丙酮醛

Briefly, coronal brain sections (100 mm)were cut with a vibratome, postfixed with 4% glutaraldehydein 0.1 mmol/L cacodylate buffer (pH 7.4) for 1 h, andthen with 1% osmium tetroxide in 0.1 mmol/L cacodylatebuffer for 2 h. After rinsing with distilled water, the brainsections were treated with 1% aqueous uranyl acetateovernight, dehydrated in an ascending series of ethanolsto 100%, followed by dry acetone, and then embedded inDurcupan ACM. Ultrathin sections (0.1 mm) were cut andstained with 3% lead citrate and subsequently examinedwith a Zeiss transmission electron microscope (Zeiss Inc.,Thornwood, NY, USA).

简单的说，先用切刀制成100um的冠状脑切片，然后用含有4%戊二醛在0.1 mmol/L的二甲砷酸缓冲液(PH7.4)中固定1小时后，放在含有1%四氧化锇的0.1 mmol/L的二甲砷酸缓冲液中2小时，接着用蒸馏水冲洗后，放在1%的aqueous uranyl acetate中过夜，接下来用梯度酒精(至100%)脱水，然后用丙酮干燥，再用Durcupan ACM包埋，切成0.1um的超薄切片后用3%的lead citrate染色，随后用透射电子显微镜观察。

In the second part of the thesis, we discussed a L-proline-catalyzed direct Aldol reaction between L-amino acid-derived N,N-dibenzyl -amino aldehydes 15 and acetone, cyclopentanone or hydroxyacetone, which afforded (-amino--hydroxy- or (-amino-,(-dihydroxy-ketones in good to excellent yields (up to 94%) and diastereoseletivities (up to 94.9%).

发现许多情况下，反应的产率和de值超过90%。接着，在碱性条件下，我们将L-亮氨酸衍生的N，N-二苄基--氨基醛15g与羟基丙酮反应得到的主要产物(，-二羟基-γ-氨基酮171d与次溴酸钠反应，得到了具有抗肿瘤活性的天然产物PM-94128的氨基酸片断184。

The results of the herbicidal effects study display that 1,4-dioxoquinoxaline formaldehyde-salicylic aldehyde dihydrazone and 1,4-dioxoquinoxaline formaldehyde acetone dihydrazone have obvious herbicidal activity.

研究结果表明1，4-二氧喹喔啉-2-甲醛-水杨醛双腙和1，4-二氧喹喔啉-2-甲醛-丙酮双腙表现较明显的活性，在500mg/L浓度时对稗草的株防效分别为51.3%和55.0%；对油菜株防效较弱，分别只有33.5%和17.5%。

Total volatile components, acetone, cyclohexadiene, cyclopentyl ethyne, acetic acid and hexanal contents show more significant correlation with storage time, physiological biochemical indexes respectively, and it can be used as an assessment index for the storage quality of stored maize.

总挥发性物含量、丙酮、对环己二烯、环戊乙炔、乙酸、己醛的含量与储藏时间、生理生化指标呈较高相关性，可作为玉米储存品质变化的评判指标。

Thus,α,β-unsaturated ketones were prepared by base-catalized aldol condensation between substituted arylaldehydes and acetones. Using iodosobenzene diacetate as oxidants, the resulting α,β-unsaturated ketones will be transformed to β,γ-unsaturated carboxylic acid esters.

以不同取代的芳香醛跟丙酮缩合后可以得到α，β-不饱和酮，再用iodosobenzene diacetate做氧化剂氧化，可以成左卤o到β，γ-不饱和碳酸酯类化合物。

Several routes for synthesizing methyl isopropyl ketone were introduced, including the main methods based on isobutyl aldehyde-acetic acid, isobutyric acid -acetic acid, methyl ethyl ketone-formaldehyde and isoprene.

介绍了甲基异丙酮的多种合成路线，主要有异丁醛-乙酸法、异丁酸-乙酸法、甲基乙基酮-甲醛法和异戊二烯法。

Finally confirmed that,The thighbone and the osteoporosis morbidity is possibly connected protein 6, respectively are: The lactoferrin light chain, membrane association protein A3, the enolase, ATP gather the enzyme, the acetyl coenzyme A reductases, the myo calcium protein; The lumbar vertebra and the osteoporosis morbidity is possibly connected protein 5, respectively are: The actin, the keratin, the enolase, ATP gather the enzyme, the myosin; The thighbone and the strong bone valuable curative effect is possibly connected protein 9, respectively are: The enolase, ATP gather the enzyme, the myo-calcium protein, the creatine activating enzyme isozyme, the phosphoglyceric acid change flavor the enzyme, the myosin, the lactoferrin light chain, the pyruvic acid activating enzyme isozyme, the crown protein; The lumbar vertebra and the strong bone valuable curative effect are possibly connected protein 8, respectively are: The carbonic anhydrase, the actin, the αB-crystal protein, 3-phospho-glycerol aldehyde oxidase, the serum albumin, ATP gather the enzyme, the myosin, the enolase.

最后确认：股骨与骨质疏松发病可能相关的蛋白6个，分别为：乳铁蛋白轻链、膜联蛋白A3、烯醇化酶、ATP合酶、乙酰辅酶A还原酶、肌钙蛋白；腰椎与骨质疏松发病可能相关的蛋白5个，分别为：肌动蛋白、角蛋白、烯醇化酶、ATP合酶、肌球蛋白；股骨与强骨宝疗效可能相关的蛋白9个，分别为：烯醇化酶、ATP合酶、肌钙蛋白、肌酸激酶同工酶、磷酸甘油酸变味酶、肌球蛋白、乳铁蛋白轻链、丙酮酸激酶同工酶、冠蛋白；腰椎与强骨宝疗效可能相关的蛋白8个，分别为：碳酸酐酶、肌动蛋白、αB-晶体蛋白、3-磷酸甘油醛脱氢酶、血清白蛋白、ATP合酶、肌球蛋白、烯醇化酶。

The results showed that Kaidimycin was chemically neutral, macrocylic polylactones, stable and liable to dissolve into water and pyridine, slight to dissolve into methanol, ethanol and N-butanol, difficult to dissolve into ethyl acetate, acetone, benzene and chloroform. Chemical reaction of functional group of Kaidimycin showed that it had glycoside, amino acid and aldehyde, no reducing sugar, polypeptide and phenol.

凯地菌素属中等极性的、中性抗生素，极性纸层析结果与多烯类抗生素的纸层析结果相似：易溶于水、吡啶，微溶于甲醇、乙醇、正丁醇，不溶于乙酸乙酯、丙酮、苯、三氯化碳；对高温、光照和紫外处理有很好的稳定性；官能团反应试验结果发现，凯地菌素可能含有糖苷键、氨基酸伯氨基和醛基，不含有还原糖、多肽和酚基，高锰酸钾、浓硫酸反应与多烯大环内酯类抗生素的特性相似；并且依据纯品，采用生物法和分光光度法对摇床发酵液进行了效价的测定。

Aluminum ; Acetone ; 2; 15-Hexadecanedion ; Computer simulation ; Aldol condensation

氧化铝；丙酮； 2； 15－十六烷二酮；计算机模拟；醛醇缩合

In the Aldol condensation of acetone with 4-nitrobenzaldehyde, two different hybrid secondary amine-functionalized mesoporous materials displayed enhanced catalytic performance in comparison to primary amine-functionalized materials. The possible reason is that the presence of organic functional groups with larger steric hindrance led to the enhanced catalytic performance of basic amino groups.

在对硝基苯甲醛和丙酮的羟醛缩合反应中，相对于一级胺功能化的材料，二级胺功能化的SBA-15展示了极大改进的催化活性，这可能是由于具有更大空间位阻效应的有机功能团的引人导致了碱性胺中心催化活性增强。

Now, however, all children continue in "comprehensive" schools, and the eleven-plus determines which courses of study the child will follow.

然而现在，所有的孩子都要在综合学校继续学习，所以这次考试只是决定他们将要学习哪些课程。

Cultivatable land , and led to a general recognition that development must not be carried at the cost of agriculture .

城区的迅速扩大在很多情况下侵占了宝贵的可耕地，使人们普遍认识到发展不能以牺牲农业为代价。