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乙氧基苯

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This article provided a new route to produce 4-dimethoxy phenethylamine. In basic condition, the product could be obtained through etherization, bromation, Grignard reaction, hydroxyethylation, esterification and Gabriel reaction with phenol as raw material, the overall yield is 45.0%.

提出了合成4-甲氧基苯乙胺的新方法,即在碱性条件下,苯酚首先与硫酸二甲酯反应,再选用高选择性的溴化剂溴化后,经格氏反应、羟乙基化反应和酯化反应,最后经Gabriel反应可以制备目标产物,反应总收率为45.0%。

Under the optimum condition, the maximum yield of more than 84% was obtained.

在最佳条件下,3-乙氧基-4-羟基苯乙醇酸的产率达84%以上。

With regard to the biological activities of paeonol and sodium paeonol sulfonate, we studied their inhibitory effects on phytopathogen and their activities of scavenging O2-and OH.

实验结果显示,丹皮酚磺酸钠的纯度为99.4804%,化学结构为2-甲氧基-4羟基-5-乙酰基苯磺酸钠。

Water,dimethicone,propylene glycol,glycerin,cyclomethicone,ppg-15 stearyl ether,sorbitan oleate,stearic acid,cetyl alcohol,glyceryl stearate,ethylhexyl methoxycinnamate,peg-100 stearate,panthenol,phenoxyethanol,phospholipids,triethanolamine,methylparaben,oenothera biennis oil,imidazolidinyl urea,carbomer,c12-13 alkyl lactate,glycyrrhetinic acid,citrus aurantium dulcisoil,propylparaben,tocopheryl acetate,benzophenone-3,triclosan,disodium edta,ethylparaben,pentadecalactone,iris germanica root extract,retinyl palmitate,bisabolol,butylparaben,sodium hyaluronate,aesculus hippocastanumseed extract,ruscus aculeatus root extract,chlorhexidine digluconate,biosaccharide gum-1,citrus aurantium amaraoil,tocopherol,lecithin,ascorbyl palmitate,glyceryl oleate,BHT,citric acid,limonene,linalool

水, 地美司康,丙二醇,甘油,环甲硅脂, PPG-15 硬脂基醚,油酸己六酯,硬脂酸,十六醇,甘油硬脂酸, 4-甲氧基肉桂酸-2-乙基己基酯,聚乙二醇硬脂酸酯,维生素B5,苯氧乙醇,磷脂质,三乙醇胺,羟苯甲酯,月见草油,尿素醛,卡波姆, c12-13烷醇乳酸酯,甘草亭酸,甜橙油,羟苯丙酯,醋酸盐维他命E,二苯酮-3,玉洁新,乙酸乙二胺二钠,羟苯乙酯,环十五内酯,鸢尾花根萃取,维他命A酯,没药醇,羟苯丁酯,透明质酸钠,欧洲七叶树籽萃取,假叶树根萃取,洗必泰葡萄糖酸盐,多醣物质,苦橙油,维生素E,卵燐脂,抗坏血酸棕榈酸酯,甘油油酸酯,二丁基羟基甲苯,柠檬酸,柠檬精油,芳樟醇水:几乎所有护肤品成分第一位都是水。地美司康:即silicon,矽灵,一般添加于霜剂中,使用后皮肤手感光滑。该成分不可吸收。

Aniline compounds are used as raw material and reacted with anthranilic acid and then phenyl iodide as alkylating agents to give alkylating products followed by cyclizing with concentrated sulphuric acid to give a N-phenyl-acridone(or 3-ethoxyl-N-phenylacridone).The structure of intermediate and target compound are determined by IR and MS.

以苯胺类化合物为原料,先后以邻氯苯甲酸和碘苯为烷基化试剂进行了N 烷基化反应,再用浓硫酸使其环化制得N-苯基吖啶酮和3-乙氧基-N-苯基吖啶酮,并用红外光谱及质谱仪检测了各中间体及目标产物的结构。

Based on the synthesis method and the function of decreasing blood glucose levels of rosiglitazone, and the report on benzoquinones which resulted in a significant decrease in blood glucose levels, a novel non-thiazolidinedione class of PPARy agonist 2, 5-Dihydroxy-3-{4-[2-(methyl- pyridin-2- yl-amino)- ethoxy] -phenyl}-6-phenyl-[l, 4] benzoquinone (4) was designed and synthesized.

在合成罗格列酮的基础上,根据某些醌类结构化合物的类似胰岛素作用,设计并合成了一种非噻唑烷二酮类PPARγ激动剂2,5-二羟基3-{4-[2-(甲基-2-吡啶氨基)-乙氧基]-苯基}-6-苯基-1,4苯醌(4)。

Water,caprylic/capric triglyceride,mineral oil,butylene glycol,stearic acid,acetylated lanolin,glycerin,ethylhexyl methoxycinnamate,dimethicone,polyisoprene,triethanolamine,cyclopentasiloxane,butyl methoxydibenzoylmethane,titanium dioxide,persea gratissima oil unsaponifiables,sodium DNA,borago officinalis seed oil,oenothera biennis oil,simmondsia chinensisseed oil,hydrolyzed RNA,tocopheryl acetate,urea,hydrolyzed extensin,retinyl palmitate,sodium hyaluronate,helianthus annuusseed oil,tocopherol,ascorbyl palmitate,ascorbic acid,lanolin alcohol,c12-20 acid peg-8 ester,cyclotetrasiloxane,glyceryl stearate,dimethiconol,ceteareth-20,carbomer,magnesium aluminum silicate,propylene glycol,peg-8,silica,BHT,citric acid,phenoxyethanol,methylparaben,butylparaben,ethylparaben,isobutylparaben,propylparaben,chlorhexidine digluconate

水,辛酸/癸酸三酸甘油酯,矿物油,丁二醇,硬脂酸,乙醯化羊毛脂,甘油,4-甲氧基肉桂酸-2-乙基己基酯,地美司康,聚异戊烯,三乙醇胺,环戊硅氧烷,丁基甲氧基二苯甲醯基甲烷,二氧化钛,酪梨油,DNA 钠盐,琉璃苣種子植物油,月见草油,荷荷巴籽油,水解RNA,醋酸盐维他命E,尿素,水解伸展蛋白,维他命A酯,透明质酸钠,葵花籽油,维生素E,抗坏血酸棕榈酸酯,维生素C衍生物,羊毛脂醇,C12-20 酸 PEG-8酯,环四硅氧烷,甘油硬脂酸,聚二甲基硅氧烷醇,鲸蜡硬脂醇醚-20,卡波姆,硅酸镁铝,丙二醇,聚乙二醇-8,二氧化硅,二丁基羟基甲苯,柠檬酸,苯氧乙醇,羟苯甲酯,羟苯丁酯,羟苯乙酯,羟苯甲酸异丁酯,羟苯丙酯,洗必泰葡萄糖酸盐

Alidase was prepared by coupling silica-gel spheres already carrying γ-aminopropyltriethoxy-silane with glutaraldehyde, and then with N-(p-aminophenyl) oxamic acid.

将γ氦丙基三乙氧基硅烷取代的微球硅胶先后与戊二醛,对氨基苯草氨酸结合,制成了一种新的吸附剂,用于唾液酸酶的亲和提纯。

One of these compounds, 2-diethyl- aminoethyl-5--(4-methoxybenzylidene) cyclo- pentanone hydrochloride (T81) possessed sig- nificant antiinflammatory and analgesic ac- tivity when administered orally.

Ⅲ类化合物完全无抗癌活性,对其中一个化合物2-二乙胺乙基-5--(4-甲氧基苯亚甲基)环戊酮盐酸盐(T81)试验结果表明,它经口给药时具有显著的抗炎、镇痛活性。

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料,经过一系列的酰基化,脱羧,还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤;其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤;还有一部分主要是阐述从以苯乙酮,盐酸氨基脲,苯肼,乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛,然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

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