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乙基氯

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Through condensing o-aminobenzoic acid, ethyl oxalyl chloride and ethylenediamine(or 1,2-propylenediamine), two new ligands N-benzoato-N′-(2- aminoethyl)oxamido(H3oxbe) and N-benzoato-N-(2-amino-2-methylethyl)oxamido(H3oxbt) have been synthesized. Their mononuclear complexes Na·1.5H2O and Na·1.5H2O have also been obtained.

2以邻氨基苯甲酸、草酸乙酯酰氯和乙二胺(或1,2-丙二胺)缩合制得了两种具有不对称草酰胺结构配体N-(2-苯甲酰基)-N&-(2-氨乙基)草酰胺(H3oxbe)和N-(2-苯甲酰基)-N&-(2-氨丙基)草酰胺(H3oxbt),并得到了它们的单核配合物:Na·1.5H2O和Na·1.5H2O。

Potassium phthalimide reacted with 2-chloroethanol under 90?℃ or 12?h in DMF solvent, and the isolation yield was about 86%.

以DMF为溶剂,邻苯二甲酰亚胺钾盐与氯乙醇在90℃下反应12h,N (2 羟乙基)邻苯二甲酰亚胺的收率为86%。

In order to find new pyrazole leading compounds, 14 1--4-(pyrazol- 5-ylcarbony)semicarbazide devivatives were synthesized from 4-chloro-3-ethyl-1-methyl-5-pyrazole car-bonydrazide and substituted phenylisocyanate.

为了寻求新的吡唑先导化合物,用4-氯-1-甲基-3-乙基-5-吡唑甲酰肼与取代苯基异氰酸酯反应得到了14个新的1-吡唑酰基-4-芳基氨基脲类化合物。

Two novel pyrazolone derivatives 2-ethylamino-6H-5-(1-phenyl-3-methyl/phenyl-5-pyrazolone-4-ylene)-1,3,4-thiadiazine (PMCP-ETSC/DPCP-ETSC) containing NNS six-membered heterocycles were synthesized by the condensation reaction of 1-phenyl-3-methyl/phenyl-4-chloroacetyl-pyrazolone-5 with 4-ethyithiosemicarbazide. The title compounds were characterized by elemental analysis, IR, 1H NMR, 13C NMR and single-crystal X-ray diffraction.

利用1-苯基-3-甲基/苯基-4-氯乙酰基-吡唑啉酮-5与4-乙基氨基硫脲发生缩合反应,生成了2个新的双杂环化合物2-乙氨基-6H-5-(1-苯基-3-甲基/苯基-5-吡唑啉酮-4-基)-1,3,4-噻二嗪(PMCP-ETSC/DPCP-ETSC),并对其进行元素分析、红外光谱、核磁共振表征和晶体结构分析。

Were detected for okadaic acid by high performance liquid chromatography with 9chloromethylanthracene (9CA) and tetramethylammonium hydroxide.

在江苏及浙江共5个地点采集了8种贝类,使用四甲基氢氧化胺和9-氯乙基蒽衍生的高效液相色谱法,检测样品的大田软海绵酸含量。

Alternatively, the chlorine-containing compound may comprise a compound selected from the group consisting of ammonium chloride, methyl ammonium chloride, tetramethylammonium chloride, tetraethylammonium chloride, and combinations thereof.

或者,所述含氯化合物可包括选自氯化铵、氯化甲基铵、氯化四甲基铵、氯化四乙基铵和它们的组合的化合物。

Two azobenzene-containing polyethers were synthesized and their thermotropic liquid crystalline properties were investigated.

氯乙基缩水甘油醚和GCE/羟丁基乙烯基醚分别通过阳离子聚合、光引发共聚合,获得两种聚醚,然后再分别与 4-硝基-4' -羟基偶氮苯反应,制备了两种侧链含偶氮苯生色团的液晶聚合物。

This research uses the triethyl phenmethyl ammonium chloride to make the catalyst, take double phenol A, the epichlorohydrine, the sodium hydroxide as raw material, to affected factors and so on effect allocated proportion, temperature, reaction time to conduct the full research.

本研究采用三乙基苄基氯化铵作催化剂,以双酚A、环氧氯丙烷、氢氧化钠为原料,对影响效果的配比、温度、反应时间等因素进行了充分的研究。

Compounds, N - methylene chloride acetyl groups - 2 - methyl - 2,5 - diethyl arene pbo.

化合物Ⅱ:N-二氯乙酰基-2-甲基-2,5-二乙基-1,3-恶唑烷。

Dichloro-3-ethyl-6-nitrophenol is an important intermediate for color film developer.

2,4 二氯 3 乙基 6 硝基苯酚是一种重要的有机合成中间体,广泛应用于照相显影剂的制备等。

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By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候,里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色,卵在发育96h后卵基本全部孵化。

There was a conflict between plebs and patricians in ancient Rome in 494BC.

在公元前494年,罗马发生了一次平民反对贵族的斗争。