中柱的

The Empire is currently a shadow of its former self, having lost a great deal of territory in Asia Minor to the Seljuk Turks, and in other areas to internal strife and civil war.

生活在过去辉煌阴影中的古老帝国，不仅在小亚细亚被土耳其塞尔柱王朝夺取大片土地，更在无休止内乱中疮痍遍体。

Adenosine was used as the raw material, dissolved in triethyl phosphate and then esterified with thiophosphoryl chloride under 0~5℃ for 8h without water and oxgen, in alkaline condition provided by 2,6-dimethylpyridine, introducing thiophosphoryl ester to adenosine.Then superfluous triethylamine was added and reacted under 5℃ for 1h to synthesize rough 5'-AMPS.The unpurified product was appled to a DEAE Sephadex A-25 column and eluted with triethylammonium bicarbonate.

用腺苷为起始原料，溶解于磷酸三乙脂中后，在无水无氧环境中及2，6-二甲基吡啶提供的碱性条件下与三氯硫磷以0~5℃下发生酯化反应8h，将硫代磷酸酯引入腺苷，然后再与过量三乙胺在5℃下反应1h，合成粗产品，再用碳酸氢三乙胺作洗脱液，过DEAE Sephadex A-25凝胶柱纯化。

To study the chemical constituents from the leaves of Celastrus gemmatus Loes., chromatographic methods were used to isolate and purify the chemical constituents, their structures were elucidated by the physiochemical characteristics and spectral data.

为研究哥兰叶(Celastrus gemmatus Loes。)中的化学成分，用Diaion HP-20，Toyopearl HW-40，silica gel等柱色谱方法，从其70﹪含水丙酮提取物中分离得到化合物，并根据理化性质和波谱数据鉴定其结构。

The dominant phytoplankton species outside and inside the bay were Cylindrotheca closterium and Skeletonema costatum, while the samples in the harbor had Skeletonema costatum, Eucampia zodiacus, and Chaetoceros curvisetus as the dominant species.

湾外和湾内站位的浮游植物组成相似，优势种为新月柱鞘藻和中肋骨条藻，港口浮游植物优势种类为中肋骨条藻、浮动湾角藻和旋链角毛藻。

A method combining HPLC, a post-column derivation device and a fluorescent detector was used to determine residues of ten carbamate pesticides （aldicarb sulfoxide, aldicarb sulfone, oxamyl, methomyl, 3-hydroxy carbofuran, aldicarb, propaxur, carbofuran, carbaryl and methiocarb） in 68 vegetable and 32 soil samples under four different cultivation systems （traditional kailyard, open field vegetable base, green house and paddy） were collected from a certain city in South Jiangsu.

本研究采用高效液相色谱-柱后衍生-荧光检测法分析了苏南某市4种不同种植方式下（传统菜地、露天蔬菜基地、大棚蔬菜基地和水稻田）68个蔬菜样品和32个土壤样品中10种N-甲基氨基甲酸酯类农药（涕灭威、涕灭威砜、涕灭威亚砜、杀线威、灭多威、残杀威、克百威、3-羟基克百威、甲萘威和灭虫威）的残留量，结果表明在蔬菜中检出的氨基甲酸酯农药残留水平多处于0.2～23μgkg^-1，土壤中为0.1～10μgkg^-1；土壤中3-羟基克百威和灭虫威全部检出，其最高检测浓度分别为10μgkg^-1和1.64μgkg^-1，其他农药仅有少数检出。

By the infiltration test of soil column, the author concludes that Cr and As has the following migration patterns by dynamic researches. 1 The absorption and migration of Cr and As in loessial soil relate to content of mucilaginous grain.

4通过土柱淋滤试验，从动态角度研究得出铬、砷在黄土中具有以下迁移规律及特点：①Cr、As在黄土中的吸附和迁移与土壤中的粘粒含量有关。

MUC2 apomucin and its mRNA were mainly located in the peri-and supranuclear area of goblet cells of duodenum and column,but no signal in the columnar-type cells.

结果发现，胃粘膜中无MUC2和MUC3基因产物的表达，MUC2核粘蛋白及mRNA主要存在十二指肠和结肠杯状细胞周及核上，柱状细胞中无表达。

Samples were saponified with 20 g/L sodium hydroxide. The sexual hormones were then extracted with dichloromethane-acetic acetate (40∶1, v/v) under acidic conditions (pH 3, adjusted with 1 mol/L HCl ). An XTerraTMRP18 column was employed and a mixture of water-methanol-acetonitrile (50∶32∶18, v/v) was used as mobile phase. The seven sexual hormones were detected at 230 nm. The average spiked recoveries for the seven sexual hormones ranged from 75.6% to 97.8% with relative standard deviations of 1.9% to 7.2%. The linear ranges of determination were from 5 to 50 mg/L with correlation coefficients of 0.9999, and the limits of detection were from 3.7 to 12 ng.

先在试样中加入20 g/L氢氧化钠溶液与油脂进行皂化反应，然后用二氯甲烷-乙酸乙酯(体积比为40∶1)混合液在酸性条件下(pH 3)萃取，选择XTerraTMRP18色谱柱，以水-甲醇-乙腈(体积比为50∶32∶18)混合液为流动相，在波长230 nm处检测。7种性激素分离良好并排除了样品中杂质峰的干扰，低、高浓度平均回收率范围为75.6%~97.8%；相对标准偏差为1.9%~7.2%；检出限为3.7~12 ng。

Carbon nanotubes after oxidation and purification were used to pack a micro-column which was incorporated into a sequential injection system for facilitating online selective sorption of lysozyme from egg-white. The retained protein was afterwards quantitatively eluted by a carbonate buffer. With a sample loading volume of 2.0 mL, an enrichment factor of 12 was obtained, along with a retention efficiency of 100% and a recovery rate of 100%.

将多壁碳纳米管经氧化和提纯后装入固相萃取柱，在顺序注射系统中实现对蛋清中溶菌酶的在线选择性萃取，以碳酸盐缓冲溶液定量洗脱，进样量为2 mL时，富集倍率为12，吸附率和洗脱率均为100%，采样速率为10 h^(-1)，精密度为3.0%。

Scape suberect, usually shorter than leaves, loosely bearing 6-12cm or more flowers; bracts 5mm long; pedicel including ovary 4cm long; flower light yellow-green, faintly fragrant like Osmanthus fragrans ; dorsal sepal nearly oblong, 4.5-6cmlong, 1.2-1.8cm wide, yellow-green ,base tinged purple-brown on back, lateral sepals oblique-oblong, slightly narrow, petals narrower than sepals, 5-12mm wide, light yellow-green, spotted purple-red at base; lip slightly short-clawed, 3-lobed, side lobes erect, striped purple-red, mid-lobe somewhat reflexed, waved at margin, disk pubescent above, with 2paralles lamellae, long-hairy.

花葶近直立，常短于叶，疏生6~12朵或更多朵；花苞片长约5mm ；花梗连子房长约4cm ；花浅黄绿色，稍有桂花香气；中萼片近矩圆形，长4.5~6cm ，宽1.2~1.8cm ，黄绿色，背面基部有紫褐色晕，侧萼片斜矩圆形，稍窄；花瓣比萼片窄，宽5~12mm ，浅黄绿色，基部有紫红色的小斑点；唇瓣略有短爪，3裂，侧裂片直立，具紫红色条纹，中裂片略反折，边缘波状，唇盘上表面被短柔毛，2条褶片平行，生长毛；合蕊柱须长，3~4.2cm 。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。