乙二酸

Apparent partition coefficient in octanol-water and binding percentage to BSA of ~(153)Sm-NTMP,~(153)Sm-HEDTMP,~(153)Sm-DCTMP,~(153)Sm-EDTMP,~(153)Sm-DTPMP,~(113,117) Sn~m-EDTMP,~(113,117) Sn~m-HEDTMP,~(113,117) Sn~m-DTPMP are measured. The results show that there is a linear relationship between the relative magnitude of the apparent partition coefficient in octanol-watetr and the relative magnitude of the binding percentage to BSA of these ~(153)Sm~(113,117Sn~m complexes.

测定了NTMP，HEDTMPN (羟乙基乙二胺基三亚甲基膦酸，DCTMP(1，2 环己二胺四亚甲基膦酸)，EDTMP(乙基二胺基四亚甲基膦酸)，DTPMP(二乙基三胺基五亚甲基膦酸)的153Sm配合物以及HEDTMP，EDTMP，DTPMP的113，117Snm配合物在正辛醇水中的表观脂水分配系数和在0 5%牛血清白蛋白水溶液中与BSA的结合率。

Diethyl fumarate was synthesized with fumaric and alcohol as raw materials and sodium acid sulfate as catalyst.

富马酸二乙酯(又名反丁烯二酸二乙酯，Diethylfumarate，简称DEF)是一种用途广泛的有机合成中间体[1，2]。

Water,cetearyl alcohol,butylene glycol,ceteth-20,glycolic acid,cyclomethicone,citric acid,sodium hydroxide,xanthan gum,lactic acid,phenoxyethanol,sodium citrate,magnesium aluminium silicate,citrus aurantium dulcisoil,disodium edta,pentadecalactone,methylparaben,iris germanica root extract,butylparaben,ethylparaben,propylparaben,silica,chlorhexidine digluconate.citrus aurantium amaraoil,limonene,linalool

水， 棕榈醇，丁二醇，鲸蜡醇聚醚 20，甘醇酸，环甲硅脂，柠檬酸，氢氧化钠，山羊胶，乳酸，苯氧乙醇，柠檬酸钠，硅酸镁铝，甜橙油，乙酸乙二胺二钠，环十五内酯，羟苯甲酯，鸢尾花根萃取，羟苯丁酯，羟苯乙酯，羟苯丙酯，二氧化硅，洗必泰葡萄糖酸盐，苦橙油，柠檬精油，芳樟醇

A novel liquid crystalline compound named p-phenylenediamine di 4-[2- benzamide] was synthesized from allyl 2-hydroxyethylether, ethyl 4-hydroxybenzoate and p-phenylenediamine.

以乙二醇单烯丙基醚、对羟基苯甲酸乙酯、对苯二胺为原料合成了末端为不饱和双键的芳香聚酰胺溶致型液晶化合物——二对烯丙氧基乙氧基苯甲酰对苯二胺，最佳合成的摩尔比为∶羧酸∶对苯二胺∶吡啶=2。

Cycloalkylation of diethyl malonate and ethyl cyanoacetate with alkyl halide was investigated in the presence of toluene.

以甲苯为溶剂及带水剂，用粉末K2CO3代替常规使用的乙醇钠，在季铵盐和聚乙二醇混合相转移催化剂的存在下，含有活泼氢的丙二酸二乙酯和氰乙酸乙酯与二卤代物进行缩合反应，得到相应的环化物。

With toluene two isocyanogen diethylene glycol dinitrate, the polyester or the polyether dihydroxy alcohol, two methylol propionic acid, the triethylamine, the ethylene diamine and so on are raw materials, uses the prepolymer dispersion method, has prepared a series of anion river character polyurethane emulsion.

用甲苯二异氰酸酯、聚酯或聚醚二元醇、二羟甲基丙酸、三乙胺、乙二胺等为原料，采用预聚物分散法，制备了一系列的阴离子水性聚氨酯乳液。

Polyester polyol which was used for polyurethane hot melt adhesives was synthesized by the condensation polymerization of adipic acid and ethanediol, butanediol, hexanediol.

以己二酸、乙二醇、丁二醇、己二醇为原料进行酯化、缩聚反应，以钛酸丁酯为催化剂，采用阶梯式升温方式，合成了聚氨酯热熔胶用已二酸系聚酯多元醇；考察了醇酸摩尔比、催化剂种类和用量以及反应条件对酯化、缩聚反应的影响。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethyl malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effective base.

在这类催化反应中，碱的选择具有重要的影响：以K3PO4为碱， Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中，富电子溴代芳烃显示较好的活性； Pd2/L1催化的乙酰乙酸乙酯α-芳基化时，以 K2CO3为碱，催化体系显示较好的活性，这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯，而不是脱乙酰基的产物。

Base played a crucial role in this reaction: in the Pd2/L1 catalyzed α-arylation of ethy malonate, K3PO4 is the base of choice; in the α-arylation of ethyl acetoacetate, K2CO3 is the most effectiv base.

在这类催化反应中，碱的选择具有重要的影响：以K3PO4为碱，Pd2/L1催化体系在丙二酸二乙酯的α-芳基化中，富电子溴代芳烃显示较好的活性；Pd2/L1催化的乙酰乙酸乙酯α-芳基化时，以K2CO3为碱，催化体系显示较好的活性，这个催化体系可控制反应得到α-芳基乙酰乙酸乙酯，而不是脱乙酰基的产物。

The synthesization technics of MPEG- MAA was studied in this paper,which is an important intermediate used for preparation of polycarboxylate superplasticizer.

本文对制备聚羧酸系减水剂的重要中间体——甲基丙烯酸聚乙二醇单甲醚酯的合成工艺进行了研究，考察了反应时间、催化剂对甲苯磺酸的用量、阻聚剂对苯二酚的用量、反应温度及甲基丙烯酸与聚乙二醇单甲醚的用量比对酯化率的影响。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐