乙氧基

The research aimed to optimize the optimum technology conditions of immobilizing bromelin with attapulgite modified by 3-aminopropyliriethoxysilane.

［目的］确定利用3-氨基丙基三乙氧基硅烷改性凹凸棒土（3-APTS-凹凸棒土）固定菠萝蛋白酶的最佳工艺条件。

In the aspects of research method, we took the method of preparing sol at first and then impregnating the wood to obtain ceramic-wood composite; this method made the wood use efficiently and increased the wood's weight gain percent. The ceramic-wood composite with performances of well decay resistance, dimensional stability, effloresce resistance and high strength was obtained by importing the cymene to the net of gel as the result of co-hydroxylation between MTES and TEOS. Making use of XPS ,we found that the apex of Si2p、O1s、C1s had evident chemical shift , which validated the existence of Si-O-C bonding.Key Words: Sol-gel, Ceramic-wood composite, Modified sol, Ecomaterials

在工艺方法上，采用先制备溶胶，然后浸注木材的工艺方法具有原料利用率高、提高增重率的优点；采用甲基三乙氧基硅烷和正硅酸乙酯共水解的方法，将甲基引入陶瓷化复合木材的凝胶内部，所制备的材料具有尺寸稳定性好、具有耐风化和耐腐朽性，强度高的特点；首次利用X射线光电子能谱，发现了Si2p、O1s和C1s谱峰发生了明显的化学位移，证实了Si－O－C键合作用的存在。

At lower temperature, the interaction between the Ir particles and the adsorbed ethoxyl species is not strong enough to abstract H atom from the nearby CH3 group, and thus acetaldehyde acts as the key intermediate. Acetaldehyde can decompose to methane and CO and/or convert to acetone through decarbonylation.

低温时Ir粒子与吸附的乙氧基的相互作用的强度不足以从-CH3基团中提取H原子，此时乙醛是关键的反应中间物，乙醛可以裂解生成甲烷和一氧化碳或脱羰基生成丙酮。

It was discovered that when ethyl nitrite was introduced to the surface of catalyst, Pd ethoxyl compound was formed and simultaneously the active site Pd was transferred to the surface of catalysts with the change from Pd〓 to Pd〓. Then lined-adsorbed CO inserted into Pd alkoxyl compound to form the carboethoxypalladium complex.

研究结果表明，在CO偶联反应过程中，亚硝酸乙酯在催化剂上吸附，生成钯乙氧基络合物，同时将催化剂表面上的活性中心氧化，由Pd〓→Pd〓，并向催化剂表面上迁移。

A new synthesizing route for ethyl-2-(p -ethoxyphenyl) propenoate preparation was proposed, in which, the ethyl-2-(p-ethoxyphenyl) propenoate was synthesized from phenetole via Friedel-Crafts reaction and Wittig G reaction.

设计了一条以苯乙醚为起始原料，经过Friedel-Crafts反应、WittigG反应合成2-对乙氧基苯基丙烯酸乙酯的新路线。

A sol containing SiO_2 particles was prepared by the base catalyzed hydrolysis and polycondensation of tetraethoxysilane through sol-gel process. A solution containing double-chain polymer of methyltriethoxysilane was also prepared under acid condition, as the introducer of water repellence.

通过溶胶-凝胶法，在碱性条件下水解缩聚正硅酸乙酯获得含有SiO2颗粒的溶胶；以甲基三乙氧基硅烷在酸性条件下水解缩聚获得双链聚合物溶液，作为疏水基团的引入剂。

METHODSThe compounds were prepared by using 2ethylpyridine, through the Whol Ziegler reaction, the Williamson reaction and aminolysis. The effects for ability of memory in mice were measured by swimming maze test.

方法］以2乙基吡啶为原料，经WholZiegler反应、Williamson反应及氨解反应得到2［1（2吡啶）乙氧基］乙酰4取代哌嗪，采用水迷宫法观察所合成的化合物对小鼠记忆力的影响。

Silicone ; hard coating ; silicone resin ; methyltriethoxy silicone ; tetraethoxy silicane ; transparent plastic

有机硅；硬质涂料；硅树脂；甲基三乙氧基硅烷；正硅酸乙酯；透明塑料

PK values of 3-ethoxy-N-desmethyldiazepam (3-EtO-NDZ) in ethanol and acetonitrile containing various concentrations of sulfuric acid, determined by spectrophotometry and spectropolarimetry, were found to be 3.4 and 0.63 respectively. Temperature dependent racemization of enantiomeric 3-EtO-NDZ in ethanol containing various acid concentrations was studied by monitoring changes of ellipticity at 365 nm as a function of time on a spectropolarimeter.

3-乙氧基－N去甲基安定（3-EtO-NDZ；diazepam=安定）在含不同硫酸浓度的乙醇和乙腈中的pK值用光谱法和旋光光谱法作了测定，其结果分别为3.4和0.63.3-EtO-NDZ之对映异构体在含各种不同酸浓度的乙醇中与温度相关的消旋过程，用旋光光谱仪选择其圆二色谱在365nm波长处强度的改变为时间函数的方法作了测定。

The main by-product s and their separation and recovery technologies were discussed for cyclohexanone gas-phase Beckmann rearrangement.

探讨环己酮肟气相Beckmann重排主要副产物及其分离回收方法，研究1-氮杂-2-乙氧基-1-环庚烯、1，3，4，5-四氧吖庚因-2-酮及其同分异十句体等副产物回收利用生成已内酰胺的方法。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。