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In this paper, SAPO-34 was microwave-assisted synthesized with diethylamine as the struc- ture-director, and the synthesized samples were calcined under air and nitrogen at 1073 K respectively.

以二乙胺为结构导向剂,在微波条件下合成了SAPO-34分子筛材料,并分别在空气和氮气氛下1073K焙烧。

Methods: All the patients recruited were randomized into the diclofenac diethylamine salt gel and diclofenac sodium gel groups and treated with local application three times daily for 14 days respectively.

4 0例患者随机分为双氯芬酸二乙胺盐凝胶组和双氯芬酸钠凝胶组进行临床对照试验,分别采用局部涂擦给药法,tid ,14d为 1疗程。

Good diastereoslectivities were observed in the addition of diethylamine to γ-ethyl-γ-methylallenyl perfluoroalkyl sulfones.

乙胺在对γ-甲基-γ-乙基氟烷基联烯砜进行加成时,反应有很好的立体选择性。

Methods: water decocting method for extracting method, ether as extraction solvent with high performance liquid chromatography, as the means, to test content of methanol 0-3 % diethylamine (73:27) as mobile phase, 242nm detected wavelength, according to the packing: Hypersil BOS C18 5 muon m size: 6 mm (4): 25 mm, standard curve basic linear, precision, accuracy, good stability and.

以水煎煮法作为提取方法,乙醚作为萃取溶剂,以高效液相色谱作为含量检测的手段,以甲醇-0。 3 %二乙胺(73∶27)作为流动相,检测波长242nm,依利特填料:Hypersil BOS C18 5μm 尺寸:4。 6 mm ×250 mm ,结果:标准曲线基本呈线性,精密度,稳定性和准确度良好。

Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液,研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

Inspected gathered in advance the body preparation method influence, the neutralizaing agent triethylamine to the disperser craft and the stability of emulsion influence, the water affinity chain extendor DMPA amount used to the river character polyurethane emulsion performance influence, the isocyanogen diethylene glycol dinitrate amount used to the river character polyurethane emulsion performance influence and the soft section low-molecular polymer dihydroxy alcohol amount used to the river character polyurethane emulsion performance influence.

考察了预聚体制备方法的影响,中和剂三乙胺对分散工艺及乳液稳定性的影响,亲水扩链剂DMPA的用量对水性聚氨酯乳液性能的影响,异氰酸酯的用量对水性聚氨酯乳液性能的影响及软段低聚物二元醇的用量对水性聚氨酯乳液性能的影响。

The sodium dihydroxy phosphate solution was added 0.4% triethylamine and adjusted its pH to 6.0 by adding 20% phosphate acid. The electrodes potential were set at 300mV, 400mV, 550mV and 650mV.

液相色谱的流动相为30mmol/L磷酸二氢钠水溶液:甲醇=90:10(其中水溶液中加入0.4%三乙胺,并用20%磷酸调pH至6.0);四组电极的检测电势分别为300mV、400mV、550mV和650mV。

The aqueous polyurethane prepolymer was prepared through step-growth polymerization of diphenylmethane diisocyanate with polyester glycol and dimethylol propionic acid, which was then neutralized by triethylamine to form the stable transparent aqueous polyurethane dispersion.

以二苯基甲烷二异氰酸酯、聚酯二醇、二羟甲基丙酸等为原料合成了水性聚氨酯预聚体,用三乙胺中和制备了水性聚氨酯的透明乳液。

The results showed that fumaric acid is most favorable to prepare MnO2 sol.

结果表明,富马酸是制备MnO2溶胶比较合适的还原剂,Span80和Tween80复配乳化剂的效果最好,在油∶溶胶=4∶1,乳状液∶三乙胺=8∶3的条件下制得的纳米MnO2微粒,其形貌为规整的球体,粒径均匀,几乎为单分散性。

The outward rectifier K+ current current was the dominant K+ current in the whole cell currents in Deiters' cells. In the presence of 200μ M linopirdine, the Ik current was not significantly effected. Our findings demonstrated that the KCNQ heteromeric or homomeric potassium channel may be the molecular basis for the peak outward K+ current and testified that the inward IKn current is mediated by KCNQ potassium channel.

在细胞外液中,加入100 μmol/L利诺吡啶后,OHCs中的四乙基二乙胺敏感的钾电流峰电流成分被抑制,稳态电流幅值减小,且电流的失活时间常数明显延长;在细胞外液中加入100 μmol/L和200 μmol/L利诺吡啶后,OHCs的内向性钾电流IKn被完全抑制;而细胞外液中利诺吡啶终浓度为200 μmol/L 时,Deiters细胞的外向整流性钾电流幅值无明显变化。

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