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With increasing DMFcontent in mixed solvents, the dipolar attracting interactions betweenglycine molecules increase; the attracting interactions arising fromhydroxyl groups between L-serine molecules increase rapidly; the repulsing interactions involving apolar side-chains between L-valine moleculeshave little fluctuate. By the present of ethanol, attractions arising fromhydroxyl groups increase obviously, repulsions arising from apolarside-chains decrease.

随溶液中DMF含量的增大,甘氨酸和L-丝氨酸两分子间的偶极吸引作用逐渐增大。L-丝氨酸羟基的吸引作用影响更加明显,因此增加速度较快。L-缬氨酸非极性侧基的排斥作用变化略有波动。

By virtue of method of continuum approximate limit, we obtained the solitons of the vibration of lattice in one-dimensional harmonic and inharmonic chains of polarized molecule, under the conditions considering and inconsidering the interaction of exciton with phonon, through solving moving equations of exciton and phonon.

运用连续极限近似方法,通过求解声子和激子的运动方程,得到了在不考虑激子与声子的相互作用和考虑激子与声子相互作用两种情况下的极性分子简谐链和非简谐链中晶格振动的孤子解,并得出了激子与声子的相互作用的非线性效应类似于晶格三次势的非线性效应,以及相同的非线性效应不论是同时作用还是单独作用都具有相同的非线性效应的结论。

The adjustment of X9241 is controlled by SCM according to the polarity of imbalance voltage signal from the output of the circuit bridge, and the adjusting of the balance of bridge and of controller is realized automatically.

单片机根据电压比较电路敏感电桥两臂不平衡电压输出信号的正负极性控制X9241,实现电桥平衡和控制器的自动调节。X9241采用二线串行I2C总线与单片机传递数据。

The aroma components of blood orange fruit were extracted by headspace solid phase microextraction and investigated by gas chromatography-mass spectrometry with two GC columns of different polarity(HP-5 and DB-WAX).

采用顶空固相微萃取对血橙的香气成分进行提取,用两个不同极性的色谱柱(HP-5和DB-WAX)进行分离,利用气相色谱-质谱联用技术对香气成分进行分析。

Visco-elasticity of micro-polar fluid is characterized by two parameters of coupling number and molecular characteristic length.

微极性流体的粘弹特性由耦合数和分子特征长度两个参数决定。

The pure screw dislocation is easily etched along the steps that the dislocation terminates. Consequently a small Ga-polar plane is formed to prevent further vertical etching,resulting in an etch pit shaped like an inverted truncated hexagonal pyramid at the terminal chiasma of two surface steps.

纯螺位错易于沿着由它结束的表面阶梯被腐蚀,形成一个小的Ga极性面以阻止进一步的纵向腐蚀,因而其腐蚀坑是位于两个表面阶梯交结处的截底倒六棱椎。

Also the molecular structure and functional effects of this active component were studied in detail. 1 Extraction, separation, purification and structural identification of the functional component in Chufa After initial handling of waste slurry to solid powder, ethanol was used to lixiviate it followed by the extraction with petroleum ether,ethyl acetate,n-butyl alcohol one by one, the polarity of three organic reagents being changed from low to high.

荸荠功能因子的提取、分离、纯化及结构鉴定以马蹄粉厂产粉废浆为原料,经过实验室初处理成固态原料粉后,用乙醇浸提,再将浸提物以水悬浮,依次通过极性从小到大的石油醚、乙酸乙酯、正丁醇三种有机溶剂两相萃取分部,并以金黄葡萄球菌、枯草芽孢杆菌和致病大肠杆菌为指示菌,检测上述各部分提取物的功能效果。

A device and method for preparing compound nano fiber endless tow, which contains feeding material liquid to pair of electric spinning nozzle on frame, each nozzle respectively applied with high dc voltage with opposite polarity, each pair of nozzle jetting out nano fiber with opposite electric charge, said nano fiber attracting and colliding each other to form compound nano fiber, then forming nano fiber endless tow after drawing and stretching, the first opposite set pair of electric spinning nozzle jetted compound nano fiber endless tow is stretched down and used as acceptor which covered by the nano fiber jetted by second pair of nozzle an d forming two layers of compound nano fiber endless tow after drawing and stretching, in turn to get multilayer compound nano fiber endless tow after drawing and stretching by godet roller.

复合纳米纤维长丝束制备装置及其制备方法是一种简单、高效电纺制备纳米纤维长丝束的方法,其步骤为将料液输送给支架(3)上的电纺喷头对(1);喷口相向的电纺喷头对(1)的每个喷头分别施加相反极性的直流高电压;每对相向喷口喷出分别带相反电荷的纳米纤维,并在空中相互吸引、碰撞形成复合纳米纤维,经牵引、拉伸后形成复合纳米纤维长丝束;第一对相向放置的电纺喷头纺丝形成的复合纳米纤维长丝束向下拉伸,并作为接受体与第二对电纺喷头喷出的分别带相反电荷并相互吸引的纳米纤维在空中相遇,被第二对电纺喷头喷出的纳米纤维包裹,经牵引、拉伸后形成两层复合纳米纤维长丝束;依次类推,最后经导丝辊对(2)牵引、拉伸后得到多层复合纳米纤维长丝束。

The contents of alt and ast in the serum were determined by chromatometry 16hr after administration of ccl4. resultsthe five kinds of extracts extracted by different heteropolarity dissolvents but ligarine extract, the free and conjugated anthraquinones significantly decreased the activities of aminopherase.

结果以不同极性溶剂提取的5种决明子提取物中,除石油醚部分外,其余各组均有显著降低转氨酶活性的作用;游离型和结合型蒽醌均有显著的降低转氨酶活性作用;决明子的生、炒两类炮制品也同样有显著的降酶作用,但生品略优。

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应,用茚〓和1,1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物,发现可控制反应条件,使1,1'-联茚与〓反应,并高产率地得到具有新颖结构的单加成物,用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征,测得它的两个〓杂化的桥头碳的化学位移为〓ppm,证明生成的衍生物为6∶6闭式环加成,〓NMR谱中共给出38个信号,表明〓联茚衍生物分子具有〓对称性;在波长532nm,脉冲宽度8ns的激光下,〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近,由于〓联茚单加成衍生物熱稳定性好,在四氢呋喃,丙酮等极性溶剂中溶解性好,能分别均匀地掺入溶胶-凝胶中,已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能;使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究,通过等温压缩曲线测试,证明浓度为〓〓时,〓联茚衍生物能够形成单层膜。

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