乙二酸

A novel method for the synthesis of α-bromo acetophenone s by the reaction of 1,3-dibromo- 5,5-dimethylhydantoin with p-toluenesulfonic acid in methanol at 20～60 ℃ was described.

报道了使用1，3-二溴-5，5-二甲基海因和对甲苯磺酸在甲醇中和20～60℃的温和条件下合成α-溴代苯乙酮的新方法。

Methods: P-toluenesulfonic acid diethoxyphosphorylmethyl ester (4) was prepared from diethyl phosphate and paraformaldehyde by condensation and esterification.

以亚磷酸二乙酯和多聚甲醛经缩合、酯化得到对甲苯磺酸羟甲基磷酸二乙基酯(4)。

Methods The lymphocytes of rats were isolated from the peripheral blood and cultured with sodium arsenite under 37 ℃.The ROS content was detected by DCFH-DA;The content of LPO was detected by fluoresce method.

体外分离大鼠外周血淋巴细胞后，施加处理因素，在37℃条件下恒温培养，用2'7'-二乙酰二氯荧光素染色法检测细胞内的ROS水平，用硫代巴比妥酸荧光法测定细胞内LPO含量。

Methods: All the patients recruited were randomized into the diclofenac diethylamine salt gel and diclofenac sodium gel groups and treated with local application three times daily for 14 days respectively.

4 0例患者随机分为双氯芬酸二乙胺盐凝胶组和双氯芬酸钠凝胶组进行临床对照试验，分别采用局部涂擦给药法，tid ，14d为 1疗程。

The synthesis methods of ethyl lactate catalyzed by P-toluene sulfonic acid, cationic exchange resin, ferric chloride hexahydrate, stannous chloride, Aluminium chloride, modified zirconium oxid, ferric-potassium vitriol, ammonium ferric sulfate dodecahydrate, rave earth sulfate, sodium bisulfate monohydrate, complex solid superacid, heteropoly acid, molecular sieve, ionic liquid and lipase etal.

评述了对甲苯磺酸，阳离子交换树脂，六水三氧化铁，氯化亚锡，三氯化铭，改性氧化锆，铁钾矾，十二水合硫酸铁铵，稀土硫酸盐，一水硫酸氢钠，复合固体超强酸，杂多酸，分子筛，离子液体和脂肪酶等催化剂催化合成乳酸乙酯的合成方法。

Alidase was prepared by coupling silica-gel spheres already carrying γ-aminopropyltriethoxy-silane with glutaraldehyde, and then with N-(p-aminophenyl) oxamic acid.

将γ氦丙基三乙氧基硅烷取代的微球硅胶先后与戊二醛，对氨基苯草氨酸结合，制成了一种新的吸附剂，用于唾液酸酶的亲和提纯。

To select the inhibitor component used to produce solid inhibitor,7 types of phosphonate scale inhibitor s are evaluated,and HEDP is proved to be most effective and have a rather good properity of heat-stability.

为筛选制作这种固体块所需的材料，评价了7种膦酸盐防垢剂，发现羟基乙叉二瞵酸对碳酸钙垢具有较高的防止能力，且热稳定性好。

The esterification of mixing binary acid with ethanol was carried out under silicotungstic acid as catalyst in this experiment.

以混合二元酸为原料酸，硅钨酸为催化剂，与无水乙醇进行酯化反应制备混合二元酸二乙酯。

A base-catalyzed novel olefination methodology based on elimination of p-toluenesulfonamide:Treatment of diethyl cyanomethylphosphonate with catalytic amount of basegave the corresponding phosphoryl-stabilized carbanion, which added to the carbon-nitrogen double bond of N-tosyl imines.

新形成的氮负离子进一步攫取另一分子膦酸酯的活泼亚甲基氢形成加成产物同时再生出膦酰基稳定的碳负离子。加成产物消除对甲苯磺酰胺，高度立体选择性地得到-α-氰基-β-芳基-乙烯基膦酸二乙酯。

ABSTRACT: In the presence of sodium t-butoxide and DMSO,ethyl 2-oxocyclopentanecarboxylate was subjected to C-alkylation with 2-(4-bromomethylphenyl)propanoic acid with high regioselectivity to give 2-［4-(1-ethoxycarbonyl-2-oxo-1-cyclopentanylmethyl)phenyl］propanoic acid (4) which was followed by hydrolysis,decarboxylation and salt formation to afford loxoprofen sodium in about 72% overall yield.

在叔丁醇钠和二甲基亚砜的存在下，2-丙酸对2-乙氧羰基环戊酮进行C-烷基化，再经水解脱羧，成盐即得洛索洛芬钠，以2-丙酸计算，总收率为72%。

Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在，'歼灭战perfuming自己与胡努特，那麼，他来到和SAT 。