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Chapter 4 The unclassical products——1-substituted aryl-4-ethoxycarbonyl5-dimethylaminometheneamino-1, 2, 3-triazole were prepared under Vilsmier conditions, and the reaction mechanism was also studied.

第四章报道了在Vilsmier条件下非经典产物—1-取代芳基-4-乙氧羰基-5-二甲基氨基甲叉氨基-1,2,3-三唑的合成及反应的机理进行了讨论。

Result: Eight compounds were isolated from ethanolic extract of the brown alga D.divaricata and their structures were identified as-torreyol,4β,5α-dihydroxycubenol,3-farnesyl-p-hydroxybenzioc acid,chromazonarol,fucosterol,phenyl acetylamine,4-hydroxybenzoic acid and n-hexadecanoic acid.

结果:从叉开网翼藻中分离得到8个化合物,分别鉴定为-torreyol,4β,5-αdihydroxycubenol,3-farnesyl--phydroxybenzioc acid,chromazonarol,岩藻甾醇,苯乙酰胺,4-羟基苯甲酸和正十六酸。

Ultrasound, Expansive Graphite, Cinnamic Acid, Ethyl Alkylidene a- Cyanoacetate, Montmorillonite, Pinacol

超声波,膨胀石墨,肉桂酸,烷叉基氰乙酸乙酯,蒙脱土,片呐醇

Chondrus ocellatus was extracted by methanol, ethanol, ethyl ether, ethyl acetate, petroleum ether and acetone, respectively.

采用甲醇、乙醇、乙醚、乙酸乙酯、石油醚、丙酮6种溶剂分别对角叉菜进行冷浸提取。

Then the protected D-mannitol, mixed with lead tetraacetate, hippuric and acetic anhydride, were refluxed in THF for 18 h in a one-pot two step reaction to afford a chiral precursor-2-phenyl-4-[-2,3-O-]-propylidene-5(4H)-oxazolones.

产物与四乙酸铅、马尿酸、乙酐于THF中回流18 h完成一釜二步反应,纯化后得到含有手性碳原子的环丙烷氨基酸前体-2 苯基-4-[-2,3-O-]丙叉?

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By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候,里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色,卵在发育96h后卵基本全部孵化。

There was a conflict between plebs and patricians in ancient Rome in 494BC.

在公元前494年,罗马发生了一次平民反对贵族的斗争。