乙二酸

Three ways leads to the synthesis of fenclorin, one way discussed here has 3 steps. Stepl :benzonitrile using as raw material goes though dry hydrogen chloride and becomes a-imino phenylmethyl ether after meet carbinol.

解草啶的合成主要有三条路线，本文选取合成路线是以苯甲腈为原料，经三步反应而成：1、苯甲腈在干燥的氯化氢通入，与甲醇形成亚氨基苯甲醚，通入氨气后置换甲氧基得到苯基脒盐酸盐(收率76.18%)。2、苯基脒盐酸盐在碱性条件下与丙二酸二乙酯环合而得嘧啶醇(收率84.39%)。3、嘧啶醇在三氯氧磷中羟基被氯化得到产品解草啶(收率87.29%)。

Urethane adduct was synthesized from decarboxylated cashew nut shell liquid,hexamethylenediisocynate and polyethylglycol,which was then reacted with melamineformaldehyde resin to form aqueous coating material.

采用天然植物油、己二异氰酸酯和聚乙二醇在较温和的条件下反应，制得了水溶性的氨基甲酸酯加成物，以此和低醚化度甲醚化三聚氰氨甲醚甲醛树脂制备了水性涂料。

The intermediate of flazasulfuron weedicide ,2-amino-4,6-dimethoxypyrimidineis conveniently obtained by treating 2-amino-4,6-dihydroxypyrimidinewith diazomethane at 20 °C for 24h.

本文利用硝酸胍和丙二酸二乙酯为起始原料，经环合及甲氧基化两步反应得到除草剂啶嘧磺隆的中间体：2-氨基-4，6-二甲氧基嘧啶。

The method of liquid phase synthesis of dioxane from the cyclodehydration of diethylene glycol catalyzed by ASP-type solid acidic catalysts was studied.

研究了ASP型固体酸催化剂一缩乙二醇环化脱水合成1，4-二氧六环的液相反应。

The preliminary stiochiometric analysis showed that when the enzyme metabolized EDDA, two acetyl groups were removed and ethylenediamine and two glyoxylates were produced in the presence of oxygen.

然后对该酶促反应进行了定量分析：结果显示在IDA氧化酶的作用下每代谢一分子的EDDA将生成二分子的乙醛酸及一分子的乙二胺，同时也检测到过氧化氢的生成。

In this report, the 59Tc labelling of Annexin V fragment modified with HYNIC (HYNIC-Anx13) using Tricine, EDDA or EDDA/Tricine as coligands was described. The effect of various factors on 99Tc labelling was investigated. Biodistribution studies in normal mice and gamma imaging of apoptosis in rats induced by cyclophosphamide were performed.

为探讨99Tc标记的HYNIC-Anx13用于细胞凋亡显像的可能性，分别以N-［三甲基］甘氨酸，乙二胺－N，N'-二乙酸和EDDA/Tricine为协同配体，对经6-肼基烟酰基修饰的膜联蛋白V片段(HYNIC-Anx13)的99Tc标记条件和主要影响因素进行了研究，并完成了HYNIC-Anx13的99Tc标记物在正常小鼠体内的生物分布和大鼠细胞凋亡模型的显像实验。

Methods: TOCA was labeled with (superscript 99m)Tc using HYNIC as bifunctional chelator, EDDA and trieine as coligand. The nude mice bearing human small cell lung cancer underwent static whole body planar imaging after the injection of (superscript 99m)Tc-HYNIC-TOCA or (superscript 99m)Tc-P829. ROIs were drawn and the radioactivity ratios of target to non-target were calculated in every planar imaging. The dynamic biodistribution study was operated in Kunming mice and the percent uptake ratios of two imaging agents in different tissue at different time were measured.

以HYNIC为双功能螯合剂(bifunctional chelator， BFC)，乙二胺－N，N'-二乙酸和三甲基甘氨酸为协同配体进行TO-CA的(上标 99m)Tc标记；以(上标 99m)Tc-HYNIC-TOCA和(上标 99m)Tc-P829为显像剂，对荷人类小细胞肺癌裸鼠进行显像，通过感兴趣区技术进行半定量分析，计算并比较两种显像剂的靶/非靶比值；在昆明鼠体内进行动态生物学分布实验，测定并比较不同时点两种显像剂在各脏器的克组织百分摄取率。

The results indicated that among sodium dodecyl benzene sulfonate, sodium oleate and glycol, the sodium oleate has good effect.

结果表明，在十二烷基苯磺酸钠、油酸钠和乙二醇3种不同的表面活性剂中，选用油酸钠效果最好。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, acetochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、电化学法、乙醛酸钙法、尿素三氯乙醛合成法、尿酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

The adsorption isotherms of Sodium Dodecyl Sulfonate onto wool fiber surface which experienced clean processing from an acid aqueous solution(pH3.0～3.5) by conductance method at 366K(93℃) were studied, so did the isotherms of wool adsorbing SDS from different aqueous solutions which containing various auxiliaries(containing glycol/benzalcohol and zinc sulfate).

戴丽 ，耿信鹏，林国栋采用电导法研究了366K(93℃)时经洁净处理的羊毛纤维在酸性(pH=3.0～3.5)水溶液中对十二烷基磺酸钠的吸附等温线，以及羊毛在不同助剂(含乙二醇/苯甲醇和硫酸锌)的水溶液中对SDS的吸附等温线。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。