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This product was prepared w ith octamethyl-cyclotetrasiloxane and tetramethyltetravinylcyclote-trasiloxane as monomers,a low visco sity hydroxyl -terminated silicone oil as an end -bl ocking agent and tetramethylammonium hydroxide as catalyst.

以八甲基环四硅氧烷为单体,四甲基四乙烯基环四硅氧烷为改性单体,羟基硅油为封端剂和相对分子质量调节剂,四甲基氢氧化铵为催化剂,在羟基硅油质量分数小于0.13%,催化剂质量分数为0.004%~0.007%时,采用共聚法制备了相对分子质量大于45×104,收率大于90%的端羟基聚二甲基硅氧烷。

Two azobenzene-containing polyethers were synthesized and their thermotropic liquid crystalline properties were investigated.

氯乙基缩水甘油醚和GCE/羟丁基乙烯基醚分别通过阳离子聚合、光引发共聚合,获得两种聚醚,然后再分别与 4-硝基-4' -羟基偶氮苯反应,制备了两种侧链含偶氮苯生色团的液晶聚合物。

Once the hernia defects are visualized, a polypropylene or expanded polytetrafluoroethylene biomaterial is then inserted and secured to the transversalis fascia and/or Cooper's ligament with tacks or staples. The material is of a size that completely covers the myopectineal orifice.

一旦缺损区出现于视野中,送入聚丙烯或可延伸聚四氟乙烯网状补片,并将其固定于腹横筋膜上和/或Cooper韧带上,补片的大小以完全覆盖住内环口为宜。

The first step was to synthesize imidazoline. The mole ratio of oleic acid and diethylene triamine was 1:1.2, the xylene was 30%. Temperature was controlled in about 160 ℃ on this stage, timing for acylation reaction was about 1.5 hours.

第一步咪唑啉的合成:油酸和二乙烯三胺摩尔比为1:1.2,以二甲苯为携水剂,反应温度控制在160℃酰化反应1.5小时,然后升温至220℃环化反应,反应时间6.5小时。

Amine terminated polyurethane resin has been synthesized with diethylene triamine and isocyanate terminated polyurethane resin mentioned above.

4利用二乙烯三胺和自制的端异氰酸酯聚氨酯预聚物合成端氨基聚氨酯树脂。

It has shown that the tensile index and ring crush index of handsheets were increased by 15.90% and 9.65%, when phenol-formaldehyde resin modified by diethylene triamine was used in OCC pulp alone (the dosage of resin was 1.0%), and then adding cationic starch to pulp (the dosage of starch was 1.0%), the tensile index and ring crush index of handsheets were increased by 32.81% and 29.29%.

实验结果表明,二乙烯三胺改性的酚醛树脂单独作用于OCC废纸浆时(用量为1.0%),抗张指数和环压指数分别增加了15.90%和9.65%,当加入阳离子淀粉时(用量为1.0%),抗张指数和环压指数分别增加了32.81%和29.29%。

The combinative effect of the fluorine substitute and the bridging unit can make complex 2 as a highly active and selective catalyst for ethylene trimerization.

氟原子效应和桥碳原子上大取代基效应两者结合在一起,可以使络合物2成为一种高活性和高选择性的乙烯三聚催化剂。

By comparing the catalytic behavior of S3/MAO and S8/MAO, a conclusion could be drawn that the coordination of the sulfur atom to the titanium center of the active species was essential for ethylene trimerization.

通过比较S3与S8不同的催化性能,可以认为,硫原子对钛活性中心可能存在配位,而这一配位对乙烯三聚反应起重要作用。

The estrogenic activities and mutation effects of nonylphenol ethoxylates before and after microbial degradation were studied with the recombinant gene yeast and SOS/Umu test.

作者中文名:吴伟;吴滟;瞿建宏摘要:采用重组基因酵母和SOS/Umu试验研究了壬基酚聚氧乙烯醚(NP10EO)经生物降解前后的雌激素活性和致突变活性。

Their half lives were 27.29 and 69.16 days respectively. Monocrotophos degraded into both methanol extractable and unextractable residues in the submerged soil.The analysis of 14C-methanol extractable. residue by TLC and ARG indicated that degraded products of monocrotophos were triether phosphate,;N-de-methyl Azodrin, O, O-dimethyl-vinyl-phosphatc,O-demethyl Azodrin,and O, C-demethyl Azodrin.The principal degraded extratable product of monocrotophos was triether phosphate, which incresed from 5% of the parent solution of monocrotophos to a range of 28-83%, furthermore and its degradation process was much faster in the unterilized soil than in the sterilized soil.

久效磷在淹水土壤中降解为甲醇可抽提态和不可抽提态残留物,对甲醇可抽提态残留物经TLC和红外光谱分析表明,其降解物为磷酸三酯、N-去甲基久效磷、O,O-二甲基乙烯基磷酸酯,0-去甲基久效磷,以及O,C-去甲基久效磷,但主要为磷酸三酯,其含量由母液中的5%增加到28—83%,这种降解过程,在未灭菌土壤中比在灭菌土壤中快。

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