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The Stille coupling reaction between 8 iodo 9 benzyl 9H purine and RSnBu 3 (R=vinyl,2 thienyl,2 furyl,phenylethynyl and phenyl) was studied using (Ph 3P) 2PdCl 2 as catalyst and DMF as solvent.

采用 (Ph3 P) 2 PdCl2 为催化剂,DMF为溶剂,对 8 碘 9 苄基 9H 嘌呤与有机锡试剂RSnBu3 (R=乙烯基、2 噻吩基、2 呋喃基、苯乙炔基和苯基等)之间的 Stille偶合反应进行了研究,合成出了5种 8位取代的嘌呤衍生物。

Organic chlorine compounds, including hexachlorethane , pentalin , hexachlorobutadiene, HCB, pentachlorobenzene, dioxin, gammexane, tetracarp, carbon tetrachloride , chloroform and etc.

有机氯化合物,包括六氯乙烷、五氯乙烷、六氯丁二烯、六氯苯、五氯苯、二恶英、六六六、四氯乙烯、四氯化碳和氯仿等污染物。

The Solidification temperature range was defined as 110-200℃ by DSC analysis. More accelerant used can increase the casing samples dynamic performance, but more than enough accelerant can induce a severe solidified reaction that result in a smaller polymeric meshwork and reducing the sample's performance. Normally the Accelerant dosage can be 2 portions; The Epoxy resin CFRP has a obvious better performances than the Vinyl-ester Resin CFRP, i.e. had a Bend Strength of 1516MPa, LSS of 85MPa, also Tg raised to 195~C~ When used the end-carboxyl polyether to reinforce the epoxy resin, the casing sample's SS, BS and Crack Elongation all increased geminately. The CFRP performance also increased a little, that is because the performance of the CFRP mainly contributed by the CF. The reinforced resin improved the interface between the CF and resin that contribute to the little increasing.

通过DSC分析确定了该环氧树脂的固化温度范围为110~200℃,促进剂增加会提高浇注体力学性能,但过多的促进剂会使固化反应剧烈,聚合网络减小,使浇注体性能下降,一般用量为2份左右;以环氧树脂为基体的复合材料性能明显比以乙烯基酯树脂的性能提高,弯曲强度达到1516MPa,层间剪切强度达到85MPa,同时Tg也上升到195℃;用端羧基聚醚增韧环氧树脂后,其浇注体的拉伸强度、弯曲强度及断裂伸长都成倍增加,复合材料的性能也有所提高,但提高幅度不大,因为复合材料的力学性能主要由碳纤维承担,树脂增韧后改善了复合材料的界面性能。

Transesterification of geranol and vinyl acetate in ionic liquids were investigated to synthesize geranyl acetate using immobilized Candida antarctica lipase B as biocatalyst. The reuse of ionic liquids and lipase were also studied in this reaction.

以固定化的南极假丝酵母脂肪酶为催化用酶催化香叶醇和乙酸乙烯酯在离子液体中的酯交换反应,合成了香料乙酸香叶酯,同时通过该反应了解了酶和离子液体的重复利用性。

Perchlorovinyl PVC resin can also be used in place of the biends or gype.

过氯乙烯树脂也可用聚氯乙烯树脂代替或二种共混使用。

Protection for sleeve, marking and sealing materials on capacitor body will not be damaged, which shouldnever be washed or cleaned by halogenous agents or solvents such as trichloroethylene. Xylene or acetone etc.

为了保护塑胶套管,印刷标示以及封口材料不被破坏,电解电容器不得以卤化化学药品或类似溶剂作为电解电容器洗涤之用,如三氯乙烯、二甲苯类或酮类等。

Protection for sleeve, marking and sealing material on capacitor body not to be damaged, capacitor body not to be damaged, capacitors should never be washed or cleaned by halogenous agents or solvents such as trichloroethene, Xylene or acetone etc.

为了保护塑胶套管印刷标示以及封口材料不被破坏,电解电容器不得以卤化化学药品或类似溶衯作为电解电容器洗濯之用,如三氯乙烯。本公司一般规格之电解电容器其品质依照 JIS C-5141W 标准。

BACKGROUND: Sponge paste made of polyvinyl alcohol polymer foam has biocompatibility, and properties of hemophagia, imbitition, and wound protection.

摘要背景:聚乙烯醇开孔型泡沫塑料具有生物相容性、吸血、吸液、保护伤口等特性,用其制成的聚氟乙烯海绵贴拟用于创伤止血材料。

A new functional electroluminescent copolymer is reported in which chromophores and hexa segments alternate along the polymer backbone.

采用Wittig反应合成了一种分子主链由烷氧基取代的1,4二苯乙烯基苯聚对亚苯基亚乙烯基(PPV的三个单元的齐聚物与柔性隔离链段五缩六乙二醇组成的交替型蓝绿色发光共聚物。

The molecular sieve is prepared in the steps: at the room temperature, hexadecyl trimethyl ammonium bromide is mixed and dissolved with the sodium hydroxide, and is added with TEOS in dropping way, and simultaneously added with Me metal salt water solution and lanthanum nitrate solution in dropping way; the pH value of the mixed solution is adjusted by acetic acid to be 10 to 11, and is mixed for 1 to 2 hours after being stabilized; the sol is moved into a polyfluortetraethylene bottle to be heated and crystallized for 2 days in the oven at the temperature of 100 DEG C; after filtering, washing and drying for nights, and being calcined in a muffle at the temperature of 550 DEG C for 3 to 7 hours, the dual-metal-atom improved MCM-41 mesoporous molecular sieve is obtained.

该分子筛的制备为室温下,将十六烷基三甲基溴化铵和氢氧化钠混合溶解,搅拌并滴加入TEOS,同时滴加入Me金属盐水溶液和硝酸镧溶液并搅拌,用乙酸调节pH值至10~11,稳定后搅拌1~2小时,溶胶转入聚四氟乙烯瓶中在100℃下烘箱水热晶化2天,经过滤、洗涤、干燥过夜,马弗炉550℃焙烧3-7h,得双金属原子改性MCM-41介孔分子筛产品。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。