乙二酰二胺

In this thesis, a convenient and efficient synthesis of highly functionalizeddihydropyrido[2,3-d]pyrimidines via a double [5 + 1] annulation strategy startingfrom easily available α-alkenoyl-α-carbamoyl ketene--acetals 1 and cheapreagents (NH4OAc, DMF, and POCl3) has been developed.

本论文探索了一种简便有效的合成高度官能化的二氢吡啶并[2，3-d]嘧啶的方法，此方法由易得的α-乙酰基-α-氨基乙酰基二硫缩烯酮1和便宜的试剂(醋酸铵，二甲基甲酰胺和三氯氧磷)通过两步[5 + 1]加成而实现。

Preparation of ethylene bis stearamide using stearyl chloride and ethylenediamine as raw materials has been studied.

研究了以乙二胺和硬脂酰氯为原料制备乙撑双硬脂酰胺的反应，讨论了原料配比、反应时间、反应温度的影响。

Solubility measurement shows synthesized benzyl alginate was soluble in formamide, glycol, propylene glycol, and water, a...

试验表明，合成的褐藻酸苄酯可溶于甲酰胺，乙二醇、丙二醇和水，在二甲基甲酰胺中可被溶胀。

Ten kinds of metal and three kinds of organic templates, including ethylenediamine, 1,4-butylenediamine and pyrazine were used in the synthesis of metal phosphonate coordination polymers.

在所合成的16种金属有机膦酸盐配位聚合物中，有机配体为2-羟基乙酰基膦酸，用于配位的金属离子共10种，模板剂3种分别为乙二胺(en，1，4-丁二胺，哌嗪。

Temperature-sensitive hydrogels P(NIPA-co-DiAB) with aromatic group as hydrophobe was were prepared by free radical micellar crosslinking copolymerization with N-isopropyl acrylamide, N,N-dially benzylamine as comonomers, N,N-methylene-bis-acrylamide as crosslinker, sodium dodecyl sulfate as surfactant and ammonium persulfatetetramethylethylenediamine as initiator system.

以N-异丙基丙烯酰胺、N，N-双烯丙基苄胺为共聚单体、N，N-亚甲基双丙烯酰胺为交联剂、十二烷基硫酸钠为表面活性剂、过硫酸铵-四甲基乙二胺为氧化还原引发体系，采用自由胶束交联共聚法合成了疏水基团为芳香基的疏水改性温敏性智能水凝胶P(NIPA-co-DiAB)。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

The diluent contain magnesium chloride, potassium citrate, sodium glutamate, dipotassium hydrogen phosphate, monopotassium phosphate and fructose, semen vitality is hightest after frozen.The average value is 0.52,highter than other 5 diluent significantly (P﹤0.01).So chose this diluent as semen cryopreservation diluent on chicken. Definite cryoprotectant, equilibrium time and thaw temperature:On the base of test one,research freeze sheltering effect about glycerin, DMSO ,DMA and DMF, each with 4 consistency.The result showed that 10%DMSO sheltering effect is the best, the next is 4%DMA,semen vitality are 0.58 and 0.55 after frozen.

冷冻保护剂、平衡时间和解冻温度的确定在试验一的基础上，研究甘油、二甲基亚砜、二甲基乙酰胺、二甲基甲酰胺4种冷冻保护剂在4种浓度下对鸡精子的冷冻保护作用，结果表明，10%DMSO保护效果最好，其次为4%浓度的DMA，精液冻后活力分别为0.58和0.55，两者之间差异不显著(P﹥0.05)。

The solvents commonly used in the solvothermal synthesis include alcohols (such as methanol, ethanol, isopropanol, alcohol, ethylene glycol, glycerine, etc.), amines (such as hexamethylenediamine, dimethylformamide, triethanolamine), Acetonitrile and Propionitrile, the differences of functional groups, varieties of kinds together with a wide differences of polarity, dielectric constant and boiling point of organic solvents greatly increase the diversities of the product.

溶剂热合成常用的溶剂有醇类(如甲醇、乙醇、异丙醇、正丁醇、乙二醇、甘油等)，胺类(如己二胺、二甲基甲酰胺、乙醇胺)，乙腈和丙腈等，有机溶剂由于带有不同的官能团，种类繁多，具有不同的极性、介电常数、沸点等，大大增加了合成产物的多样性。

They are insoluble in water, ethanol, methanol, acetone, chloroform and benzene, but soluble in DMA, DMF and DMSO.

它们溶于N，N-二甲基甲酰胺、N，N-二甲基乙酰胺和二甲基亚矾等溶剂，但不溶于水、乙醇、甲醇、丙酮、氯仿和苯。

Cellulose benzoate,the degree of substitution of which was calculated from the content of C determined by element analysis,was prepared from microcrystalline celluloseand benzoyl chloride under heterogeneous condition and characterized by FT-IR and~1H-NMR.

研究了微晶纤维素和苯甲酰氯在多相条件下合成制备纤维素苯甲酸酯的反应，通过元素分析所得碳的质量百分含量计算了产物的取代度，并系统研究了吡啶与N，N-二甲基乙酰胺或与三乙胺混合反应溶剂、苯甲酰氯与纤维素羟基的摩尔比r、反应温度和反应时间对D S的影响，用FT-IR和1H-NM R对产物进行了表征。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。