乙氧基

With regard to the biological activities of paeonol and sodium paeonol sulfonate, we studied their inhibitory effects on phytopathogen and their activities of scavenging O2-and OH.

实验结果显示，丹皮酚磺酸钠的纯度为99.4804％，化学结构为2-甲氧基-4羟基-5-乙酰基苯磺酸钠。

Chapter 4 The unclassical products——1-substituted aryl-4-ethoxycarbonyl5-dimethylaminometheneamino-1, 2, 3-triazole were prepared under Vilsmier conditions, and the reaction mechanism was also studied.

第四章报道了在Vilsmier条件下非经典产物—1-取代芳基-4-乙氧羰基-5-二甲基氨基甲叉氨基-1，2，3-三唑的合成及反应的机理进行了讨论。

The first asymmetric synthesis of trans-β-hydroxy-γ-butyrolactones:-(3R, 4R, 5S)-4-(1-acetoxy-isopropyl)-3-hydroxy-butyrolactone 65a was achieved starting from isobutylaldehyde through nine steps. The key steps involve the construction of three chiral carbon centers by the Sharpless's asymmetric epoxidation and Substrate directable chemical reaction.

以异丁醛为起始原料，经过九步反应首次设计合成了具有三个手性中心的trans-β-羟基-γ-丁内酯：-（3R，4〓，5S）-4-（1-乙酰氧基-异丙基）-3-羟基-丁内酯65a，关键步骤是Sharpless不对称环氧化和底物定向不对称合成反应。

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e，7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟醚类氨基甲酸甲酯3a-e，进一步胺解之后得到了肟醚类氨基甲酰甲胺3f-j。

Deoxybenzoin(3) was prepareded by using the resorcinol and substituted phenylacetic as starting meterials in microwave-mediated.Then the compound(3) was reacted with acetic anhydride to produce(4).The compound(4) was hydrolyzed to convert compound(5) in the acid-mediated. The compound(5) was reacted with the 1,2-dibromo-ethane and 1,3-dibromo-propane in refluxed condition with acetone as solvent to give(6) or(7),respectively.Lastly,the title compounds were synthesized by refluxing(6) or(7) with 2-methyl-benzimidazole and potassium carbonate in acetone solution.

以取代苯乙酸和间苯二酚为起始原料，用微波辐射法合成脱氧安息香(3)，(3)与乙酸酐缩合生成2-甲基-7-乙酰氧基异黄酮(4)，(4)在酸性条件下水解生成相应的异黄酮(5)，化合物(5)分别与1，2-二溴乙烷和1，3-二溴丙烷反应生成(6)和(7)，化合物(6)和(7)再分别与2-甲基苯并咪唑偶合生成目标化合物。

Results Six compounds were isolated and identified as:5α,8α-epidioxy-(22E,24R)-ergosta-6,22-dien-3β-ol,scopoletin,isofraxidin,p-hydroxy benzaldehyde,3,4,5-trimethoxy benzoic acid,protocatechuic acid ethyl ester...

结果得到6个化合物，分别鉴定为：5α，8α表二氧(22E，24R)麦角甾6，22二烯3β醇、东莨菪素、异秦皮啶、对羟基苯甲醛、3，4，5三甲氧基苯甲酸、原儿茶酸乙酯。结论化合物Ⅰ～Ⅵ均为首次从该属植物中分离得到。

The cis-decalin 79 was obtained from 2-methoxy-4-methylphenol (77) via a sequence of reactions involving intermolecular Diels-Alder reaction of masked o-benzoquinone derived from 77 and ethyl vinyl ketone, silyl enol ether formation and Cope rearrangement.

第一部份：以2-甲氧基-4-甲基酚(77)为起始物，经由二乙醯基亚碘苯氧化、分子间Diels-Alder反应、烯醇矽醚的形成及Cope重排反应得到具有十氢萘骨架化合物79。

Main products are Perfluorosulfonated acid resin, PFSA aqueous dispersion, and on the basic of them, HFPO,TFE sultone,PSVE,PPVE,MTPME etc fluorinated fine chemicals,and FEP,FKM,PVDF etc fluorpolymers.

公司主导产品有全氟磺酸离子交换树脂、全氟磺酸离子交换树脂溶液，同时以此为依托，配套生产六氟环氧丙烷、四氟磺内酯、PSVE、PPVE、甲氧基四氟丙酸甲酯等含氟精细化学品，聚全氟乙丙烯树脂（FEP，F46）及分散液、氟橡胶、聚偏氟乙烯等含氟高分子材料。

Compounds were identified by NMR etc, and they are veraflorizine 1, ebeinone 2, verticinone 3, isoverticine 4, trilinolein 5, phenanthrene 6, 2,5-dimethoxy-1,4-benzoquinone 7, tetradecane 8. All of them were isolated from this plant for the first time.

从安徽舒城县产舒城贝母的干燥鳞茎中分离得到了14个单体化合物，应用核磁共振等手段鉴定了8个化合物的结构，其中4个化合物为异甾体生物碱，4个为非生物碱，分别为：veraflorizine 1、鄂贝乙素2、浙贝乙素3、异浙贝甲素4、三亚麻油酸甘油酯5、菲6、2，5—二甲氧基苯醌(2，5-dimethoxy-1，4-benzoquinone)7和正十四烷8，这些化合物均为首次从该植物中分离得到。

Mercaptopropyl methyldimethoxysilane was synthesized by thiourea in the presence of tetramethylammonium iodine as a catalyst and mixed liquid containing ethylenediamine and trichloroethylene as a neutralizer, without solvent, in which the reaction temperature, catalysts ,neutralizer and their amounts were optimized.

以四甲基碘化铵为催化剂，乙二胺和三氯乙烯的复合液为中和剂，在无溶剂体系中，用硫脲法合成了甲基巯丙基二甲氧基硅烷。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。