乙二酸

Lactide, glycolide or caprolactone, biodegradable polyester and diisocyanate as materials are first bulk melt polymerized to prepare the degradable polymer with thermal deformation transforming temperature of about 37 deg.c. The obtained material is processed at temperature over melting temperature so as to shape into spiral rack, applied with stress at temperature higher than Ttrans to form shape easily operational handling and frozen to eliminate stress into the product.

本发明以丙交酯、乙交酯或己内酯，生物可降解聚酯及二异氰酸酯为原料，通过本体熔融聚合制备得到热致形变温度转化点在37℃左右的可降解高分子材料，将得到的材料在熔融温度以上进行加工、赋形制作成用于不同管腔内的螺旋管状支架；在T＞T trans 条件下施加应力，加工为便于手术操作的形状；冷冻定型消除应力，即得产品。

By reacting isobutyraldehyde with diethyl oxalate using sodium methoxide as catalyst,3-methyl-2-oxobutanoic acid,sodium salt was prepared by one pot.

采用甲醇钠催化异丁醛与草酸二乙酯反应，一釜法合成了3-甲基-2-氧代丁酸钠。

Acetylpyruvic acid methyl ester can be synthesized by the condensation of dimethyl oxalate and acetone in the presence of sodium methoxide.

叙述了在催化剂甲醇钠的存在下，以草酸二甲酯和丙酮为原料合成乙酰丙酮酸甲酯的工艺。

By using gas chromatography technique nine kinds of fragrance components(acetic aldehyde,ethyl acetate,ethanol,propyl acetate,3-hydroxy-2-butanone,acetic acid,furfural,metacetonic acid,2,3-butylene glycol)were measured quantitatively in different kinds of Shanxi overmature vinegar and the other kinds of vinegar.

应用气相色谱方法对山西老陈醋和其他种类醋的9种香气成分(乙醛、乙酸乙酯、乙醇、乙酸丙酯、3-羟基-2-丁酮、乙酸、糖醛、丙酸、2，3-丁二醇)进行了定性、定量测定，并用聚类分析、模糊综合评判、方差分析、回归分析的方法对实验结果进行了数理分析。

A new method for the synthesis of 1 methyl 3 propyl pyrazol e 5 carboxlic acid from 2 pentanone and diethyl oxalate is reported.

以 2 -戊酮和草酸二乙酯为起始原料，经缩合、与甲基肼环合、水解等三个步骤合成了 1 -甲基-3-丙基吡唑-5 -羧酸。

In this work,the new kind of polyurethane have been prepared from Bis(4—β—hydroxyphnyl)sulphone,polyhydrofuran, 4,4′—di—phenylmethane diisocyanate,by one—step reaction metho -d and block copolymerizatiano.

本文用一步反应法，由双(4-β-羟基乙氧基苯)砜，聚四氢呋喃，4，4′—双苯基甲烷二异氰酸，采用嵌段共聚法，制成了一种新型聚氨酯。

Aldol condensation 2, 5-dimethoxymethoxyacetophone with 2, 4, 6 -tri methoxymethoxybenzendehyde, then hydrogenation, reductive, the key intermediate 83 (84) of natural product 3, 5, 7, 2′, 5′- pentahydroxyflavan, was obtained; Mini reviewed EGCg activity, Then gallic acid and phloroglucin were used to synthsis EGCg, The key intermediate Chalcone 109 of EGCg was abtained through 7 steps from gallic acid.

重点介绍了以没食子酸为原料，经酯化，保护，还原，氧化，格氏反应，氧化六步反应得到3，4，5-三苄氧基苯乙酮，以间苯三酚为原料，经维斯迈尔反应，苄基保护，甲氧甲氧基保护三步反应得到2，4-二苄氧基-6甲氧甲氧基苯甲醛，酮106与醛108经羟醛缩合得到EGCg重要反应中间体查尔酮109。

DHCC Constance in the chemistry belongs to the onlighted Cyclopentanoperhydrophenanthrene when it reacted together with the acid Constance it could transform into the fluorescence phenol.we did the flouric determination for the DHCC, in which treated by the ethanol-sulfuric acid or acetic anhydride-methylene chloride-sulfuric acid, acquired standard curve in the 0-40μg/ml presented the liner relet...

DHCC类物质在化学上属于不发光的环戎烷多氢菲类，但与酸性物质一起反应时，可转化为产生荧光的酚类。用乙醇硫—酸或乙酸酐—二氯甲烷—硫酸处理后的DHCC进行荧光检测，获得标准曲线0—40μg/ml范围内呈线性关系，检出的最高灵敏度可达300ng/ml。该方法可用于分离后的DHCC及单一种DHCC代谢物的定性及定量分析。

By chemical and spectroscopic analysis , the five compounds were identified as isosakuranetin , 4′,7-dimethylkaempferol, eriodictyol-7-methylether, Rhamnetin, daucostorol .

采用气相色谱-质谱联用技术，对有效部位B进行分析，鉴定出34种化合物，主要为不饱和脂肪酸类和萜烯类成分，其中9，12-十八碳二烯酸乙酯的含量最大。

Twelve new Schiff bases of 5-amino-1H-1,2,3,4-tetrazolyl were synthesized. These Schiff bases were further converted into α-(5- tetrazolyl)-aminoalkyl phosphonates.

合成了12个新的5—氨基—1H—1，2，3，4—四唑的Schiff碱，而后与亚磷酸二乙酯反应，合成出了12个新的含四唑基的α-氨基烃基膦酸酯，通过IR，^1H NMR，^31P NMR和元素分析证实了它们的结构。

Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在，'歼灭战perfuming自己与胡努特，那麼，他来到和SAT 。