乙氧基

Dihydroxy-7, 4′-dimethoxy-dihydrflavonol and -3, 5, 7 -trihydroxy-4′-methoxy- dihydrflavonol were synthesized by selective protection, condensation, epoxidation, cyclization and deprotection from 2, 4, 6-trihydroxyacetophone and anisaldehyde.

以2，4，6-三羟基苯乙酮和茴香醛为起始原料，经选择性保护、缩合、环氧化、关环等步骤首次完成了-3，5-二羟基-7，4′-二甲氧基二氢黄酮醇和-3，5，7-三羟基-4′-甲氧基二氢黄酮醇全合成。

In this thesis, a convenient and efficient synthesis of highly functionalizeddihydropyrido[2,3-d]pyrimidines via a double [5 + 1] annulation strategy startingfrom easily available α-alkenoyl-α-carbamoyl ketene--acetals 1 and cheapreagents (NH4OAc, DMF, and POCl3) has been developed.

本论文探索了一种简便有效的合成高度官能化的二氢吡啶并[2，3-d]嘧啶的方法，此方法由易得的α-乙酰基-α-氨基乙酰基二硫缩烯酮1和便宜的试剂(醋酸铵，二甲基甲酰胺和三氯氧磷)通过两步[5 + 1]加成而实现。

The intermediate of flazasulfuron weedicide ,2-amino-4,6-dimethoxypyrimidineis conveniently obtained by treating 2-amino-4,6-dihydroxypyrimidinewith diazomethane at 20 °C for 24h.

本文利用硝酸胍和丙二酸二乙酯为起始原料，经环合及甲氧基化两步反应得到除草剂啶嘧磺隆的中间体：2-氨基-4，6-二甲氧基嘧啶。

Thirty patients (M 23, F 7; age 50 a±s 15 a) with chronic eczema were treated with etofesalamide ointment (given th inly on the surface 3 times daily) for 4 wk; Another 30 patients (M 24, F 6; age 44 a±14 a) were treated with ointment base (given thinly on the surface 3 tim es daily) for 4 wk.

60例慢性湿疹病人，30例(男性23例，女性7例；年龄50 a±s 15 a)用乙氧苯柳胺软膏均匀涂布患处，tid， 4 wk为一个疗程；另30例(男性24例，女性6例，年龄44 a±14 a)采用乙氧苯柳胺软膏基质均匀涂敷患处，tid， 4 wk为一个疗程。

The main products are: phosphorous trichloride 300,000 tons / year, phosphorus oxychloride 100,000 tons / year, phosphorus pentachloride 50,000 tons / year, 10,000 tons trichloroisocyanuric parathion / year chloromethyl ether 5000 tons / year, triethyl phosphite 10,000 tons / year, triphenyl phosphite 5000 tons / year, three phosphoric acid ethyl butoxy 2000 tons / year.

主要产品有：三氯化磷30万吨/年、三氯氧磷10万吨/年、五氯化磷5万吨/年、三氯硫磷1万吨/年、氯甲基甲醚5000吨/年、磷酸三乙酯10000吨/年、磷酸三苯酯5000吨/年、磷酸三丁氧基乙酯2000吨/年。

He first synthesis of the precursor 45b of Tuxpanolide was accomplished fromβ-alkoxy aldehyde and β-acetoxy-γ-butyrolactone by the Aldol reaction.

uxpanolide的合成前体45b的首次不对称合成：以β-烷氧基开链醛和β-乙酰氧基-γ-丁内酯参与的Aldol醛醇缩合反应首次得到了前体化合物45b。

Ib was synthesized by condensation of phthalic anhydride with 2-methylresorcinol in fused AlCl〓/NaCl (5∶1), followed by selective acetylation, methylation, NBS bromination and condensation with sodium ethoxide.

邻苯二甲酸酐在熔融的三氯化铝-氯化钠(5：1)中和-2，6-二羟基甲苯环合得1，3-二羟基-2-甲基蒽醌〓后经选择性乙酰化、甲基化、NBS溴化、乙醇钠缩合得1-甲氧基-2-乙氧甲基-3-羟基蒽醌。

NOBS PAG , can obviously activate hydrogen peroxide thus , the efficiency of hydrogen peroxide bleaching can be advanced greatly .

研究结果初步表明，此类有机酰化剂类如：四乙酰乙二胺，四乙酰甘脲，异壬酰氧基苯磺酸钠，五乙酰葡萄糖等有着非常明显的活化过氧化氢的作用，从而能在很大程度上提高纸浆过氧化氢漂白的效率。

Five chalcones were synthesized via the aldol condensation reaction of acetophenone or parasubstituted acetophenones with 1-phenyl-3-methyl-5-phenoxyl-pyrazol-4-aldehyde, which reacted with two kinds of hydrazine in glacial acetic acid under refluxing to give a series of bipyrazoline derivatives. In this synthetic course, glacial acetic acid is not only a solvent, but also a catalyzer.

以1-苯基－3-甲基－5-苯氧基－吡唑-4-甲醛为原料，与苯乙酮发生羟醛缩合，生成相应的查尔酮，再在冰醋酸中与不同的肼反应，高产率的合成出10种新的5位含1-苯基－3-甲基－5-苯氧基－吡唑基的吡唑啉类衍生物。

In chapter four, molecular imprinting polymers against amino acid derivatives utilizing 2-VP+AM as combined functional monomer and trimethylolpropane trimethacrylate as tribasic cross-linker were prepared and result was compared with those with the same amino acid derivative as the imprinted molecules utilizing ethyleneglycol dimethacrylate as dibasic cross-linker. It was found that cross-link intensity of the molecular imprinting polymer is higher when TRIM was utilized and baseline separation for the imprinted molecule could be achieved. When TRIM was utilized as cross-linker more molecule is imprinted during the polymerization.

第四章采用2-乙烯基吡啶+丙烯酰胺复合功能单体，考察了三元交联剂三甲氧基丙烷三甲基丙烯酸酯烙印氨基酸衍生物的情况，并与二元交联剂乙二醇二甲基丙烯酸酯烙印相同氨基酸衍生物的情况进行了对比，发现三甲氧基丙烷三甲基丙烯酸酯交联剂在较小的用量下就可使分子烙印聚合物达到足够的交联度，实现烙印分子的基线分离。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。