中柱的

In connection with the application of concrete-filled steel tubular column in the engineering practice in this country at present,a new fashioned connection in framed structure of concrete-filled square steel tubular column with reinforced concrete beam was proposed,being a connection of concrete beam with non-through hidden steel corbel steel tubular column filled with concrete.

结合我国现行钢管混凝土柱在实际工程中的应用状况，提出了用于方钢管混凝土柱-钢筋混凝土梁框架结构的新型连接节点形式非穿心暗钢牛腿方钢管混凝土柱与混凝土梁节点，采用了X型加载试验方案，制作了1∶3的试验模型，进行了低周反复荷载作用下的试验研究，得到了相关的钢筋应力应变发展规律和相应的滞回曲线，通过对试验结果节点破坏的机理分析，提出了进一步的改进措施。

FASS(field amplified sample stacking) is a technique for oncolumn enrichment in capillary zone electrophoresis. The distribution of solute in column during injection can be divided into two parts: the stack zone in running buffer and the sample solution zone imported by electroosmosis.

直接柱头场效应进样是一种毛细管区带电泳柱内富集，其进样过程中样品在柱内的分布可分为两部分，即在运行缓冲溶液中的堆积区段和由电渗流引入的样品溶液区段。

A new method using gel permeation chromatographic cleanup followed by high performance liquid chromatography-tandem mass spectrometry has been established for quantitative determination of Maleic hydrazide,Prowl and butralin residues in tobacco.

建立了用凝胶渗透色谱净化-液相色谱-串联质谱分析烟草中3种抑芽剂残留的方法。卷烟中的待测抑芽剂组分用V∶V=1∶1超声提取后通过凝胶渗透色谱净化；凝胶色谱柱为Biobeads S-X3玻璃柱(50 g，400 mm×25 mm)，流动相为V∶V=1∶1溶液，流速5 mL/min；收集第10~25 min流出的液体用液相色谱色谱-三重四极杆串联质谱仪测定。

A SPE procedure was suggested for extracting and concentrating fisetin by using different volume fractions of ethanol in aqueous solution as the loading conditions.

分别以中药黄栌的主要成分非瑟酮为印迹分子、丙烯酰胺为功能单体及乙二醇二甲基丙烯酸酯为交联剂，通过封管聚合法合成了分子印迹聚合物；将其装于自制的固相萃取柱中，研究了以不同体积比的乙醇-水溶液为溶剂时非瑟酮在柱上的保留行为；通过优化清洗及洗脱条件，使非瑟酮与它的结构相似物槲皮素在柱上得到了很好的分离。

Quercetin, quercetin rhamnoside, hyperin, syringoside and eleutheroside E wereisolated from the flower of Acanthopanax senticosus. Searching bioactive natural compound and establishing quality evaluation standard arefocused on this experiment. Using cold immersing of 70% methanol to extract from flower ofAcanthopanax senticosus and integrating macroporous resin, silica gel column chromatography,sephadex gel to abstract. We obtained five monomer compounds (compoundⅠ-compoundⅤ),quercetin, quercetin rhamnoside, hyperin, syringoside and eleutheroside E. That five compoundswere determined by HPLC in eight parts of Acanthopanax senticosus (flower, root, leaf fruit,shoot, new shoot, phloem of shoot, skin of shoot), which provide science bases for establishingquality evaluation system and settle infarctate foundation.

本文以从刺五加花蕾中寻找具有重要生物活性的天然化合物和建立质量评价标准为主要目的，对其化学成分进行研究，采用70％甲醇冷浸的方法对刺五加花蕾中的成分进行提取，运用大孔树脂吸附色谱法、硅胶柱层析法以及葡聚糖凝胶柱层析相结合的方法进行分离，得到5种单体化合物，分别为槲皮素、槲皮素鼠李糖苷、金丝桃苷、紫丁香苷和刺五加苷E；利用高效液相色谱法对这5种化合物在刺五加花蕾中的含量进行了测定；考察了8个部位(花蕾、根、叶、果、茎干、新枝、茎韧皮部、茎皮)中这5种化合物的含量分布情况，并作一比较，为今后建立刺五加质量评价体系提供了科学依据，奠定了坚实的基础。

The Cretaceous sedimentary rocks were baked by the basaltic lava flow erupted in the Early Miocene, contracting in volume owing to loss of water contained mainly in the clays of the clastic rocks, and thus forming the columnar jointing. According to the occurrences of jointing and the sedimentary strata the authors calculated the two different rotations of the Mellit block: the block tilted toward 338° for 18° from Late Cretaceous to the beginning of Miocene, and tilted toward 138° for 18° since Miocene.

可以合理地假定柱状节理在形成时是垂直于大地基准面的，根据柱状节理和沉积岩层的产状，笔者计算出Mellit地块的两期旋转事件：自晚白垩世初期到中新世初期该地块向338°方向倾斜了18°，而自中新世以来又向138°方向倾斜了18°。

By tailoring the scale between hydrophilic region and lipophilic region, smectic, columnar and cubic mesophases were observed in compounds I-F and II-F. By changing the length of the lateral chains, a series of new columnar phases and a non-conventional semctic phase were obtained in III-F.

通过调节亲水部分和亲脂部分的比例，在I和II-F中观察到了从近晶层相到柱相再到三维立方相的液晶相序列；在波拉分子III-F中通过改变侧链的长度，获得了一系列柱相及新型层相。

Under different combustion pressuring rates of the solid motor, the relations among the convecting combustion flow characteristics, especial the pattern of flame spreading, and the variation of stress intensity factor at the crack tip are discussed in detail.

文中详细描述了在固体火箭发动机燃烧室环境中，药柱裂纹对流燃烧流场特性和固相裂纹体变形特性；燃烧室增压率对裂纹中火焰传播方式的影响；燃烧室增压率、燃烧室平衡压力的设计值、药柱裂纹径向长度对固相裂纹尖端应力强度因子、燃烧室压力的影响。

To purify platelets by magnetic activated cell soring LD and MS respcctively. To evaluate karyotc clearance by leucocount method and to detect the platelets activation grade by flow cytometry method.

血细胞分离机单采外周血中的血小板，分别采用磁性细胞MS柱和LD柱纯化浓缩血小板，采用白细胞绝对计数法对分选前后血小板中的有核细胞进行检测，计算有核细胞去除率。

The lung tissues were extracted with acetonitrile and 0.1M potassium dihydrogen phosphate buffers. The extracts purified by C18 solid-phase extraction cartridges. The eluates were determined by HPLC at 288nm. Limits of detection were 0.025 ug/mL for tilmicosin in plasma and 0.025ug/g for tilmicosin in lung, respectively.

采用C18 SPE柱分离和提纯血浆中的替米考星，用乙腈和0.1M磷酸二氢钾缓冲液提取肺脏中的替米考星，用C18 SPE柱净化，均采用反相高效液相色谱测定替米考星，检测波长288nm。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。