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1H NMR spectroscopic analysis of aromatic protons combined with theoretical analysis of molecular structures proved the existence of two rotational isomers at 300 K, as well as a rapid interconversion equilibrium at 330 K for both compounds Ⅰ and Ⅱ. However, only one conformer exists for compound Ⅲ and puerarin containing 7-phenolic hydroxyl instead of propyl in A-ring as the case of compounds Ⅰ and Ⅱ. Based on UV-Visible absorption data of neutral and basic solutions, and on the density function calculations, the 7-phenolic hydroxyl group in A-ring was found to be more acidic than the 4'-phenolic hydroxyl group in B-ring. The mechanism of derivation reaction and the structure-reactivity relationship of puerarin as an antioxidant were further discussed.

其中7-丙基葛根素Ⅱ属于新型取代衍生物;变温1H NMR和理论计算结果表明,在300 K时,葛根素和4'-丙基葛根素以单一构型存在;而7,4'-二丙基葛根素和7-丙基葛根素则存在两种核磁可分辨的旋转异构体,当温度升至330 K时,两种异构体可以相互转化;通过对比分析葛根素及其衍生物脱质子产物的紫外可见吸收光谱并结合理论计算,确定了A环上7位酚羟基比B环上4'位酚羟基先脱去质子,并由此进一步阐明了葛根素衍生化反应机理以及在抗氧化作用中可能的活性位点和结构活性关系。

Main objectives of medium-temperature tempering: to get high elastic limit and yield strength as well as certain toughness and anti-fatigue.

中温回火的目的是获得高的弹性极限和屈服强度,并具有一定的韧性和抗疲劳能力。

Magnesium silicide (Mg2Si) is one kind of narrow-band-gap n-type semiconductor, and is a promising environmentally friendly thermoelectric material because of its high electrical conductivity and low thermal conductivity, and also because it is non-toxic and non-polluting.

硅化镁(Mg2Si)是一种窄带隙n-型半导体,具有高的电导率和低的热导率且无毒无污染、耐腐蚀,是很有潜力的环境友好型中温域热电材料。

In the present paper,the Palaeozoic strata in the Wenduhala region,Xinjiang are chemostratigraphically divided based on the systematic data of spectral semiquantitative analysis obtained from the regional geological survey by means of the optimal partitioning method and the half moving window method for the ordered sample analysis.

本文利用在区调工作中获得的较为系统的岩石光谱半定量全分析数据,采用有序样品最优分割法和对分移动窗口法,对新疆温都哈拉一带的古生代地层进行了化学地层划分,并与野外根据宏观岩性特征划分的岩石地层单位进行了比

The basic principles of thermocouple temperature measurement are two different components of the composition of the homogeneous conductor closed-loop, when the temperature gradient at both ends of existence, the circuit current will have passed, at this time exist between the two ends of Seebeck electromotive force -- Thermal electromotive force, which is the so-called Seebeck effect.

热电偶测温的基本原理是两种不同成份的均质导体组成闭合回路,当两端存在温度梯度时,回路中就会有电流通过,此时两端之间就存在 Seebeck 电动势——热电动势,这就是所谓的塞贝克效应。

The Company production of porcelain stoneware temperature, color range, variety, production and technical force is rich, is now the company owns a high-quality management team has many years of working experience in ceramic designers, senior technicians.

本公司生产的中温炻瓷,颜色繁多,品种多样,生产和技术力量雄厚,现公司拥有一支高素质的管理团队,有多年陶瓷工作经验的设计师,高级技师。

N-type lead telluride compounds doped with Bi2Te3 were prepared under 3 GPa and 1200 K by HPHT technology.

PbTe是研究较早的最为成熟的热电材料之一。可以被用来制作适合在中温区(400~800K)工作的温差发电装置[1]。

Firstly, through the measurement of temperature dependence of luminescence combined with the thermoluminescence curves, it is demonstrated that the effect of trap states in the crystals on the temperature dependence of luminescence.

第一,在不同的变温方式下测量PbWO〓发光的温度依赖并结合热释光分析,证实了PbWO〓在X射线激发下的发光温度依赖曲线受到晶体中陷阱的影响。

The upper limit of operating load of the fluidized bed is determined by the basic load, stable combustion temperature of barks and the ability of the attemperation system.

流化床实际运行负荷的上限值可根据基本蒸汽负荷、流化床中树皮的稳定燃烧温度和减温系统的工作能力来确定。

The tectonic rocks along the fault zone are composed of cataclastic rocks and mylonites formed in higher, middle and lower temperature. Respectively, both of structural features and rocks have the features of multiple phase's of deformation. The deformation features of main minerals in the high temperature mylonites show that: the quartz has the form of long single crystal and the fabric feature of point maximum near X axis; the feldspar has the form of recrystallization assemblage, They present a high amphibolite-granulite facies with temperature >600℃ and depth >20km. The deformation features of mylonites formed in middle temperature show that: the quartz has the form of polycrystal banding and the fabric feature of point maximum near Y axis and small circle girdle with Y rotational axis; the feldspar has the form of a coremantle structure, They reflect a high greenschist-lower amphibolite facies with temperature from 400℃ to 600℃ and depth from 15km to 20km.

其中,高温糜棱岩主要矿物变形特征组合为:石英为长矩状或长条状单晶、组构为近X轴的点极密,长石为几乎完全重结晶的集合体,形成温度>600℃,相当于高角闪岩—麻粒岩相,形成深度>20km;中温糜棱岩主要矿物变形特征组合为:石英为多晶条带、组构为近Y轴点极密和以Y轴为旋转轴的小圆环带,长石发育核幔结构,形成温度为400~600℃,相当于高绿片岩—低角闪岩相,形成深度为15~20km;低温糜棱岩主要矿物变形特征组合为:石英发育核幔结构、组构特征为近Z轴点极密,长石以碎裂为主,形成温度<400℃,相当于中低绿片岩相,形成深度为8~12km;碎裂岩则主要代表了地表浅层的变形。

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And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

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