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Acetate Substitution, A benzene solution (10 mL, 20% w/v) of alkyl halide also containing 0.5 g of PEG or tergitol was added to 1.5 g of solid, dry potassium acetate and the resulting suspension heated to reflux.

醋酸换人,苯液( 10毫升, 20 %瓦/五)烷基卤化物还含0.5 g的聚乙二醇或tergitol添加以1.5克的固体,干燥醋酸钾和由此产生的悬浮加热回流。

The alkylation of a-methylene of PhSO2CH2COPh with alkyl halides catalyzed by quaternary ammonium base resin in 50% aqueous sodium hydroxide solution was investigated.

本文以季铵碱树脂作为聚合物固载的相转移催化剂,在50%氢氧化钠水溶液中催化α-苯磺酰基苯乙酮(1)的α-亚甲基的烷基化反应。

And the morphologies of lead tungstate crystal were different when different surfactants of polygycol 200 and cetyltrimethyl ammonium bromide were added in the experiments.

以钨酸钠和醋酸铅为原料,分别加以表面活性剂聚乙二醇200和十六烷基三甲苯溴化铵,用沉淀法合成出钨酸铅纳米晶和菱形微晶。

Industrial synthetic oils currently us a variety of base oils, such as PAOs, diesters, polyalkylene glycols, and phosphate esters, among others.

工业合成油目前我们的基础油,如公共事务干事,二酯,聚亚烷基乙二醇,磷酯等,品种。

The main aromatic production technologies are reviewed which included catalytic reforming, aromatic extraction, toluene disproportionation and transalkylation process, isomerization of xylenes and separation of PX.

分析了近年来国内外聚酯和对二甲苯的供需状况及未来需求发展趋势;介绍了当前芳烃主要生产技术,包括催化重整、芳烃抽提、甲苯歧化与烷基转移、二甲苯异构化和二甲苯分离等;指出了扩大芳烃原料来源、通过催化剂的改进提高甲苯歧化过程的对二甲苯选择性、提高C9及以上重芳烃处理能力、提高乙苯转化率等将是未来芳烃技术的主要发展方向。

Examples of suitable polar volatile liquid are amines ethers especially lower alkyl ethers organic acids esters ketones glycols alcohols amides ureas sulphoxides sulphones and water.

合适的极性挥发性液体的例子有胺,醚,尤其是低级烷基醚,有机酸,酯类,酮类,乙二醇,乙醇,酰胺,尿素,sulphoxides,砜和水。

Surfactant p-octyl polyethylene glycol phenyl ether (Triton X-100) or cetyltrimethylammonium bromide was mixed with n-hexane, n-hexanol, and water for preparing reverse microemulsion.

分别以聚乙二醇辛基苯基醚(Triton X-100)或十六烷基三甲基溴化铵为表面活性剂,与正己烷、正己醇和水构成反相微乳液。

In the present dissertation, a surfactant-templated mesoporous silica molecular sieve with high pore volume, high porosity and narrow bimodal mesopore size distribution was synthesized for the first time in a reaction system, which was used usually in the synthesis of mesoporous MCM-41 molecular sieves, by a judiciously controlled two-phase sol-gel processing under basic conditions.

在本论文中,我们通过对一个通常用于制备介孔MCM-41分子筛的反应体系中正硅酸乙酯水解与缩合反应相对速率的精确调控,首次在弱碱性体系中合成了一种具有高孔隙率、大孔体积和双介孔孔分布特征的新型二氧化硅分子筛材料,简记为BMS,并对BMS二氧化硅分子筛中双介孔结构形成的原因及各种可能对其结构和性质产生影响的合成因素如Ammonia/silica摩尔比、组分浓度的变化、表面活性剂烷基链长度的调节、辅助有机物均三甲苯的引入、催化剂的结构和性质、溶剂和助溶剂的极性和用量、老化和干燥条件的变化及合成后水热处理等,利用不同的测试手段如XRD,SEM,TEM,〓Si MAS NMR,TG-DTA,N〓吸附测试等进行了系统的表征研究。

A novel method to prepare Au nanorings by self-reduction of HAuCl4 in the soft template composed of sodium dodecyl sulfate-PEG 20000 cluster at ambient temperature and atmosphere was reported, in which no hard template and extra reducer was needed. TEM image displays that the diameter of Au nanorings is (500±50)nm.

介绍一种由十二烷基硫酸钠与聚乙二醇(PEG 20000)组成的团簇为软模板,在室温、常压、无硬模板及无外加还原剂条件下自还原HAuCl4合成金纳米环的新方法。

The intermediate 5-amino-1H-pyrazole-4-carboxylic acid ethyl ester prepared in the first part underwent successively hydrazinolysis, condensations with ketene dithioacetals and alkylations to give rise to the dipyrazolyhnethanes.

从第一部分中的中间体5-氨基-1H-吡唑-4-羧酸乙酯开始,经过肼解、与乙烯酮二硫代缩醛的缩合反应和烷基化反应,合成了二吡唑基甲酮类化合物。

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