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To minimize the contamination of detrimental elements such as sulfurand chlorine, a two-step sol-gel process was successfully developed to synthesize SiC precursors with oxalic acid and hexamethylenetetramine HMTA as the catalysts, which are free of sulfur and chlorine. Tetraethoxysilane TEOS and phenolic resin were used as the silicon source and carbon source, respectively.

为了尽量减少硫、氯等有害元素的含量,本文用不含有害元素的草酸和六次甲基四胺HMTA为催化剂,正硅酸乙酯TEOS为硅源,酚醛树脂为碳源,成功探索出了制备SiC前驱体的两步法溶胶-凝胶工艺。

Aluminosilicate mesoporous sieves with 13X zeolite units in the pore wall were synthesized with a natural ore, microcline ,as the main raw material,and the precursors of 13X zeolite as the crystal source,by integrating the procedures for MCM-41 and 13X zeolite synthesis.

以天然矿物微斜长石为主要原料,以13X沸石前驱体为晶核剂,结合介孔分子筛MCM-41与13X沸石合成工艺,合成了孔壁中含有13X沸石基本结构单元的铝硅酸盐介孔分子筛。

In two paralytic and one furious rabies patients who hadsevere paresthesias as a prodrome, electrophysiologic studies suggested dorsal root ganglionopathy.

在以严重感觉异常为前驱症状的2例麻痹型和l例狂躁型狂犬病患者中,电生理学研究显示为背根神经节病变。

For this pyrolysis, cadmium acetate dihydrate and sulfur powder were used as the cadmium source and sulfur source, respectively.

以三辛基膦为单一配位溶剂,二水合乙酸福和硫粉为前驱体,用高温热解的方法制备CdS纳米棒。

The synthesized products are mainly composed of equiaxial β-SiC particles with the size of around 100 nm and nanorods with the diameter of ~500 nm and the length of ~20 μm.

在1700℃下反应1h,反应前驱体全部转化为β-SiC,产物为SiC颗粒和纳米棒的混合物。

Factors influencing TiO_2-PILC photocatalystic properties were discussed, including the ratio of CH3COOH and Ti, the temperature and aging time of pillaring agents, pH value of reaction solution, the temperature of calcined, etc.

以钛酸四丁酯为前驱物,冰醋酸为鳌合剂,重点考察了[CH3COOH]/比、柱化剂制备温度和陈化时间、催化剂煅烧温度等对TiO_2柱撑蒙脱土结构的影响。

The results indicate that the pillaring process and crystal growing of anatase can be more easily realized by increasing the acid-base ratio of pillaring agents, raising the pillaring temperature and adding proper quantities of alkali. The calcination of Ti-pillared precursor brings the growth of TiO2 grain, at the same time the layer distance is declined. In order to obtain ideal products, the right pillaring conditions are: the acid-base ratio of pillaring agents of 13, pillaring temperature of 65 ℃ and the volume of alkali (2 mol/L) in pillaring liquid of 6 mL.

结果表明:在一定范围内增大柱撑剂酸碱比、提高柱撑温度以及加入适量碱,有利于插层复合反应的进行和锐钛晶型的生长;柱撑前驱物焙烧后TiO2晶粒长大,同时焙烧引起的脱水导致膨润土层间距的下降;为获得较理想的产物,合适的柱化条件为:柱撑剂酸碱比 n n (HNO3)为13、柱撑温度65 ℃和柱撑液加碱量为(2 mol/L NaOH) 6 mL。

In this paper,the SMO-type lithium ion sieve was the main research object,the manganates and lithium salts were taken as the main raw materials.Two LISs with high uptake capacity,better selectivity and stable structure were successfully prepared by hydrothermal method and coprecipitation method based on the discussion of correlation between Li+ uptake performance and the preparation conditions of LIS precursors.The effects of preparation conditions on Li+ uptake were also investigated.

本文以SMO型锂离子筛为研究对象,以锰盐和锂盐为主要原料,在采用固相法探讨离子筛前驱体制备条件与离子筛提锂性能关系的基础上,分别采用水热法、共沉淀法为主要合成方法,成功制备了具有高提锂容量、选择性好及结构稳定的两种锂离子筛材料,并研究了合成条件对材料制备及提锂性能的影响。

In order to study the influence of preparation techniques on stability of different morphological silver colloid s, stable silver colloid s were produced by the reduction of AgNO3 with the protection of polyvinylpyrroli-done using KBH4 and N2H4 ----------- H2O as reductants.

为了研究制备工艺条件对不同形貌银胶体稳定性的影响,在超声场作用下,以AgNO3为前驱物,聚乙烯吡咯烷酮为保护剂,KBH4和N2H4·H2O分别为还原剂,制备了稳定的银胶体,并利用透射电镜和分光光度技术对制备的银胶体进行了表征。

In this paper, a series of solid base MgO were synthesized via an exotemplating pathway with pine-wood as the template and magnesium acetate as MgO precursor, and were characterized by XRD, SEM, adsorption of n-hexane or nitrogen, Hammett indicator, ICP, JR and TG-DSC techniques.

以松木为模板,乙酸镁为前驱物,通过外模板法制备了一系列的MgO固体碱材料,并用XRD、SEM、正己烷吸附、低温液氮吸附、Hammett指示剂法、ICP、IR和TG-DSC等手段对其进行了表征。

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推荐网络例句

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。