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This article provided a new route to produce 4-dimethoxy phenethylamine. In basic condition, the product could be obtained through etherization, bromation, Grignard reaction, hydroxyethylation, esterification and Gabriel reaction with phenol as raw material, the overall yield is 45.0%.

提出了合成4-甲氧基苯乙胺的新方法,即在碱性条件下,苯酚首先与硫酸二甲酯反应,再选用高选择性的溴化剂溴化后,经格氏反应、羟乙基化反应和酯化反应,最后经Gabriel反应可以制备目标产物,反应总收率为45.0%。

In a system consisting of 20% PEG 400 and 12% magnesium sulfate, the partition coefficient of PGA was less than 0.01, PGA almost completely partitioned into the magnesium sulfate-rich bottom phase. Meanwhile, the partition coefficient of cephalexin was 6.7, the partition coefficients of phenylglycine methyl ester and 7-ADCA were 1.5 and 1.2, respectively.

通过考察头孢氨苄、苯甘氨酸甲酯和7-氨基脱乙酰氧基头孢烷酸(7-ADCA)在ATPS中的分配行为建立了一个含20%PEG 400和12%硫酸镁的ATPS,在此体系中头孢氨苄的分配系数为6.7,苯甘氨酸甲酯的分配系数为1.5,7-ADCA的分配系数为1.2,且青霉素酰化酶的分配系数小於0.01。

The synthesis of nalbuphine hydrochloride from thebaine as starting material was through following processes:oxidation,high-pressure hydrogenation,acetylation,removing methyl of 3-methoxy,hydrolysis,condensation,reduction and finial salification.

以蒂巴因为起始原料,经氧化、高压氢化、乙酰化、氰化、脱3-位甲氧基的甲基、水解、缩合、还原、成盐,合成了盐酸纳布啡,总收率达18。

The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.

报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物,邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证

Chapter four. Two glucosamide-based trisiloxane Gemini surfactants which were connected with the short carbon chain dialcohol diglycidyl ether spacer were synthesized and their properties were determined. These compounds were structurally characterized by their 1H and 13C NMR spectra and elemental analysis.

界面性能通过K12表面张力仪测定,在临界聚集浓度CAC为1一3、10一5时可以显著地降低水的表面张力值至约21 mN/m,比连接基为低碳链二缩水甘油醚的略低,其CAC值随着乙氧基数的增加而增加,其CAC值比相应的单体低1~2个数量级,而且有两个CAC值。

Pharmaceutical characteristics of dimethylamino ethyl(4-chlorophenylmethfoxy )acetate hydrochloridein rabbit was studied and several parameters at different timeand way of medicine administration were determined.

研究了4-氯代苯甲氧基乙酸二甲氨基乙酯盐酸盐在家兔体内的药代动力学,测定了不同时间不同给药方式家兔体内的血药浓度及动力学参数。

A promising candidate for that purpose is the novel LiMAx test maximal liver function capacity based on 13C-methacetin (MA kinetics, which was developed by Dr.

LiMAx检测法根据13C-乙酰替对甲氧基苯胺动力学判断最大肝功能储备能力,很可能是满足上述目标的备选方法。

One of these compounds, 2-diethyl- aminoethyl-5--(4-methoxybenzylidene) cyclo- pentanone hydrochloride (T81) possessed sig- nificant antiinflammatory and analgesic ac- tivity when administered orally.

Ⅲ类化合物完全无抗癌活性,对其中一个化合物2-二乙胺乙基-5--(4-甲氧基苯亚甲基)环戊酮盐酸盐(T81)试验结果表明,它经口给药时具有显著的抗炎、镇痛活性。

Rosolic acid reacted with acetic anhydride to synthesize rosolic acid -triacelate ester [tri(4-acetoxy) phenyl methane] under reflux condition.

以玫红酸、醋酸酐为原料,采用加热回流法合成了玫红酸三乙酸酯[三(4-乙酰氧基)苯基甲烷]。

The invention relates to a method for manufacturing polyesters, in particular, to using a lithium titanyl oxalate as the catalyst for such reaction to provide fast reactions with excellent color properties for the resulting polyester.

本发明涉及一种制备聚酯的方法,尤其涉及采用钛氧基乙二酸锂作为此类反应的催化剂以加快反应,并使所得聚酯具有优良的色泽性能。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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