中柱

Results indicate that the optimum extraction conditions are as follows: ultrasonic power is 600W, temperature is 53℃, the ratio of liquid to solid is 8︰1, ultrasonic treating time is 70min, reflux extraction time is 120min, the extraction rate of oleanolic acid is 3.000 mg/g; XDA-1 resin is favorable in purification of OA in Chaenomeles sinensis Koehne, the optimum purification conditions are found to be 0.794 mg/mL of OA concentration, the flow rate of adsorption is 0.5 mL/min; the desorption solvent is 90% ethanol, and the flow rate of elutant is 1.0 mL/min.

结果表明，超声波辅助提取最佳工艺条件为：超声功率600 W、提取温度53℃、液料比8：1、超声波提取70 min，回流提取120 min，齐墩果酸得率为3.000 mg/g；XDA-1型大孔树脂对齐墩果酸具有较好的吸附和解吸效果，最佳纯化工艺条件为上柱液浓度0.794 mg/mL，吸附流速0.5 mL/min；以90%浓度乙醇洗脱，洗脱流速1.0 mL/min，纯化后得提取物中齐墩果酸纯度可达26.55%。

Use cacl2 solution to make dissolve infusion, through column dip percolation filtration the experiment inspected calcium of chloridize of infusion of ore granuality, dissolve the parameter such as length of method of speed of solution quality mark, percolation filtration, percolation filtration is right the effect that the dissolve of the potassium in miscellaneous bittern stone gives.

梗概： 采用cacl2溶液作溶浸剂，通过柱浸渗滤试验考察了矿石粒度、溶浸剂氯化钙溶液质量分数、渗滤速度、渗滤路径长度等参数对杂卤石中钾的溶出的影响。

After acid hydrolysis of urine, primary amino acids were derivatized with ortho-phthaldialdehyde and removed from the sample by use of silica gel, followed by devivatized of hydroxyproline with 9-fluorenylmethyl chloroformate, and then injected into a C8 reversed-phase column.

采用邻苯二甲醛和芴甲基氯甲酸酯两个衍生剂，先后处理尿标本，以国产C8柱为固定相，在醋酸钠缓冲液中加入23%的乙腈作为洗脱液，3，4-脱氢脯氨酸作为内标。

The study on the extracting small experiment of Choleic acid, Glycocholic acid and Taurocholic acid.The extracting small experiments of Choleic acid, Glycocholic acid and taurocholic acid were studied by adopting deproteinizatio, depigmentation, extraction and column chromatographic fractionation.

提取胆酸、甘氨胆酸、牛磺胆酸的小试工艺研究采用脱蛋白、除色素、萃取、柱层析分离等方法开展了从牛羊混合胆汁中分离、提取和纯化胆酸、甘氨胆酸及牛磺胆酸三种有效成分的小试提取工艺研究。

The free radical scavenging properties of six Aloe species are to be investigated in some modified chemical system. The antioxidant was purified by silica column and thin layer chromatography and analyzed by HPLC. A fraction was purified from A. brevifolia Mill showed the most effective scavenging activities on 〓 and ·OH (66. 01% and 38. 98% respectively). With the analysis of IR spectrum, UV spectrum and mass spectrum, the structure of FA was identifed as 8-C-D-glucopyranosyl-2- [2-hydroxy] propyl-5-methyl-7-hydroxychromone. Its scavenging activity on free radicals is higher than that of aloe-emodin. Its antioxidant activity may be due to the phenoxyl on glucosyl chromone which can be react with free radicals and form relatively stable free radicals.

本研究利用分别产生超氧阴离子自由基和羟自由基的化学模型体系研究比较了不同品种芦荟提取物的清除活性氧自由基的抗氧化作用，进一步利用硅胶柱结合薄层层析法和反相高压液相色谱法，从短叶芦荟叶子中首次分离了具有较强自由基清除能力（超氧阴离子自由基和羟自由基清除率分别为66.01％和38.98％）的成分FA，利用红外光谱、紫外光谱和质谱等仪器分析结果推断出该活性成分的分子结构为8-C-吡喃葡萄糖-2-[2-羟基]-丙基-5-甲基-7-羟基对氧萘酮，它的自由基清除能力高于芦荟大黄素，是一种天然抗氧化剂。

By comparison between SMM HXRBS observation and ground observation of Hα and CaIIK lines, especially through the combined study between SMM HXRBS observation and chromospheric flare models, the results show that: in the initial stage of impulsive phase, there is a correlative relation betweem Hα line intensity and hard X-ray emission; different spike in hard X-ray flux curve represents the burst at different location; the energy taken by non-thermal electron beam is larger than the radiative loss in chromosphere; for the flare studied here, the chromospheric evapporation is explosive; if the chromosphere is in balance between electron beam bombardment and radiative loss, the column mass density at the top of chromospheric flare model can not be taken as measure from the source of electrons and then the total material between the source of electrons and the top of chromosphere can be estimated.

通过一个具体耀斑的SMM HXRBS观测结果与同时基于地面得到的Hα和CaⅡK可见光谱观测结果对比，特别是将硬x谱观测结果与色球半经验模型联立研究，结果显示出：在脉冲相上升段，硬x发射与Hα辐射之间存在对应关系；硬x线光变曲线中不同脉冲爆发分量不太可能起源于同一位置；硬x辐射所反映的高能非热电子总携带能量大于色球总辐射损失；对所研究的耀斑而言，其色球蒸发过程是爆发性的；在详细比较了非热电子色球总沉积和色球辐射损失的基础上，指出半经验模型中色球顶部柱数密度不能看成是从非热电子源度量的，从而估计了色球顶部到非热电子源之间的总物质。

Guide slots (108) in a guide sleeve (32) receive a stop pin (52) carried by a plunger shaft (48), and the slots (108) define two axially and circumferentially spaced lower stops (104, 106) for aspirating and dispensing strokes respectively.

在引导衬套(32)中的引导狭槽(108)装有止动器销(52)，该止动器销(52)装在柱塞杆(48)上，该狭槽(108)确定了两个轴向和周向间隔开的下部止动器(104、106)，分别用于吸取冲程和分配冲程。

During annealing process, two steps occured: one is the propergation of the copper nanograins towards silicon pillars; and the other is the coalescent of the adjacent nanoparticles.

在退火过程中，铜纳米颗粒发生了两个变化：一是铜纳米颗粒向硅柱的运动；二是铜纳米颗粒间的合并。

The gigantic columned hall of that temple was partially built during his reign.

神殿中巨大的多柱厅，有一部分是在他统治的时期建造的。

Then, columniform detonator blast under water is simulated.

然后计算了柱形炸药在无限水域中爆炸时，几种不同起爆方式下炸药的爆炸威力。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。