乙胺

This dissertation is mainly focused on the reactivity of methylenecyclopropanes and comprises six parts. 1 The reactions of methylenecyclopropanes with phenylsulfenyl chloride, phenylselenyl chloride and diphenyl diselenide; 2 The coupling reactions of the ring-opening products derivated from methylenecyclopropanes; 3 The palladium-catalyzed ring-enlargement of mono-aryl group substituted methylenecyclopropanes to cyclobutenes. 4 The gold-catalyzed domino ring-opening and ring-closing hydroamination of methylenecyclopropanes with sulfonamides; 5 The Lewis acid-catalyzed reactions of mono-aryl group substituted methylenecyclopropanes with diethyl ketomalonate in the presence of water; 6 The iodobenzene diacetate mediated novel 1,3-dipolar cycloaddition of methylenecyclopropanes, vinylidenecyclopropanes, and methylenecyclobutane with phthalhydrazine.

本论文主要研究了亚甲基环丙烷类化合物的一些化学反应性能，共由以下六部分组成：1、亚甲基环丙烷类化合物与苯硫氯、苯硒氯及二苯基二硒的反应；2、亚甲基环丙烷类化合物开环产物的偶联反应；3、单芳基取代的亚甲基环丙烷类化合物在钯催化剂作用下的扩环反应；4、金化合物催化磺酰胺对亚甲基环丙烷类化合物的串联开环关环氨氢化反应；5、路易斯酸催化亚甲基环丙烷类化合物与丙酮二羧酸二乙酯在有水存在下的反应；6、醋酸碘苯促进的亚甲基环丙烷类化合物、亚乙烯基环丙烷类化合物及亚甲基环丁烷类化合物与邻苯二甲酰肼的新型1，3-偶极环加成反应。

Preservatives in general are troublesome to crystalline structures and especially disodium EDTA.

一般的防腐剂对水晶结构是有麻烦的，特别是乙二胺四乙基二钠。

Bi2Te3 nanocapsules have been synthesized by the aqueous chemical route at 65℃ with the addition of disodium ethylenediaminetetraacetate salt.

采用65℃低温湿化学合成方法，在添加乙二胺四乙酸二钠的情况下，制备了Bi2Te3纳米囊。

Effects of microorganism and environmental factors on persistence of acetochlor in soils were studied by bioassay using Echinochloa crusgalli.

以稗草为生物测定材料，研究了土壤微生物及环境因子对乙草胺持效性的影响。

The research aimed to establish a FIPIX method for the determination of fipronil and acephate in 36% emulsifiable concentrate.

［目的］建立在同一液相色谱条件下测定混刹中氟虫腈和乙酰甲胺磷含量的方法。

Subsequently,enol methylation of P in basic condition completed the synthesis of malyngamide O.Applied this route to the synthesis of malyngamides Q and R,the chiral unsaturated acid was connected with the vinyl chloride part by amidation,then the resulting product was converted into the corresponding aldehyde,followed by aldol condensation of the aldehyde with the chlorotitanium enolate of pyrrolidone to complete the skeleton of malyngamides Q and R,then the synthesis of them was completed via enol methylation in acid condition.

该合成路线拓展应用到malyngamides Q和R的合成时，首先用酰胺键将手性不饱和脂肪酸和烯氯片段连接，再转化成相应的醛，与乙酰基吡咯酮进行TiCl_4催化的aldol反应即得到malyngamides Q和R的骨架结构，再经过酸催化的烯醇甲基化反应完成了Q和R的全合成。

The extremities were titanic, and there was no response to touch stimulations.Our results suggested that Pentobarbital sodium inhibited neuronal firing through GABA_A receptors, therefore the local field potentials and neural firing rates were inhibited; Urethane acted on many kinds of receptors including inhibitory and excitory ones, so the local field potentials did not change significantly; however, because of the multiform receptors on the neurons, the changing of firing rates to different neurons were not the same; Ketamine mainly acted on the NMDA receptors, therefore the local field potentials and neural firing rates were enhanced, and most neural firing rates would be increased.

从这三种麻醉剂的底层作用机制来看，戊巴比妥钠通过作用于GABAA受体对神经细胞发挥抑制性作用，因此表现为场电位和神经元放电的降低；氨基甲酸乙酯同时作用于多种受体通道，既有兴奋性受体，也有抑制性受体，因此，对场电位的影响不大，但对单个神经元来说，每个神经细胞上的受体通道分布差异较大，因此，单个神经元的放电频率变化会有所不同；盐酸氯胺酮主要作用于兴奋性的NMDA受体，故整体场电位活性增加，多数神经元的放电频率也会有所升高。

A SPE procedure was suggested for extracting and concentrating fisetin by using different volume fractions of ethanol in aqueous solution as the loading conditions.

分别以中药黄栌的主要成分非瑟酮为印迹分子、丙烯酰胺为功能单体及乙二醇二甲基丙烯酸酯为交联剂，通过封管聚合法合成了分子印迹聚合物；将其装于自制的固相萃取柱中，研究了以不同体积比的乙醇-水溶液为溶剂时非瑟酮在柱上的保留行为；通过优化清洗及洗脱条件，使非瑟酮与它的结构相似物槲皮素在柱上得到了很好的分离。

Most of fluorenyl cardo polyimides exhibited excellent solubility in common organic solvents such as m-cresol,chloroform(CHCl_3), tetrahydrofuran,N-methyl-2-pyrrolidinone,N,N-dimethylacetamideetc and intrinsic viscosity in N,N-dimethylacetamideranged from 0.31-1.00dL/g.

大部分芴基Cardo型聚酰亚胺可以溶解在间甲酚，氯仿(CHCl_3)，四氢呋喃，N—甲基吡咯烷酮，N，N—二甲基乙酰胺等有机溶剂内，在DMAc内的特性粘度范围为0.31～1.00dL/g。

Methods: The model of evaluating T cell proliferation stimulated with polyclonal activators, ConA was established by vital dye carboxyl fluorescin diacetate succinmidyl ester labeling technique. The effect of a specific inhibitor for p38 MAPK, SB253580, on T cell proliferation on different doses and in different time was estimated by flow cytometry. At the same time, the percentage of proliferating T cells and proliferation index were measured by CellQuest and SPSS10.0 for Windows softwares.

以活体染料羧基荧光素乙酰乙酸琥珀酰亚胺酯染色，建立了在多克隆刺激剂刀豆蛋白A刺激下评价小鼠T细胞增殖的模型，通过流式细胞术分析p38丝裂原活化蛋白激酶的特异性抑制剂SB203580在不同剂量、不同时间对T细胞增殖的作用，并应用CellQuest和SPSS10.0 for Windows软件分析增殖细胞各代所占比例和增殖指数。

They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性，但我大喊，并在他们的方向扔石头让他们过的线索，远离我，以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。