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The synthesis of the intermediate amidetriazinone was a crucial step in the synthesis of triazinone. Ethyl acetate was used as the initial material then was carried out for five steps hydrazine hydrate, triphosgene, chloroacetone, hydrazine hydrate respectively with the yield of 59.8%.

三嗪酮类化合物的合成关键是中间体氨基三嗪酮,本文以乙酸乙酯为起始原料,经过酯的肼解、成环反应、胺的烷基化、酮和肼的缩合、酰胺的水解五步反应合成中间体氨基三嗪酮,其收率达59.8%。

The poisoning effects of alkyl sulfur compounds on the reactivity of isoprene hydrogenation over supported Pd catalyst are more and more serious with the decrease of the molecular mass of alkyl thiols and dialkyl disulfides.

乙硫醇和二甲基二硫醚使Pd/树脂催化剂中毒的机理是,它们分别在催化剂上发生SH和S-S键断裂,并与Pd形成带烷基基团的S-Pd吸附络合物,致使催化剂上异戊二烯选择加氢活性降低。

The preparation method comprises the following steps in sequence:(1) metric acetonitrile is added into a dual-bottleneck distilling flask that is provided with a refluxing and condensing tube, and simultaneously, long-chain dialkyl methyl tertiary amine and relevant saturated dihalide are added thereof;(2) nitrogen is pumped for 10 to 20 minutes for deoxidizing;(3) a magnetic mixing reaction is carried through for 10 to 15 hours under the condition of 78 to 83 DEG C.

其制备方法依次包括以下步骤:(1)在装有回流冷凝管的二颈蒸流烧瓶中,加入计量的乙腈,同时按一定比例加入二长链烷基甲基叔胺与相应的二卤代烷;(2)通氮气10-20分钟,排除氧气;(3)在78-83℃条件下磁力搅拌反应10~15h。

Good diastereoslectivities were observed in the addition of diethylamine to γ-ethyl-γ-methylallenyl perfluoroalkyl sulfones.

二乙胺在对γ-甲基-γ-乙基氟烷基联烯砜进行加成时,反应有很好的立体选择性。

Supersonic wave disperse research indicated, ethanediol as the disperse medium, it could got suspending liquid about for firve days, but relatively large in grain size. However, combined use of lauryl sodium sulfate and maleic anhydride as disperse medium, the disperse result among water was better than the former, and it would be steady for two days.

超声分散研究表明,使用聚乙二醇作为分散介质,可得到分散五天左右的悬浮液,但分散后粒度较大,使用十二烷基硫酸钠和顺丁烯二酸酐混合作为分散介质在水中分散效果较好,可稳定两天左右。

Activity-stability experiment for the liquid phase alkylation of benzene with ethylene was proceeded for 2000hrs, the average values of ethylene conversion, ethyl-benzene selectivity and ethylation selectivity were 100%, 94.5% and 99.0% respectively.

进行了苯和乙烯液相烷基化的2 000 h 活性稳定性试验,乙烯转化率、乙苯选择性、乙基化选择性分别平均为100%、94.5%和99.0%。

Water, Sodium Laureth Sulfate, Cocamidopropyl Betaine, Cocamide MEA, Disodium Cocamphodiacetate, Sodium Lauryl Sulfate, PEG 40 Hydrogenated Castor Oil, Perfume, Sodium Chloride, Propylene Glycol, Quaternium 80, Methylparaben, Polyquaternium 10, Hydroxypropyl Guar Hydroxpropyltrimonium Chloride, Citric Acid, Diazolidinyl Urea, Tetrasodium EDTA, Polyquaternium 7, Propylparaben, Sodium Hydroxide, Panthenol, Persea Gratissima Oil, Penta Sodium Pentetate, Hedera Helix Extract, Bambusa Vulgaris Extract

水,月桂醇聚醚硫酸酯钠,椰油酰胺丙基甜菜碱,椰油酰胺MEA,椰油酰两性基二乙酸二钠,月桂醇硫酸酯钠,PEG 40 氢化篦麻油,香料,氯化钠,丙二醇,季铵盐-80,苯甲酸甲脂,聚季铵盐-10,羟丙基瓜尔胶羟丙基三甲基氯化铵,柠檬酸,重氮烷基咪唑脲,乙二氨四醋酸四钠,聚季铵盐-7,对羟基苯甲酸丙酯,氢氧化钠,泛酰醇,酪梨油,喷替酸五钠,常春藤萃取物,银竹萃取物。

The process was methanolysis ed alkyl inino-acetic acid ester hydrogen chloride salt from methyl-cyanide.

研究了由乙腈为原料经烷基亚氨基醋酸酯盐酸盐醇解制备原乙酸三甲酯的工艺方法,对投料比、反应温度、反应时间及中和指示剂等工艺条件进行了研究,得出较优惠的工艺条件。

In this paper, SiO_2-based air-water interfacial films with nano structure are templated by cationic surfactant cetyl trimethyl ammonium bromide with tetraethyl orthosilicate as precursor.

本文以正硅酸乙酯为前驱体、以十六烷基三甲基溴化铵为模板,用自组装的方法在特殊的区位——空气—水界面上制备了SiO_2的无机纳米薄膜。

Polyethylene glycol ethers of alkyl alcohols having the general formula CH3(CH2)xCH2(OCH2CH2)nOH wherein x is 8 to 20 (of which ceteareth-20, steareth-20 and steareth-100 are preferred), poloxamer 185, poloxamer 407, N,N-dimethyl dodecylamine N-oxide, and mixtures thereof, are employed to increase follicular delivery and/or follicular residence time of certain water soluble ornithine decarboxylase inhibitors of which 2-2,5-diamino pentanoic acid and its pharmaceutically acceptable salts, hydrates, optical enantiomers and racemic mixture are preferred.

使用通式为CH3(CH2)xCH2(OCH2CH2)nOH的烷基醇的聚乙二醇醚,其中x为8-20(其中鲸蜡硬脂醇醚-20、硬脂醇醚-20和硬脂醇醚-100是优选的)、poloxamer 185、poloxamer 407、N,N-二甲基十二烷胺N-氧化物及其混合物来提高某些水溶性的鸟氨酸脱羧酶抑制剂的毛囊传输和/或毛囊停留时间,优选的抑制剂是2--2,5-二氨基戊酸及其药学上可接受的盐、水合物、光学对映异构体及外消旋混合物。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。