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乙交酯

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Meanwhile the influence of the amount of catalyst alkali ethylate and absolute alcohol,the temperature and time of reaction on interesterification was studied.

利用正交试验研究了酯交换法制备卤虾油脂肪酸乙酯的工艺,分析了催化剂用量、反应温度、反应时间、无水乙醇用量等对醇解率的影响。

A series of UV-cured AB crosslinked polymers based on vinyl-terminated polyethylene adipate polyurethane and methyl methacrylate were prepared.

用紫外光聚合方法制备出一系列端乙烯基聚己二酸乙二醇酯聚氨酯和甲基丙烯酸甲酯AB交联聚合物。

The title anti-fogging coating was prepared from film-forming substance such as UV curing of n-butyl methacrylate,β-hydroxy ethyl acrylate,acrylamide and sodium propenyl alkyl ether hydroxyl sulfonate,and proper solvents, crosslinker s,photoinitiators and additives.

以光敏丙烯酸酯低聚物、甲基丙烯酸丁酯、丙烯酸-β-羟乙酯、丙烯酰胺及丙烯基烷醚羟磺酸钠为主要成膜物质,再配以适量的溶剂、交联剂、光敏剂及各种助剂制成UV固化防雾涂料。

This paper deals with making stop bleeding sponge with dried small shrimps. Firstly breaking away with inorganic salt and proteir in the dried small shrimps with acid and NaOH, secondly, taking off vinyl-in the chitin with 50% NaOH, temperature is 110 ℃. the last, reacting with chitosamine and PVA-124 make stop bleeding sponge were produced, catalyst is PdCl 2. The sponge film and sparkce is setatisfaction.

用虾壳经除盐,去蛋白处理后,用50%的NaOH溶液在110℃的温度下脱乙酰基制备壳聚糖;以1∶9的稀醋酸溶作溶剂,氯化钯作催化剂,甲苯二异氰酸酯作发泡剂、交联剂,使壳聚糖与PVA-124进行交联成膜,发泡用氨水洗成中性后在80℃的红外灯烘箱下烘干,制得止血海棉

The title nano-sized polymeric microgels were synthesized by emulsion polymerization method,using divinyl benzene as crosslinking agent and methyl methacrylate,hydroxyl ethyl methacrylate,butyl acrylate as monomers.

通过乳液聚合的方法,以二乙烯基苯为交联剂,用甲基丙烯酸甲酯、甲基丙烯酸-β-羟乙酯、丙烯酸丁酯等丙烯酸酯类单体合成纳米尺寸的聚合物微凝胶粒子。

A fully ethoxy-terminated polymethylsilsesquioxane has been prepared via a dehydration ethanolysis reaction between absolute ethanol and an ordered ladder-like HO-Me-T, which improved long-term storage stability of HO-Me-T. Meanwhile, EtO-Me-T can still participate in the cross-linking reaction with hydroxy-terminated PDMS in the presence of catalyst.

利用含端羟基的LPS与无水乙醇之间的催化脱水反应合成了一种乙氧基为末端基团的活性梯形聚甲基倍半硅氧烷,有效地改善该类聚合物的长期稳定性;同时,该乙氧基封端聚合物仍然具有活性,可以代替常用的正硅酸乙酯与羟基硅油进行交联反应。

In the polymerization procedure,S--α-phenyl ethylamine was used as target template molecules,methacrylic acid was selected as functional monomers, ethylene glycol dimethacrylate or divinylbenzene as crosslinker, azobisisobutyronitrile or benzophenone was used as irritator.

以S--α-苯乙胺为模板,甲基丙烯酸为功能单体,分别以二甲基丙烯酸乙二醇酯、二乙烯基苯为交联剂,偶氮二异丁睛或二苯甲酮为引发剂,采用了本体聚合法、悬浮聚合法合成了一系列的S--α-苯乙胺印迹聚合物。

With the increase in CO(NH2)2 concentration,the molecular weight significantly increased,and the best concentration scope of DMAEMA was 0.06%-0.10%.Inaddition,the agents for preventing cross-linking were used to prevent the cross-linking reaction and it content was not allowed too high,and the best concentration scope of sodium acetate(the regulator of molecula weight)was

在此中和度下,AMPS的适宜用量范围为AM的75%~16.25%;AA的适宜用量范围44%~55%;(NH4)2S2O8的适宜用量范围为AM/AA/AMPS总量的0.07%~0.12%;分子量随CO(NH2)2的增加而明显升高;甲基丙烯酸N,N-二甲氨基乙酯的适宜用量范围为0.06 %~0.10%;使用抗交联剂可以解决产品交联造成的难溶问题,但加入量不宜过多,否则分子量会下降;分子量调节剂醋酸钠的用量在1.24 %~1.54%范围内可以使产品的分子量达最佳值。

A micro-monolithic column was prepared by in-situ free radical polymerization of stearyl methacrylate with ethylene glycol dimethacrylate in the presence of the initiator AIBN and a mixture of porogens including iso-amyl alcohol and 1,4-butanediol.

以甲基丙烯酸碳酰十八酯为单体,乙叉二甲基丙烯酸酯为交联剂,异戊醇和1,4-丁二醇为二元致孔剂,偶氮二异丁腈为引发剂,原位制备了具有强疏水性的SMA整体微柱,并利用此整体微柱在普通高效液相色谱仪上测定滴眼液中氧氟沙星的含量。

In this research, liposoluble chlorogenic laurate was synthesized by the acylation with lauroy chloride in the existence of alkali catalyst in non-water phase, and yellowish CGL powders with a yield of 81.24% were obtained under the optimal synthesis conditions determined via single-factor tests and orthogonal experiments, that is, carrying out the acylation at 35℃ for 8h with a n:n: n ratio of 1:1:1.5 and with dimethylformamide as the solvating agent and the thinner.

文中对绿原酸进行了改性,即在碱性催化剂催化的条件下使其与月桂酰氯进行非水相的酯化反应,得到了脂溶性的绿原酸月桂酸酯。经过单因素及正交试验,确定了最佳合成条件为:以N,N-二甲基甲酰胺作为溶解、稀释剂,绿原酸/月桂酰氯/三乙胺的摩尔比为1:1:1.5,温度控制在35℃,反应时间8h。

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