid.

脱穷牙胱印⒀翘?离子氧,抗坏血酸和乙四胺四乙酸混合物。

Edta titrimetric method and flame atomic absorption spectrometric method.

乙二胺四乙酸滴定法和火焰原子吸收光谱测定法

The value of oil/water partition coefficient of etofesalamide demonstrated that etofesalamide was fit to be used topically.

采用改进的Valia-Chien水平扩散池研究了卡必醇对乙氧苯柳胺体外经皮渗透性及在皮肤中的药物滞留量的影响。

In chapter four, molecular imprinting polymers against amino acid derivatives utilizing 2-VP+AM as combined functional monomer and trimethylolpropane trimethacrylate as tribasic cross-linker were prepared and result was compared with those with the same amino acid derivative as the imprinted molecules utilizing ethyleneglycol dimethacrylate as dibasic cross-linker. It was found that cross-link intensity of the molecular imprinting polymer is higher when TRIM was utilized and baseline separation for the imprinted molecule could be achieved. When TRIM was utilized as cross-linker more molecule is imprinted during the polymerization.

第四章采用2-乙烯基吡啶+丙烯酰胺复合功能单体,考察了三元交联剂三甲氧基丙烷三甲基丙烯酸酯烙印氨基酸衍生物的情况,并与二元交联剂乙二醇二甲基丙烯酸酯烙印相同氨基酸衍生物的情况进行了对比,发现三甲氧基丙烷三甲基丙烯酸酯交联剂在较小的用量下就可使分子烙印聚合物达到足够的交联度,实现烙印分子的基线分离。

Methods 42 cases of intractable heart failure were dividedinto 3 groups, and received intravenous infusion of nesiritide (12 cases), glycerol trinitrate (15 cases), and dobutamine (15 cases) respectively. Plasma rennin activity, aldosterone and angiotensin II were measured before and after infusion in 24h and 48h.

42例患者分成三组:甲组应用rhBNP;乙组应用硝酸甘油;丙组应用多巴酚丁胺静脉注射,同时检测血浆肾素活性、血管紧张素II、血浆醛固酮浓度,并在24、48h再次复查上述指标,复查左室射血分数,进行比较。

In addition, we used a modified MTT 3-(4,5-dimethylthiazol-2-yl-2,5-diphenyltetrazolium bromide assay to examine cell proliferation by dissociating the cell/alginate constructs using trisodium citrate and trypsin/EDTA.

此外,我们用改良的MMT测定被枸橼酸钠-胰蛋白酶-乙二胺四乙酸分离细胞结构的细胞增殖情况。

Polyethylene glycol, undecylenic acid, dodecylamine, nanoparticles

聚乙二醇,十一烯酸,十二胺,纳米粒子

Research result indicated that the cooperative effect between swell and precursor is main factor for the nanoparticle loaded in Nafion, and moreover, polarity of solvent and water content in Nafion also affects the load largely. To improve away the surface concentration of CdS nanocrystal on two side of membrane for general preparation, thioacetamide was first used as a precursor instead of inorganic sulfur source(H2S and Na2S) in synthesis of CdS nanocrystal. The assembly mechanism for several sulfur source had been studied, and CdS/Nafion with the character of homogeneous disperse had been prepared, which is fit for mass transmission in photocatalitic reaction. Following the investigation of several crystallizing way, simple and reliable hydrothermal-crystallizing was found. According to this way, maximal TiO2 load in Nafion achieved 43%. Activity of TiO2/Nafion or CdS/Nafion as a photocatalyst was explored initially for disintegrating liquid contamination. Maximal decompose rate achieved 86% under condition of this research.

研究结果表明:Nafion膜对纳米粒子负载量的主要影响因素是溶胀作用与前驱体协同效应,同时溶剂极性和薄膜含水量对负载量也影响相当大;本课题首次使用硫代乙酰胺代替传统无机硫源(H2S、Na2S)合成CdS纳晶,研究了各种硫源的组装机理,克服了常规技术存在的CdS纳晶趋于膜表面富集的缺点,得到了有利于光催化传质需要的体相均匀分布CdS/Nafion;研究了多种Nafion膜内纳米粒子晶化途径,找到了简单可靠的水热晶化法,TiO2纳晶最高负载量达43%;初步探索了TiO2/Nafion、CdS/Nafion作为光催化剂降解水中模拟污染物的活性,在本实验条件下最高降解率达86%。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。