乙基氰

The diazotization condition of 4-methyl-1-ethyl-3-cyano-5amino-6-hydroxy-2-pyridone and coupling condition of its diazo salt were researched, and the structure of its diazo salt was confirmed.

研究了4-甲基-1-乙基-3-氰基-5-氨基-6-羟基-2-吡啶酮的重氮化反应及其重氮盐发生偶合反应的条件，确定了重氮盐的结构。

Effect of heat treatment on the ndcrophase separation of a segmented poly copolymer based on poly diol, 3, 5 dithyltoluene diandne and 4,4'-diphenylmethane diisocyanate has been studied bymeans of fourier transform infrared spectroscopy.

用傅里叶变换红外光谱方法研究了热处理对由聚环氧丙烷聚醚多元醇、3.5－二乙基甲苯二胺和4，4－二苯基甲烷二异氰酸酯组成的多嵌段聚氨酯脲的微相分离行为的影响。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent.

方法采用溴化氰活化多糖，以无水己二酸二肼为连接剂，1-乙基-1-3-(3-二甲基氨基-丙基)-碳化二亚胺为偶联剂，制备结合物并免疫小鼠，检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent. Immunize mice with the conjugates and determine the antibodies against GAMP and carrier proteins in their sera as well as the bactericidal activity of antibody against GAMP.

采用溴化氰活化多糖，以无水己二酸二肼为连接剂，1-乙基－1-3-（3-二甲基氨基－丙基）－碳化二亚胺为偶联剂，制备结合物并免疫小鼠，检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

Benzyl isothiocyanate and phenethyl isothiocyanate induced apoptosis of DU-145 cells which also were confirmed by DAPI staining and DNA gel electrophoresis.

除此之外，苯甲基异硫氰酸酯和苯乙基异硫氰酸酯也会造成人类前列腺癌细胞株DU-145粒线体膜电位的改变，活性氧化物质和钙离子的释放以及造成DNA的损伤。

Western blotting show that benzyl isothiocyanate and phenethyl isothiocyanate treatment gradually decreased the level of anti-apoptotic proteins, but increased the level of pro-apoptotic proteins.

接著，由西方点墨法的结果发现苯甲基异硫氰酸酯和苯乙基异硫氰酸酯会造成人类前列腺癌细胞株DU-145凋亡蛋白的增加和Caspase活性的上升。

Besides, benzyl isothiocyanate and phenethyl isothiocyanate also decreased the levels of mitochondria membrane potential, induced reactive oxygen species and calcium ion production in examined DU-145 cells.

由结果显示，苯甲基异硫氰酸酯和苯乙基异硫氰酸酯确实会造成人类前列腺癌细胞株DU-145细胞周期停滞以及诱导细胞凋亡的产生。

Besides, benzyl isothiocyanate and phenethyl isothiocyanate increased caspase-3 activity. Therefore, benzyl isothiocyanate and phenethyl isothiocyanate induce apoptosis in human prostate cancer DU-145 cells.

由此可知，苯甲基异硫氰酸酯和苯乙基异硫氰酸酯会造成人类前列腺癌细胞株DU-145走向凋亡的命运，值得更进一步研究发展为抗癌药物。

The volatile components were separated and identified using GC-MS technique. RESULTS Seven ingredients were. isolated: 2-ethyl-hexyl-adipate (66.5%), 1-methoxy-4-(1-propenyl)benzene (12.5%), isopropyl isothiocyanate (6%), isobutylisothiocyanate (6%), 6-methyl-5-heptene-2-one (3.5%), benzaldehyde (1.4%), phenylacetaldehyde (0.8%).

结果 分离出7个成分，采用峰面积归一化法确定了各成分的相对含量，分别为66.5%双－2-乙基己基－己二酸、12.5%1-甲氧基－4-（1-丙烯基）苯、6%异硫氰酸异丙酯6%、6%异硫氰酸异丁酯、3.5%6-甲基－5-庚烯－2-酮、1.4%苯甲醛、0.8%苯乙醛。

The invention relates to a pipeline polyurea outer anticorrosive coating and the making method thereof, making heated prepolymerization reaction on dibenzo-methane diisocyanate, carbodiimide diisocyanate, polyether binary alcohol and polyether trihydric alcohol to prepare prepolymer solution A, and making end amino polyethylene oxide ether, dimethyl sulfur-based toluene diamine, diethyl diamine, iso-propyl titanate solution, polyacrylate, carbon black, titanium dioxide and lightweight calcium carbonate into solution B, and as using, respectively heating the solutions A and B to 65 deg.C and then mixing them, then quickly spraying and curing to form a coat.

本发明涉及一种管道用聚脲外防腐涂料及制造方法，由二苯基甲烷二异氰酸酯、碳化二亚胺化二异氰酸酯、聚醚二元醇和聚醚三元醇通过加热预聚反应制成预聚物的A液、由端氨基聚氧化乙烯醚、二甲硫基甲苯二胺、二乙基甲苯二胺、钛酸异丙酯溶液、聚丙烯酸酯溶液、碳黑、钛白粉和轻质碳酸钙配制而成的B液组成，使用时将A液和B液分别加热至65℃后混合，然后快速喷涂固化形成涂层。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。