主要产物

The image showed that the ratio of raw material of RPC and particle distribution accorded with maximum packing density theory, and the porosity of accumulation was the least. The DSC showed the reaction rate of RPC was very fast and main hydration process focused in shorter time; SEM and X-ray showed that structure of the harden body of RPC was much denser, which mainly composed of some abnormal flat grains that got maximum packing density, and hydration products were mostly composed of Ⅲ type C-SH gel and a small amount of Ca2 and no AFt crystal.

由图象分析可知，即C原材料的比例及颗粒度符合密实堆积原理，堆积物的孔隙率达到最小；差示扫描量热分析表明，RPC的水化反应速度很快，主要的水化过程集中在较短时间内；扫描电镜及X衍射试验表明，RPC硬化体的结构非常致密，主要由一些不规则状的扁平粒子紧密堆积在一起，水化产物主要是Ⅲ型C-S-H， Ca2晶体的量稀少且没有钙矶石。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

They are 2,3-epoxynopyl acetate,1-hydroxy-2,3-epoxynopyl acetate and 5-hydroxy-2,3-epoxynopyl acetate.The results suggested that the four-ring of nopyl acetate cleaved firstly in th...

分析结果表明反应主要是四元环开裂，并进一步水合，另外伴有少量双键环氧化的产物，这些环氧化的产物还可进一步在C1和C5处发生叔氢氧化。

A detailed analysis of the experimental results implied that the attractive forces play a main role in the collisional quenching processes of NCO by the quenchers studied in this work, and for some quenchers, the quenching of NCO is probably controlled by the entrance-channel and might be ascribed to the contribution of chemical reactions.

这一加成过程是一个入口势能面属于纯吸引型的无垒过程，故是NCO+O反应的主要通道。二是O原子攻击NCO分子的O原子得到中间物tran-NCOO，再通过C-O键的断裂生成产物CN+OO。该产物通道由于是吸热的，故很难发生。

For the first time,a Raman microscopic investigation of the patinas grown on the beautifully shaped bronzes collected in the Dengzhou Museum ,Penglai City,Shandong Province,was done.

首次运用显微喇曼光谱技术，对山东省蓬莱市登州博物馆馆藏古代青铜器的锈蚀产物进行分析，发现锈蚀产物的成分比较复杂，主要有蓝铜矿、孔雀石、氯铜矿、副氯铜矿、白铅矿、黄铅矾及方解石。

The absorption , metabolism and the major forms of metabolites of PAHs in urine are reviewed in the paper.

本文系统介绍了多环芳烃的吸收、代谢、尿中PAHs 代谢产物的主要存在形式、主要的生物标志物以及它们的主要影响因素。

The lumbar spinal cord in normal rat was immunohistochemically stained with ABC method using HAP1B antibody. Under light microscope, it was observed that HAP1 immunoreactants is mainly distributed in the pericaryon and neuropil in superficial lamella of the gray nucleus with little or no expression in other layers of the spinal horn. The substantia alba show no HAP1B immunoreactants.

对正常大鼠腰段脊髓进行HAP1B的ABC法免疫组织化学染色，光镜下观察显示，HAP1免疫反应产物主要分布在脊髓灰质背角浅层神经元胞体和神经毡内，灰质其他各层无或极少HAP1B表达，白质内未见明显HAP1B免疫反应产物。

A series of erosion-corrosion test has been done to J55 steel under the influence of current of gas-liquid phase by indoor self-made devices, and the corrosion mechanism of current of gas-liquid phase to oil pipe's inner surface has been got. The results show that oil pipe's inner surface will be corroded fleetly by liquid medium and corrosion products will form on it. But at the same time, the corrosion products or protective layer will be removed from the inner surface of steel pipes under the alternate impact of high speed gas and liquid flow, and on this bare steel surface corrosion film will form again and be removed again. Thus, by these ways the corrosion is exacerbated. Surface erosion-corrosion failure comes into being with the circulation of this process going on.

本文主要在气液两相流作用条件下，通过室内自制装置，对管材钢J55做了系列冲刷-腐蚀试验，结果表明，气液两相流对钢管内表面冲刷－腐蚀的机理是钢管内表面会受到液体介质的快速腐蚀，生成腐蚀产物，同时钢管金属表面不断被具有高流速的气液相交替地冲击，不断地从金属表面脱去保护膜或腐蚀产物，裸露的钢表面又会被介质快速腐蚀形成腐蚀膜后，再被两相流冲掉，如此反复，造成管内金属表面膜的连续破坏，使腐蚀加剧，最终导致钢铁表面的冲刷腐蚀失效。

Based on the kerogen type, the pyrolysate is high-wax paraffin oil, which is similar to Green River oil shale.

与美国绿河页岩相似，研究区油页岩的热解产物以高蜡-石蜡基原油为主，干酪根结构差异是影响热解产物类型的主要因素。

The detection of gas products was performed by the coupled simultaneous Fourier transform infared spectroscopy. The experimental results showed that the principal product of the pyrolysis is tetrafluoroethylene.

同步傅立叶变换红外光谱仪对氮气气氛下热解的气体产物进行检测，检测分析到PTFE的主要热解产物为四氟乙烯单体。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。