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乙二醇

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When methoxyethanol was used as the solvent,tantalum ethoxide can be chemically modified with acetic acid to producetantalum alkxo-acylate precursor, and therefore the hydrolysis of 〓can be slowed down.

在以乙二醇单甲醚为溶剂时,乙醇钽与醋酸作用生成乙醇钽的乙酰基配位化合物,可以减弱水解反应的进行。

The volume ratio of furaldehyde to acetic anhydride is 1∶2; the mole ratio of furaldehyde with anhydrous potassium carbonate is 1.00∶0.54. The best phase transfer catalyst is PEG1000, the mass ratio of PEG1000 with furaldehyde is 4.3%, the reaction time is 11 min, the reaction power of microwave is 260 W. The yield ofα-furanacrylicacid is up to 72.3% under these reaction conditions.

研究结果表明:在微波辐射功率为260 W、微波反应时间为11 min、以聚乙二醇1 000(PEG1000)为相转移催化剂,糠醛与乙酐的体积比为1∶2,糠醛与无水碳酸钾的量比为1.00∶0.55时,α-呋喃丙烯酸的产率为72.3%。

In order to enhance the compatibility of ABS/PP/CaCO3 composites, the effects of reactive blends of the composites were studied by using Haake rheometer. The effects of various assistant cross-linkingers, such as castor oil, triallyl isocyanurate, turpentine (JS-1) and glycol dimethacrylate, and the used amount of cross-linkinger-dicumyl peroxide on the torques of the melting composites were investigated.

为提高ABS/PP/CaCO3复合材料相容性,采用转矩流变仪观察了ABS/PP/CaCO3三元复合物反应性共混后的扭矩,考察了不同的助交联剂蓖麻油、异氰脲酸三烯丙酯、松香酯(JS-1)、二甲基丙烯酸乙二醇酯以及交联剂过氧化二异丙苯的用量对共混物的影响。

The condensation reaction of levulinates with ethylene glycol brings about corresponding ketal , with respective productivity of 74%, 75% and 75%, and respective structure being verified by IRS.

由乙酰丙酸酯类化合物与乙二醇进行缩合反应,得到相应的环状缩酮化合物,产率分别为 74 %,75 %和 75 ,其结构为红外光谱所证

In this dissertation, polyethylene glycol monomethyl ether of 2000 molecular weight as soluble support, an array of soluble polymer-supported tartrate esters were designed, synthesized, and applied in asymmetric epoxidation of allylic alcohols.

本论文以平均分子量为2000的聚乙二醇单甲醚为可溶性支载体设计和合成了一系列可溶性聚合物支载的酒石酸酯配体,并将它们用于烯丙基醇的不对称环氧化反应。

Nonion surfactants 1dodecanol polyethylene oxider 23 (Brij-35), polyethylene glycol-6000 (PEG-6000) made nickel deposit became dentrite.

非离子表面活性剂月桂醇聚氧乙烯23醚Brij 35)、聚乙二醇-6000(PEG-6000使镀层由无添加剂时的粒晶变成了枝晶。

Thus, in order to attain acetal can be used as precursor of its matrix olefine aldehyde, 2-undecental glycol acetal was synthesized, and the corresponding optimum reaction conditions as: 2-undecental 0.2mol, glycol 0.3mol, cyclohexane as solvent, catalysed by vitamin C, the optium reaction time was 6h, its reaction yield could reach over 77.25%.

为了进一步探求效果更理想的前体化合物,本文继续合成了2-十一烯醛乙二醇缩醛,通过单因素优化实验得到最佳反应条件为:环己烷作溶剂,VC作催化剂,用量0.42%,醛醇物质的量之比0.2:0.3,反应时间6h,此条件下产品收率达77.25%。

A good agreement existed between STT and UPSIT results and patients' reports.

问卷、乙酚乙二醇气味侦测阈值检查和宾州大学嗅觉识别检查的结果有好的一致性。

Extracted DNA by CTAB, in proportion to the additions of PVP and β-mercap toethanol to the extraction buffer were capable of preventing browning from taking place in the extraction, Tris-Phenol (Stabilized with 0.1M Tris, pH 8.0)/Chloroform/isoamyl alcohol were used to remove protein and impurity in the second extraction, during crude DNA used to Isopropanol DNA and deterged by DNA detergent, without using RNase remove RNA, we detected the quality and concentration of DNA respectively for normal leaves and drought stress leaves by Agarose gel electrophoresis of genomic DNA and ultraviolet spectrometry photo.

用20%聚乙二醇(polyethylene glycol,PEG6000)模拟干旱,采取CTAB提取缓冲液,按一定比例加入PVP和β-巯基乙醇,用Tris平衡酚-氯仿-异戊醇除去蛋白质及杂质,在粗提时用异丙醇沉淀DNA,并用DNA洗液(10mmol/L醋酸铵,75%乙醇)洗涤DNA,在纯化时用乙醇沉淀DNA,且没有加入RNase去除RNA的方法,分别提取2个品种正常和干旱胁迫的苹果属叶片总DNA,并对提取的DNA进行琼脂糖凝胶电泳和紫外分光光度计检测。

The synthetic condition s of benzaldehyde and glycol acetals by 732#strong acidic ion exchange resin are studied.

研究了苯甲醛与乙二醇在732#强酸性阳离子交换树脂催化下的合成条件,得到了缩醛化反应的最佳合成条件:醛/醇摩尔比为1∶1。

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