主要产物

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist"s attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What"s more, PILM was mainly studied as a catalyst in oil refining process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有&三明治&结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist's attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What's more, PILM was mainly studied as a catalyst in oil refinin g process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有&三明治&结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

The shredding of agro-residues, such as corn stalk, straw, wood sawdust and other herbaceous biomass, were investigated in this dissertation. According to the machinery mechanics of shredding, the components, shearing strength and pressive strength of the biomass were analysed in theory, which played a critical role during the shredding process. And the powder was examined by Scanning Electron Microscopy. It was founded that shearing,splitting and grinding force were appropriate for shredding biomass. The results also showed that primary shredding was the bulk shredding model, which was mainly affected by shearing and splitting force, therefore the curly knife and the straight knife were useful; while the fine shredding was the surface shredding model, affected by splitting and grinding force, and the straight knife useful.

本文以农林废弃生物质为研究对象，结合机械力破碎基础理论，从影响其破碎的化学组分和剪切强度、抗压强度等力学角度进行了理论研究，并运用扫描显微镜对破碎产物的微观结构进行了实际分析，结合二者得出如下结论：最适合生物质的施力方式为剪切力、劈碎力和磨削力；生物质粗破碎为体积破碎，主要受剪切力和劈碎力作用，刀片宜设计成弯口刀和单面直刃刀；细破碎为表面破碎，主要受剪切力和磨削力作用，刀片宜设计成双面直刃刀。

The normally brominated Baylis-Hillman adducts were formed as the major product at low temperature. While at room temperature or heating, the α,γand β,β-dibrominated compounds were formed as the major products using 3-butyn-2-one and methyl propiolate or propynenitrile as substrate, respectively.

贫电子炔类化合物的Baylis-Hillman反应的研究在这部分工作中我们发现在用TiBr〓或BBr〓为Lewis酸催化贫电子炔类化合物和芳香醛的Baylis-Hillman反应时，温度对反应的影响很大：当反应在低温下进行时，通常生成的是正常的β-溴代的Baylis-Hillman反应产物；而在室温或加热条件下反应，以丁炔酮为底物时，主要生成的是α，γ-二溴化合物，而以丙炔酸甲酯及丙炔腈为底物时，主要生成的是β，β-二溴化合物。

In order to investigate the source of nucleic acid in the sera of host infected with S. japonicum, single or dual sex cercariae of S. Japonicum infected mice models were set up for further research.

结果初步证实在日本血吸虫感染早期，血清中的核酸物质可能主要来源于移行过程中死亡的童虫以及虫体发育过程中更新脱落的表皮组织，而在感染的急性期和慢性期，小鼠血清中的核酸物质可能主要来源于虫卵的分解产物。

Furthermore, the theory about denitrifying by oxidation in gas phase and absorption in liquid phase and desulfurizing by absorption and oxidation in liquid phase is deduced.

理论表明，放电等离子体对SO2 的去除有一定作用，但主要取决于水的吸收；NO的去除主要归于发生在气相的氧化反应，水的存在起到了吸收氧化产物的作用。

In these three kinds of fishes,Gnrh2 was not only expressed in midbrains,but also expressed in pituitaries and gonads.And Gnrh2 mRNA was mainly located in posterior end of midbrain.It was indicated that Gnrh2 might mainly act as the neurotransmitter and neuromodulator,and it also might participate in the regulating of other hormones releasing,such as GTH and STH.

Gnrh2基因在三种鱼的中脑、垂体和性腺中均有表达，其转录产物主要定位于中脑的后部，说明Gnrh2基因可能主要起神经递质或神经调节剂的作用，但也参与调节促性腺激素、生长激素等的释放。

The major reaction product of coal in the arc plasma reaction is acetylene and CO. The acetylene is come from the saturates and aromatics in the coal.

2煤在电弧等离子体中反应的主要的产物是乙炔和一氧化碳，乙炔的来源主要是煤中的饱和分和芳香分。

It is concluded that lead source of all the nine deposits studied in this paper can be located to the specific position by the comparison method. Only by the comparison of Pb compositions of ore with those of the other rocks, the studying conclusions may be trustworthier.

结果表明，与岩浆活动有关的夕卡岩型和岩浆热液型矿床有两种情形，一种是纯岩浆源铅，另一种是部分围岩铅也参与了成矿；热水沉积矿床的铅主要来自深部；改造型矿床的铅主要来自围岩；像留龙金矿这样看似与岩浆活动关系密切的矿床，对金而言，是改造成矿的产物。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。